Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      124 059
      Simultaneous high-performance thin-layer chromatographic quantification of withaferin A and withanolide A in Solanum nigrum L. “Black Nightshade”
      R. PREET*, R. GUPTA, M. KAUR (*Department of Botany, Punjabi University, Patiala, India, ramanbrar247@gmail.com)

      J. Planar Chromatogr. 32, 339-342 (2019). HPTLC of withaferin A (1) and withanolide A (2) in Solanum nigrum on silica gel with toluene - ethyl acetate - formic acid - ethanol 60:30:1:6. Detection by spraying with p-anisaldehyde sulfuric acid (1 mL of p-anisaldehyde solution in 2 mL of concentrated sulfuric acid and 100 mL of acetic acid). Quantitative determination by absorbance measurement at 530 nm. The hRF values for (1) and (2) were 43 and 55, respectively. 

      Classification: 14
      124 001
      Cytotoxic flavones from the stem bark of Bougainvillea spectabilis Willd.
      L.T.M. DO, T. AREE, P. SIRIPONG, N.T. VO, T.T.A. NGUYEN, P.K.P. NGUYEN, S. TIP-PYANG* (*Department of Chemistry, Faculty of Science, Chulalongkorn University, Bangkok, Thailand; santi.ti@chula.ac.th)

      Planta Medica 84(2), 129-134 (2018). TLC of subfractions obtained from normal-phase LC and size-exclusion chromatography of an ethanolic extract of Bougainvillea spectabilis (Nyctaginaceae) stem-bark on RP-18 with methanol – water 2:3 and 1:1 to isolate six flavones (bougainvinones J, K, L, M, and two dimethylflavone derivatives).

      Classification: 8a, 32e
      124 002
      Three new abietane-type diterpenoids from Plectranthus africanus and their antibacterial activities
      R.T. NZOGONG, B.K. NGANOU, A.T. TEDONKEU, M.D. AWOUAFACK, M. TENE*, T. ITO, P. TANE, H. MORITA** (*Laboratory of Natural Products Chemistry, Department of Chemistry, Faculty of Science, University of Dschang, Dschang, Cameroon; ** Institute of Natural Medicine, University of Toyama, Toyama, Japan; * mtene2001@yahoo.fr; ** hmorita@inm.u-toyama.ac.jp)

      Planta Medica 84(1), 59-64 (2018). A multi-step fractionation through silica gel column chromatography (CC) of a methanolic extract of Plectranthus africanus (whole plant, Lamiaceae) was monitored through TLC on silica gel with various solvent mixtures (n-hexane or dichloromethane with either acetone or methanol). Zones were detected under UV and further by spraying with sulfuric acid 20 % and heating at 100°C. For each fraction or TLC profile, the authors provide the CC gradient, the optimal proportions of the solvents used for the TLC mobile phase, as well as the RF values of the molecules isolated by this CC method: new abietane-type diterpenoids (plectranthroyleanones A, B, C), betulinic and oleanolic acids, heterosides of apigenin, rhamnetin and sitosterol.

      Keywords: herbal
      Classification: 8a, 14, 15a, 32e
      124 045
      Bioactivity-guided investigation of the anti-inflammatory activity of Hippophae rhamnoides fruits
      D. RÉDEI, N. KÚSZ, N. JEDLINSZKI, G. BLAZSÓ, I. ZUPKÓ, Judit HOHMANN* (*Department of Pharmacognosy, University of Szeged, Szeged, Hungary; hohmann@pharm.u-szeged.hu)

      Planta Medica 84(1), 26-33 (2018). For the monitoring of the multi-step fractionation through VLC (vacuum liquid chromatography) of the chloroform-soluble parts of a methanol – water 7:3 percolate of Hippophae rhamnoides (Eleagnaceae) fruit peels, TLC on silica gel and RP-18, detection by spraying with sulfuric acid and heating. Preparative TLC on silica gel with cyclohexane – dichloromethane – methanol 5:15:1 to isolate, from VLC subfractions, three lignans (nectandrin B, fragransin A2, saucernetindiol) that are diastereoisomers of each other.

      Classification: 7, 8b, 32e
      124 015
      Denudatin A, a dimeric acylphloroglucinol from Hypericum denudatum presents an antinociceptive effect in mice
      H. BRIDI, G. de CARVALHO MEIRELLES, S. A. de LORETO BORDIGNON, St. M. KUZE RATES, Gilsane LINO von POSER* (*Laboratory of Pharmacognosy, Faculty of Pharmacy, Federal University of Rio Grande do Sul, Porto Alegre, Brazil; gilsane@farmacia.ufrgs.br)

      Planta Medica 83(17), 1329-1334 (2017). Two acetone-soluble subfractions of an n-hexane maceration of Hypericum denudatum aerial parts (Hypericaceae) were submitted to repeated centrifugal planar chromatography (CPC) on silica gel using n-hexane – ethyl acetate (gradient from 100:0 to 90:10), obtaining four dimeric acylphloroglucinols (denudatin A, hyperbrasilol A, uliginosin B and isouliginosin B), which were purified by crystallisation with n-hexane – dichloromethane 9:1. From the most apolar CPC eluates, a monomer (selancin A) was isolated on preparative TLC silica gel layer by elution with n-hexane – ethyl acetate 97:3. Furthermore, all the purification steps were monitored through TLC on silica gel with n-hexane – ethyl acetate 19:1 or with n-hexane – dichloromethane 1:1. Detection under UV light after derivatization with anisaldehyde – sulfuric acid, monomeric acylphloroglucinols appeared purple, whereas dimers appeared yellow-orange.

       

       

       

      Classification: 7, 32e
      124 037
      Comparison between HPLC and HPTLC densitometry for the determination of spinosin from Ziziphus jujuba Mill. fruit extracts
      Z. SOBHANI, S. EMAMI, O. RAJABI* (*Department of Pharmaceutical Control, School of Pharmacy, Mashhad University of Medical Sciences, Mashhad, Iran, Rajabio@mums.ac.ir)

      J. Liq. Chromatogr. Relat. Technol. 42, 563-569 (2019). HPTLC of spinosin in the fruits of Ziziphus jujuba on silica gel with ethyl acetate - dichloromethane - methanol - water 18:10:15:5. Quantitative determination by absorbance measurement at 334 nm. The hRF value for spinosin was 38. Linearity was between 10 and 120 ng/mL. Intermediate precision was below 2 % (n=6). The LOD and LOQ were 12 and 35 ng/mL, respectively. Recovery rate was between 98.7 and 101.3 %. The HPTLC method provided similar reproducibility, accuracy and selectivity for the quantitative determination of spinosin compared with a HPLC method.

      Classification: 8a
      124 049
      Simultaneous quantification of pharmacological markers quercetin and berberine using high-performance thin layer chromatography (HPTLC) and high-performance liquid chromatography (HPLC) from a polyherbal formulation Pushyanuga Churna
      S. SHAILAJAN*, Y. PATIL, M. JOSHI, S. MENON, M. MHATRE (*Herbal Research Laboratory, Ramnarain Ruia Autonomous College, Matunga, Mumbai, India, sunitashailajan@gmail.com)

      J. AOAC Int. 102, 1003-1013 (2019). HPTLC of quercetin (1) and berberine (2) in Pushyanuga Churna on silica gel with toluene - ethyl acetate - methanol - formic acid 6:6:2:1. Quantitative determination by absorbance measurement at 254 nm for (1) and 366 nm for (2). The hRF values for (1) and (2) were 63 and 24, respectively. Intermediate precisions were below 2 % (n=3). The LOD and LOQ were 1 and 3 µg/mL for (1) and 0.05 and 0.1 µg/mL for (2), respectively. Recovery rate was between 93.5 and 100.6 % for (1) and 95.2 and 97.6 % for (2).

      Classification: 8a
      124 061
      Tempeh & soybean seed coat: the alternative sources of trans-resveratrol as neuroprotective agents
      Yulia IRNIDAYANTI*, D. SUTIONO (*Departement of Biology, Faculty of Mathematics and Science, Universitas Negeri Jakarta, Hasyim Asyarie Building, Rawamangun muka, Indonesia, yirnidayanti@unj.ac.id)

      Int. J. Morphol. 37, 1164-1171 (2019). HPTLC of transresveratrol in traditional fermented soybean seed coat on silica gel with chloroform - ethyl acetate - formic acid 25:10:1. Qualitative identification under UV light at 254 and 366 nm. The hRF value for transresveratrol was 64.

      Classification: 7
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