Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      124 001
      Cytotoxic flavones from the stem bark of Bougainvillea spectabilis Willd.
      L.T.M. DO, T. AREE, P. SIRIPONG, N.T. VO, T.T.A. NGUYEN, P.K.P. NGUYEN, S. TIP-PYANG* (*Department of Chemistry, Faculty of Science, Chulalongkorn University, Bangkok, Thailand;

      Planta Medica 84(2), 129-134 (2018). TLC of subfractions obtained from normal-phase LC and size-exclusion chromatography of an ethanolic extract of Bougainvillea spectabilis (Nyctaginaceae) stem-bark on RP-18 with methanol – water 2:3 and 1:1 to isolate six flavones (bougainvinones J, K, L, M, and two dimethylflavone derivatives).

      Classification: 8a, 32e
      124 045
      Bioactivity-guided investigation of the anti-inflammatory activity of Hippophae rhamnoides fruits
      D. RÉDEI, N. KÚSZ, N. JEDLINSZKI, G. BLAZSÓ, I. ZUPKÓ, Judit HOHMANN* (*Department of Pharmacognosy, University of Szeged, Szeged, Hungary;

      Planta Medica 84(1), 26-33 (2018). For the monitoring of the multi-step fractionation through VLC (vacuum liquid chromatography) of the chloroform-soluble parts of a methanol – water 7:3 percolate of Hippophae rhamnoides (Eleagnaceae) fruit peels, TLC on silica gel and RP-18, detection by spraying with sulfuric acid and heating. Preparative TLC on silica gel with cyclohexane – dichloromethane – methanol 5:15:1 to isolate, from VLC subfractions, three lignans (nectandrin B, fragransin A2, saucernetindiol) that are diastereoisomers of each other.

      Classification: 7, 8b, 32e
      124 015
      Denudatin A, a dimeric acylphloroglucinol from Hypericum denudatum presents an antinociceptive effect in mice
      H. BRIDI, G. de CARVALHO MEIRELLES, S. A. de LORETO BORDIGNON, St. M. KUZE RATES, Gilsane LINO von POSER* (*Laboratory of Pharmacognosy, Faculty of Pharmacy, Federal University of Rio Grande do Sul, Porto Alegre, Brazil;

      Planta Medica 83(17), 1329-1334 (2017). Two acetone-soluble subfractions of an n-hexane maceration of Hypericum denudatum aerial parts (Hypericaceae) were submitted to repeated centrifugal planar chromatography (CPC) on silica gel using n-hexane – ethyl acetate (gradient from 100:0 to 90:10), obtaining four dimeric acylphloroglucinols (denudatin A, hyperbrasilol A, uliginosin B and isouliginosin B), which were purified by crystallisation with n-hexane – dichloromethane 9:1. From the most apolar CPC eluates, a monomer (selancin A) was isolated on preparative TLC silica gel layer by elution with n-hexane – ethyl acetate 97:3. Furthermore, all the purification steps were monitored through TLC on silica gel with n-hexane – ethyl acetate 19:1 or with n-hexane – dichloromethane 1:1. Detection under UV light after derivatization with anisaldehyde – sulfuric acid, monomeric acylphloroglucinols appeared purple, whereas dimers appeared yellow-orange.




      Classification: 7, 32e
      124 051
      A reliable, simple and cost-efficient TLC-HPLC method for simultaneously determining florfenicol and florfenicol amine in porcine urine: application to residue surveillance
      M. QIAN, D. ZHOU, Q. WANG, J. GAO, D. LI, Y. LI, B. YANG* (*Hubei Engineering Research Center of Viral Vector, Wuhan University of Bioengineering, NO. 1 Hanshi Road, Xinzhou District, Wuhan City, Hubei Province 430415, P. R. China,

      Food Addit. Contam. Part A. 36, 1218-1227 (2019). Preparative TLC of florfenicol and florfenicol amine in porcine urine on silica gel with dichloromethane - acetone - ammonium hydroxide 20:20:1. Qualitative identification under UV light at 254 nm. Zones were scraped off and extracted for HPLC analysis.

      Classification: 28a
      124 056
      Bioprofiling of Salvia miltiorrhiza via planar chromatography linked to (bio)assays, high resolution mass spectrometry and nuclear magnetic resonance spectroscopy
      E. AZADNIYA, Gertrud E. MORLOCK* (*Chair of Food Science, Institute of Nutritional Science, Interdisciplinary Research Center (IFZ), Justus Liebig University Giessen, Heinrich-Buff-Ring 26-32, 35392, Giessen, Germany,

      J. of Chromatogr. A 1533, 180-192 (2018). HPTLC-UV/Vis/FLD-(bio)assay-HRMS of polar (phenolics) and nonpolar (tanshinones) extracts of Salvia miltiorrhiza Bunge root (Danshen), followed by streamlined scale-up to preparative layer chromatography with 1H-NMR. For phenolics, HPTLC on silica gel first with toluene - chloroform - ethyl acetate - methanol - formic acid 4:6:8:1:1 and second development with petroleum ether - cyclohexane - ethyl acetate 25:14:11. Confirmation of the acetylcholinesterase inhibitors salvianolic acid B (1), lithiospermic acid (2), rosmarinic acid (3), cryptotanshinone (4) and 15,16-dihydrotanshinone I (5). In the polar extracts, compounds (1), (2) and (3) exhibited free radical scavenging activity in the 2,2-diphenyl-1-picrylhydrazyl assay (DPPH* radical reagent), (4) and (5) were active against Bacillus subtilis and Aliivibrio fischeri (LOD of 12 ng/zone for (4), and 5 ng/zone for (5). For the first time, the unidentified, most active zone of the nonpolar Danshen extract was identified as a co-eluting zone of 1,2-dihydrotanshinone and methylenetanshinquinone 2:1.

      Classification: 32e
      124 008
      Diarylheptanoid, a constituent isolated from methanol extract of Alpinia oficinarum attenuates TNF-α level in Freund's complete adjuvant-induced arthritis in rats
      V. HONMORE, A. KANDHARE, P. KADAM, V. KHEDKAR, A. NATU, S. ROJATKAR, S. BODHANKAR* (*Department of Pharmacology, Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune, Maharashtra, India,

      J. Ethnopharmacol. 229, 233-245 (2019). HPTLC of diarylheptanoid in the rhizomes of Alpinia officinarum on silica gel with chloroform - methanol - formic acid 85:20:2. Detection under UV light at 254 nm. The hRF value for diarylheptanoid was 90.

      Classification: 7
      123 010
      Diterpene lipo-alkaloids with selective activities on cardiac K+ channels
      T. KISS, B. BORCSA, P. ORVOS, L. TÁLOSI, J. HOHMANN, D. CSUPOR* (*Department of Pharmacognosy, Faculty of Pharmacy, University of Szeged, Szeged, Hungary;

      Planta Med. 83(17), 1321-1328 (2017). Benzoyl-aconine esters (lipo-alkaloids) produced by transesterification of aconitine (isolated from Aconitum sp.) with long-chain fatty acids were purified by a multistep chromatographic method, including cyclodextrane gel filtration chromatography, centrifugal planar chromatography on aluminium oxide layer using cyclohexane – chloroform – methanol 70:30:1 followed by 70:30:3 and/or preparative thin-layer chromatography on aluminium oxide layer with toluene – acetone – ethanol – concentrated ammonia 70:40:10:3.

      Classification: 4d, 4e, 11a, 22, 32e
      123 011
      Terpenoids from leaves of Guarea macrophylla display in vitro cytotoxic activity and induce apoptosis in melanoma cells
      Geanne Alexandra A. CONSERVA, N. GIROLA, C.R. FIGUEIREDO, R.A. AZEVEDO, S. MOUSDELL, P. SARTORELLI, M.G. SOARES, G.M. ANTAR, J.H.G. LAGO* (*Centre of Natural and Human Sciences, Federal University of the ABC, Santo-André, State of São Paulo, Brazil;

      Planta Med. 83(16), 1289-1296 (2017). A cycloartene-diol, a dihydroxycicloartenone and an isopimaradiene-diol were isolated from subfractions of an ethanolic extract of Guarea macrophylla (Meliaceae) leaves through elution on preparative TLC silica gel layers with chloroform – acetone 19:1, or with n-hexane – ethyl acetate 9:1 or 1:1, respectively.

      Classification: 15a, 32e