Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      118 039
      In vitro and in vivo assessment of meadowsweet (Filipendula ulmaria) as anti-inflammatory agent
      J. KATANIC*, T. BOROJA, V. MIHAILOVIC, S. NIKLES, S. PAN, G. ROSIC, D. SELAKOVIC, J. JOKSIMOVIC, S. MITROVIC, R. BAUER (*Department of Chemistry, Faculty of Science, University of Kragujevac, Radoja Domanovi?a 12, 34000 Kragujevac, Serbia, jkatanic@kg.ac.rs)

      J. Ethnopharmacol. 193, 627-636 (2016). HPTLC of hyperoside (1), rutoside (2), apigenin (3), spiraeoside (4), quercetin (5), and isoquercitrin (6) on silica gel with ethyl acetate – formic acid – glacial acetic acid – water 100:11:11:26. Detection by spraying with natural product/PEG reagent, followed by drying for 10 min. Quantitative determination by absorbance measurement at 366 nm. The hRF values for (1) to (6) were 55, 37, 95, 6, 92 and 57, respectively._x000D_

      Classification: 8a
      118 066
      Aphrodisiac and spermatogenic potential of alkaloidal fraction of Hygrophila spinosa T
      N. VYAS*, M. RAVAL (*Department of Pharmacognosy, Ramanbhai Patel College of Pharmacy, Charotar University of Science and Technology, CHARUSAT Campus, Changa, 388421, Ta-Petlad, Dist-Anand, Gujarat, India, nirajvyas.ph@charusat.ac.in)

      Ander in rats. J. Ethnopharmacol. 194, 947-953 (2016). HPTLC of alkaloid (1) and (2) in the whole plants of Hygrophila spinosa on silica gel with hexane – dichloromethane – methanol 5:90:8. Detection by spraying with Dragendorff's reagent and drying at room temperature. Qualitative identification at 520 nm. The hRF values for (1) and (2) were 48 and 56, respectively.

      Classification: 22
      119 041
      Anti-inflammatory activity of Crateva adansonii DC on keratinocytes
      infected by Staphylococcus aureus – From traditional practice to scientific
      approach using HPTLC-densitometry
      K. AHAMA, C. BODET, A. QUASHIE, M. GARCIA, I. THERY, J. DORAT, C. DE SOUZA, C. ENGUEHARD, L. BOUDESOCQUE* (*Université de Tours, UMR INRA 1282 Infectiologie et Santé Publique, 31 avenue Monge, 37200 Tours, France, leslie.boudesocque@univ-tours.fr)

      J. Ethnopharmacol. 204, 26-35 (2017). HPTLC of quercitrin (1), isoquercitrin (2), quercitrin-3-O-β-D-xylopyranosyl-α-L-rhamnopyranoside (3) on silica gel with ethyl acetate – formic acid – acetic acid – water 100:11:11:26. Detection by spraying with NEU`s reagent (diphenylborinic acid 2-aminoethylester, natural product reagent), followed by drying at 110 °C for 2 min. Quantitative determination by absorbance measurement at 265 nm. LOD and LOQ were 31 ng/zone and 75 ng/zone for (2). Recovery was between 99.8 and 101.1 % for (2). Intermediate precision was <2 % (n=3).

      Classification: 8a
      119 065
      Pharmacokinetics and comparative metabolic profiling of iridoid enriched fraction of Picrorhiza kurroa – An Ayurvedic Herb
      S. ZAHIRUDDIN, W. KHAN, R. NEHRA, M. JAVED, N. MALLICK, R. PARVEEN, S. AHMAD* (*Bioactive Natural Product Laboratory, Department of Pharmacognosy and Phytochemistry, Faculty of Pharmacy, Jamia Hamdard (Hamdard University), New Delhi 110062, India, sahmad_jh@yahoo.co.in)

      J. Ethnopharmacol. 197, 157-164 (2017). HPTLC of picroside I (1) and picroside II (2) in Picrorhiza kurroa on silica gel with ethyl acetate – methanol – acetic acid 46:1:1. Quantitative determination by absorbance measurement at 270 nm. The hRF values for (1) and (2) were 52 and 68, respectively.

      Classification: 15a
      120 024
      Effect-directed fingerprints of 77 botanical extracts via a generic high-performance thin-layer chromatography method combined with assays and mass spectrometry
      S. KRÜGER, L. HÜSKEN, R. FORNASARI, I. SCAINELLI, Gertrud E. MORLOCK* (*Justus Liebig Univ. Giessen, Inst. of Nutrit. Sci., Chair of Food Sci., Heinrich-Buff-Ring 26-32, 35392 Giessen, Germany, gertrud.morlock@uni-giessen.de)

      J. Chromatogr. A 1529, 93-106 (2017). Presentation of the quantitative effect-directed profiles of 77 industrially and freshly extracted botanicals like herbs, spices, vegetables and fruits, widely used as food ingredients, dietary supplements or traditional medicine for their quality assessment with regard to potential health-promoting activities. Fast assignment of single active compounds and evaluation of their contribution to the overall activity, originating from a food or botanical sample by combination of HPTLC hyphenated with UV/Vis/FLD detection and effect-directed analysis, using the 2,2-diphenyl-1-picrylhydrazyl radical, Gram-negative Aliivibrio fischeri, Gram-positive Bacillus subtilis, acetylcholinesterase and tyrosinase assays. Characterization of bioactive compounds of interest eluted using an elution head-based interface by HPTLC-UV/Vis/FLD-EDA-ESI-(HR)MS method. Demonstration of the excellent quantification power of the method by applying for rosmarinic acid, contents ranged from 4.5 mg/g (rooibos) to 32.6 mg/g (rosemary), for kaempferol-3-glucoside from 0.6 mg/g (caraway) to 4.4 mg/g (wine leaves), and for quercetin-3-glucoside from 1.1 mg/g (hawthorn leaves) to 17.7 mg/g (thyme). The mean repeatabilities (%RSD, n=18) were ≤ 2.2 % for the three compounds and the mean intermediate precision (%RSD, n=3) was 5.2 % over three different days.

      Classification: 4e
      120 069
      Biological evaluation, overpressured layer chromatography separation, and isolation of a new acetylenic derivative
      compound from Prangos platychlaena ssp
      N. TABANCA*, D. WEDGE, X. LI, Z. GAO, T. OZEK, U. BERNIER, N. EPSKY, K. BASER, G. OZEK (*USDA-ARS, Subtropical Horticulture Research Station, Miami, FL 33158, USA, Nurhayat.Tabanca@ars.usda.gov)

      platychlaena fruit essential oils. J. Planar Chromatogr. 31, 61-71 (2018). Overpressured layer chromatography (OPLC) of two Prangos platychlaena ssp. platychlaena fruit essential oils on silica gel with toluene – isooctane 4:1, external pressure 50 bar, flow rate 100 mL/min. Bioautography by spraying with a spore suspension (105 spores/mL) of Colletotrichum species without chemical derivatization, followed by incubation for 4 days at 26 °C with a 12 h photoperiod. Detection by spraying with vanillin–sulfuric acid reagent (0.1 g vanillin in 100 mL ethanol and 2 mL sulfuric acid), followed by heating at 110 °C for 3 min.

      Classification: 15b
      121 030
      Four new xanthones from Cratoxylum cochinchinense and their in vitro antiproliferative effects
      C. ITO, T. MATSUI*, A. NIIMI, H.T.-W. TAN, M. ITOIGAWA (*Faculty of Pharmacy, Meijo University, Tempaku-ku, Nagoya, Japan; tmatsui@aichi-med-u.ac.jp)

      Planta Med. 83(09), 812-818 (2017). Some of the column subfractions obtained (with different mixtures of hexane – acetone – isopropanol) from an ethyl acetate extract of Cratoxylum cochinchinense twigs and boughs were submitted to a preparative TLC on silica gel for the isolation of the following xanthones and anthracenones: (1) β-mangostin, cochinchinone and cratoxanthone D with chloroform – acetone 10:1, (2) allanxanthone by three-stage elution with benzene – acetone 10:1, n-hexane – ethyl acetate 3:1, and n-hexane – acetone 3:1, (3) cratoxanthone A by similar three-stage elution (third step: chloroform – acetone 10:1), (4) visminone F by two-step elution with benzene – acetone 10:1, and isopropanol – acetone 5:1, (5) cratoxanthone B and garcinone E by a two-step elution with isopropanol – acetone 4:1, and n-hexane – acetone 3:1, (6) α-mangostin and mangostenol by a two-step elution with chloroform – acetone 20:1, and n-hexane – isopropanol – acetone 5:5:1, (7) cratoxanthone C by a two-step elution with benzene – ethyl acetate 5:1, and chloroform – acetone 20:1.

      Keywords: herbal
      Classification: 7, 8b, 15a
      121 059
      Triterpenoids with antiplatelet aggregation activity from the roots of Ilex pubescens
      Q. TAN, M. QIU, D. CAO, T. XIONG, L. ZHANG, L. ZHOU, L. RONG, J. ZHOU, J. JIN*, Z. ZHAO (*School of Pharmaceutical Sciences, Sun Yat-Sen University, Guangzhou, Guangdong Province, China; jinjing@mail.sysu.edu.cn)

      Planta Med. 83(09), 797-804 (2017). For the analysis of their sugar moieties, five new triterpene saponins (ilexpusons B, D, E, F, G), isolated from a methanolic extract of Ilex pubescens roots, were hydrolyzed at 90 °C in water containing HCl and dioxane. TLC of the dried aqueous phases on silica gel with chloroform – methanol – water 8:5:1. Detection by spraying with aniline – diphenylamine reagent (2 mL aniline, 2 g diphenylamine, 10 mL phosphoric acid 85%, in 100 mL acetone) and heating for 2-5 min at 85 °C. By comparison with standards, the sugar moiety was identified (before confirmation by GC) as glucose (hRF 49) in ilexpuson B, as xylose (hRF 81) in ilexpusons D and E, and as glucuronic acid (hRF 44) in ilexpusons F and G.

      Classification: 14, 32e
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