Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

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      124 060
      Development and validation of a high-performance thin layer chromatographic (HPTLC) method for simultaneous quantification of reserpine, atropine, and piperine in Sarpagandha Ghanvati, a classical Ayurvedic preparation
      K. PUNDARIKAKSHUDU, A. SHARMA, C. BHATT, N. KANAKI (*L.J. Institute of Pharmacy, L.J. Campus, between Kataria Motors and Sarkhej-Sanand Circle, S.G. Rd, Ahmedabad, India, p_kilambi@yahoo.com)

      J. AOAC Int. 102, 1021-1026 (2019). HPTLC of reserpine (1), atropine (2) and piperine (3) in Sarpagandha Ghanvati on silica gel with toluene - ethyl acetate - diethyl amine 7:2:1. Quantitative determination by absorbance measurement at 269 nm for (1), 220 nm for (2) and 254 nm for (3), respectively. The hRF values for (1) to (3) were 57, 30 and 92, respectively. Linearity was between 200 and 600 ng/zone for (1), 1000 and 5000 ng/zone for (2) and 100 and 500 ng/zone for (3), respectively. Intermediate precision was below 1 % (n=3). The LOD and LOQ were 60 and 200 ng/zone for (1), 600 and 800 ng/zone for (2) and 20 and 10 ng/zone for (3), respectively. Recovery rate was 98.9 % for (1), 99.5 % for (2) and 99.1 % for (3). The recovery from the formulation was 90.3 %, 92.4 % and 90.0 % of the expected values of (1) to (3), respectively.

      Classification: 22
      124 024
      Development of a reversed-phase high-performance thin-layer chromatography method for the simultaneous determination of trigonelline and diosgenin biomarkers in Trigonella foenum-graecum L. seeds grown in variable environment
      A. FOUDAH, P. ALAM, M. ALQARNI, M. SALKINI, M. KADER* (*Department of Pharmacognosy, College of Pharmacy, Prince Sattam Bin Abdulaziz University, P.O. Box 173, Al-Kharj 11942, Saudi Arabia, mpharm101@hotmail.com)

      J. Planar Chromatogr. 32, 379-384 (2019). HPTLC of trigonelline (1) and diosgenin (2) in the seeds of Trigonella foenum-graecum L. on silica gel with acetonitrile - water 3:1. Quantitative determination by absorbance measurement at 267 nm for (1) and at 430 nm after derivatization with vanillin - sulfuric acid for (2). The hRF values for (1) and (2) were 29 and 17, respectively. Linearity was between 200 and 1400 ng/zone for (1) and 50 and 300 ng/zone for (2). Intermediate precision was below 2 % (n=6). The LOD and LOQ were 7 and 1 ng/mL for (1) and 7 and 19 ng/mL for (2), respectively. Recovery rate was between 97.8 and 99.1 % for (1) and 98.2 and 99.3 % for (2), respectively.

      Classification: 14, 22
      123 010
      Diterpene lipo-alkaloids with selective activities on cardiac K+ channels
      T. KISS, B. BORCSA, P. ORVOS, L. TÁLOSI, J. HOHMANN, D. CSUPOR* (*Department of Pharmacognosy, Faculty of Pharmacy, University of Szeged, Szeged, Hungary; csupor.dezso@pharmacognosy.hu)

      Planta Med. 83(17), 1321-1328 (2017). Benzoyl-aconine esters (lipo-alkaloids) produced by transesterification of aconitine (isolated from Aconitum sp.) with long-chain fatty acids were purified by a multistep chromatographic method, including cyclodextrane gel filtration chromatography, centrifugal planar chromatography on aluminium oxide layer using cyclohexane – chloroform – methanol 70:30:1 followed by 70:30:3 and/or preparative thin-layer chromatography on aluminium oxide layer with toluene – acetone – ethanol – concentrated ammonia 70:40:10:3.

      Classification: 4d, 4e, 11a, 22, 32e
      123 012
      Microscopic and phytochemical comparison of the three Leonurus species L. cardiaca, L. japonicus, and L. sibiricus
      Anna PITSCHMANN, C. WASCHULIN, C. SYKORA, S. PUREVSUREN, S. GLASL* (*Department of Pharmacognosy, University of Vienna, Vienna, Austria; sabine.glasl@univie.ac.at)

      Planta Med. 83(14/15), 1233-1241 (2017). HPTLC of standards and methanolic extracts of L. cardiaca, L. japonicus and L. sibiricus (Lamiaceae) acidified with formic acid on silica gel with ethyl acetate – acetic acid – formic acid – water 100:11:11:26, in an automatic development chamber with 48 % humidity (20 min presaturation). Detection under white and UV light, before and after immersion in 1) anisaldehyde – sulphuric acid (followed by heating) for the detection of iridoids; 2) natural product reagent A for phenylpropanoids; 3) modified Dragendorff reagent (bismuth oxynitrate 0.17 %, sulfuric acid 3.5 %, glacial acetic acid 2 %, potassium iodide 4 %) for alkaloids. Ajugoside (hRF 29) and verbascoside (hRF 53) were found in L. cardiaca and L. sibiricus, but absent in L. japonicus. The opposite was true for leonurine (hRF 52), whereas stachydrine (hRF 14) was found in the three species. This method allows to distinguish L. japonicus from the other species, which have to be distinguished from each other through morphology.

      Classification: 8, 22, 32e
      123 014
      A harmonized HPTLC method for identification of various caffeine containing herbal drugs, extracts, and products, and quantitative estimation of their caffeine content
      Tien DO*, I. SANTI, E. REICH (*CAMAG Laboratory, Sonnenmattstrasse 41, 4132 Muttenz, Switzerland, tien.do@camag.com)

      J. Liq. Chromatogr. Relat. Technol. 42, 274-281 (2019). HPTLC of caffeine in caffeine-containing botanicals and caffeinated products on silica gel with toluene - acetone - formic acid 9:9:2. Detection by dipping into NP reagent (1 g of diphenylborinic acid aminoethylester in 200 mL of ethyl acetate), followed by derivatization with anisaldehyde reagent, then heating at 100 ºC for 3 min. Quantitative determination by absorbance measurement at 273 nm. The hRF value of caffeine was 70. Linearity was between 30 and 120 ng/zone. The intra-day and inter-day precision was below 5 % (n=3). The LOD and LOQ were 10 and 30 ng/zone, respectively. Recovery rate was between 101 and 118 %.

      Classification: 22
      123 039
      Development and validation of a High-Performance Thin-Layer Chromatography based method for the quantification of Trigonelline in fenugreek (Trigonella foenum-graecum) seeds
      O. LAILA, I. MURTAZA*, M. ABDIN, S. AHMAD, M. KHAN (*Biochemistry and Molecular Biotechnology Laboratory, Division of Basic Sciences and Humanities, SKUAST-K-190025, India, imz_murtaza@hotmail.com)

      J. Planar Chromatogr. 32, 95-102 (2019). HPTLC of trigonelline in the seeds of Fenugreek
      (Trigonella foenum-graecum) on silica gel with n-propanol - methanol - water - ammonia 40:6:15:1. Quantitative determination by absorbance measurement at 270 nm. The hRF value of trigonelline was 40. Linearity was between 100 and 1200 ng/zone. The intermediate precision was 0.7 % (n=6). The LOD and LOQ were 14 and 52 ng/zone, respectively. Recovery rate was 100.1 %.

      Classification: 22
      123 057
      A comparative estimation of the morphine content of the Ayurvedic formulation ‘Kamini Vidrawan Ras’ using validated High-Performance Thin-Layer Chromatography and High-Performance Liquid Chromatography techniques
      A. SHARMA, C. DHAL, R. SRIVASTAVA* (*Department of Applied Chemistry, Delhi Technological University, Delhi 110042, India, richa_srivastava@dce.ac.in)

      J. Planar Chromatogr. 32, 47-50 (2019). HPTLC of morphine hydrochloride in the Ayurvedic formulation "Kamini Vidrawan Ras" on silica gel with ethyl acetate - methanol - ammonia solution 17:2:1. Quantitative determination by absorbance measurement at 280 nm. The hRF value of morphine was 36. Linearity was between 0.4 and 1.2 µg/mL. The intermediate precision was below 1 % (n=6). The LOD and LOQ for morphine were 0.5 and 1.5 µg/mL, respectively. Recovery rate was 100.0 %. Results were comparable to a validated HPLC method.

      Classification: 22
      100 046
      HPTLC quantitation of camptothecin in Nothapodytes foetida (Wight) Sleumer stem powder
      V. DIGHE, R.T. SANE, G. PAREKH*, V. GOKARN, O. DHOTRE (*Department of Chemistry, Ramnarain Ruia College, Matunga (East), Mumbai-400 019, India; gaurangparekh80@yahoo.co.in)

      J. Planar Chromatogr. 20, 131-133 (2007). HPTLC of camptothecin (4-ethyl-4-hydroxy-1H-pyrano[3’,4’:6,7]indolizino[1,2b]quinoline-3,14(4H,12H)dione) on silica gel with toluene - acetonitrile - glacial acetic acid 65:35:1. Detection and quantitation were performed by densitometric scanning in fluorescence mode at 370 nm.

      Classification: 22