Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      112 127
      (Qualitative and quantitative determination of the effective components of Aristolochia fangchi in Fufang Hafangji Keli granules) (Chinese)
      SH. ZHANG (Zhang Shuyu)*, Y. YU (Yu Yanli), SH. LIU (Liu Shijun), Y. BI (Bi Yunsheng), CH. NI (Ni Chenming) (*General Hosp. of Jinan Milit. Area, Shandong, Jinan 250031, China)

      J. of China Pharm. 27 (7), 725-728 (2013). Fufang Hafangji Keli granules, with Aristolochia fangchi as key component drug, are a herbal TCM preparation for improving the liver function, and are used for treatment of acute and chronic hepatitis, cirrhosis, and fatty liver. TLC of the extracts and standards (+)-tetrandrine and fangchinoline on silica gel with cyclo hexane – chloroform – acetone – methanol 10:6:1:1, detection by spraying with (bismuth subnitrate – glacial acetic acid – water 1:10:40) – potassium iodide – glacial acetic acid – water 1:1:4:20. Quantification of (+)-tetrandrine and fangchinoline by HPLC.

      Classification: 32c
      113 028
      Determination of antidiabetic polysaccharides of Ocimum basilicum seeds indigenous to Xinjiang of China by high-performance thin-layer chromatography–UV/Vis–mass spectrometry
      A. YILI (Yili Abulimiti), H. YIMAMU (Yimamu Hurxid), S. GHULAMEDEN (Ghulameden Saideiahmat), Z. QING (Qing Zhao Hai), H. AISA (Aisa Haji), Gertrud MORLOCK* (*Food Science, Justus Liebig University Giessen, Institute of Nutritional Science, Heinrich-Buff-Ring 26-32, 35392 Giessen, Germany, gertrud.morlock@ernaehrung.uni-giessen.de)

      J. Planar Chromatogr. 27, 11-18 (2014). HPTLC of fructose (1), glucuronic acid (1), galacturonic acid (3), rhamnose (4), xylose (5), arabinose (6), and galactose (7) in the seeds of Ocimum basilicum on silica gel with isopropyl acetate - ethyl acetate - ethanol - water 50:40:10:1. Detection by dipping into aniline diphenylamine o-phosphoric acid reagent (20 % of o-phosphoric acid [85%] added to 1:1 mixture of 2 % solutions of diphenylamine and aniline in acetone), followed by heating at 110 ºC for 5 min. Quantitative determination by absorbance measurement at 630 nm except for (4) which was determined at 370 nm. The hRF values for (1) to (7) were 80, 58, 51, 40, 25, 18 and 9, respectively.

      Classification: 10a
      113 072
      Simultaneous estimation of kaempferol, rutin, and quercetin in various plant products and different dosage
      forms of Bhuiamla and Amla
      S. JIRGE, P. TATKE*, S. GABHE (*Shah College of Pharmacy, S.N.D.T. Women’s University, Mumbai 400 049, India, patatke@gmail.com)

      J. Planar Chromatogr. 27, 267-273 (2014). HPTLC of kaempferol (1), rutin (2), and quercetin (3) in marketed formulations containing_x000D_ Phyllanthus niruri (Bhuiamla) and Emblica officinalis (Amla) on silica gel with chloroform - methanol - formic acid 82:15:10. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (3) were 69, 53 and 12. Linearity was in the range of 21-840 ng/zone for (1), 56-1008 ng/zone for (2) and 60-1800 ng/zone for (3), respectively. The intermediate/interday/intra-day precisions were below 1 % (n=3). The LOD and LOQ were 21 and 63 ng/zone for (1), 56 and 168 ng/zone for (2) and 300 and 600 ng/zone for (3), respectively. Recoveries for (1) to (3) were obtained in the range of 81.8-119.0 %.

      Classification: 32e
      113 096
      (Identification of olibanum and illegally adulterated colophony in Xihuang Wan pills and Huoxue Zhitong San powders by thin-layer chromatography) (Chinese)
      L. SUN (Sun Lei)*, Y. LIU (Liu Yan), Y. PENG (Peng Yu), H. JIN (Jin Hongyu) (*National Inst. for Food & Drug Contr., Beijing 100050, China)

      J. of China Pharm. 27 (7), 722-724 (2013). Xihuang Wan pill is a herbal TCM prescribed for treatment and adjuvant therapy of various cancers. Huoxue Zhitong San powder is a herbal TCM prescribed for traumatic injury and ecchymoma. In the drug market fraud rosin was found to be added to the key ingredient olibanum. For quality control, HPTLC of the sample extracts and the standards acetyl-11-keto-beta-boswellic acid (AKBA), 11-keto-beta-boswellic acid (KBA), beta-boswellic acid (beta-BA), acetyl-beta-boswellic acid (beta-ABA), and abietic acid (LOD=1.0 µg), on silica gel with toluene – ethyl acetate – heptane – formic acid 80:20:10:3 with chamber saturation for 20 min, detection 1) under UV 254 nm and UV 366 nm; 2) by spraying with a fresh solution of anisaldehyde – sulfuric acid – acetic acid 1:10:1000 and heating at 105 °C until the zones were visible in daylight. Verification of abietic acid from added rosin by HPLC. The method was used for the analysis of 63 batches of Xihuang Wan pills sampled from 13 pharmaceutical factories and 10 batches of Huoxue Zhitong San powder from 4 factories.

      Classification: 32e
      113 114
      (Study of the method for the quality control of Gushangling Jiaonang capsules by high-performance thin-layer chromatography) (Chinese)
      M. ZHENG (Zheng Meishan)*, X. CUI (Cui Xuan), L. XU (Xu Lianhua) (*Yanbian State Inst. for Food & Drug, Jilin, Yanji 133000, China)

      J. of China Pharm. 22 (3), 13-15 (2013). Gushangling Jiaonang capsule is a herbal TCM for post traumatic functional recovery, prescribed to treat muscle atrophy, bone hyperplasia, neck and lumbar diseases, nerve injuries etc. For quality control, HPTLC on silica gel 1) for Paeonia lactiflora Pall., with chloroform – ethyl acetate – methanol – formic acid 200:25:50:1, detection by spraying with 3 % vanillin in sulfuric acid – water 1:200 and heating mildly until the zones are visible in daylight; 2) for Angelica sinensis, with n-hexane – ethyl acetate – 9:1, detection under UV 366 nm; 3) Astragalus membranaceus (Fisch.) Bunge., with chloroform – methanol – water 13:7:2, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible in daylight.

      Classification: 32e
      114 024
      A developed and validated high-performance thin-layer chromatographic method for the quantitative determination of quercetin in Satyrium nepalense tubers
      A. MISHRA*, S. SAKLANI, V. PARCHA, L. MILELLA (*Department of Pharmaceutical Chemistry, H.N.B. Garhwal (A Central) University Srinagar Garhwal, 246174 Uttarakhand, India, abhaypharmachemhnbgu@gmail.com)

      J. Planar Chromatogr. 27, 444-448 (2014). HPTLC of quercetin in fresh tubers of Satyrium nepalense on silica gel with toluene – ethyl acetate – formic acid 7:5:1. Quantitative determination by absorbance measurement at 366 nm. The hRF value of quercetin was 54. Linearity was in the range of 2-12 μg/zone. The intermediate intra-day and inter-day precisions were below 1 % (n=3) for quercetin. The LOD and LOQ was 40 and 120 ng/zone, respectively. Mean recovery for quercetin was 99.8 %.

      Classification: 8a
      114 061
      (Study of the method for the quality control of Danggui Buxue Wan pills) (Chinese)
      X. BI (Bi Xiaoli)*, Q. CHENG (Cheng Qingyun), S. LI (Li Sumei) (*Guangdong Prov. Inst. of TCM, Guangdong, Guangzhou 510095, China)

      Shanxi J. Trad. Chinese Med. 9, 43-46 (2013). Danggui Buxue Wan pill is TCM compound for the treatment of psoriasis (blood dryness type), chronic eczema, neurodermatitis, skin pruritus and other skin diseases. For the quality control, TLC on silica gel (1) for Angelica sinensis with cyclohexane – dichloromethane – ethyl acetate – formic acid 4:1:1:0.1, detection at UV 366 nm; (2) for Fallopia multiflora (Thunb.) Harald. with the upper phase of toluene – ethyl acetate – formic acid 20:2:1, detection at UV 366 nm; (3) for Paeonia lactiflora Pall. with chloroform – ethyl acetate – methanol - formic acid 45:5:10:0.2, detection by spraying with 5% vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C until the spots were visible. All were identified by fingerprint comparison with the standard (paeoniflorin or ferulic acid) and/or the standard ingredient drug.

      Classification: 4d, 32e
      114 086
      (Studies of the improved method for the quality control of Tiaojing Huoxue Jiaonang capsules) (Chinese)
      F. PENG (Peng Feicheng)*, Y. DING (Ding Ye), J. ZHENG (Zheng Jinfeng), W. LI (Li Wen Li) (*Hunan Provinc. Inst. for Food & Drug Contr., Hunan, Changsha 410001, China)

      Strait Pharm. J. 1, 53-55 (2014). Tiaojing Huoxue Jiaonang capsule is a TCM compound used clinically for the treatment of irregular menstruation, menstrual pain and other gynecological diseases. TLC on silica gel (1) for Salvia miltiorrhiza Bunge and protocatechuic aldehyde with dichloromethane – acetone – formic acid 60:5:2, detection by spraying with 5 % ferrum trichloride in ethanol and viewing under white light; (2) for Rehmannia glutinosa (Gaert.) Libosch. ex Fisch. et Mey. with petroleum ether (60-90 ˚C) – ethyl acetate 1:1, detection under white light after spraying with 2,4-dinitrophenylhydrazine – ethanol – hydrochloric acid 1:100:10. Quantitative determination of paeoniflorin by HPLC. Applying to real life samples indicated that the method was simple, specific, accurate, reproducible, robust and able to be the better alternative for the purpose to that specified in the Chinese Pharmacopoeia 2010.

      Classification: 4d, 32e
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