Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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J. Planar Chromatogr. 20, 267-274 (2007). Comparison of retention factors in pure water, log kw, determined by linear extrapolation and by a numerical method based on Oscik’s equation, and calculated values of log P as hydrophobicity indices for nine homologues s-triazines. The effect of mobile phase pH on solute retention was investigated as well as the effect of mobile and stationary phase properties on chromatographic behavior; 3 different organic modifiers (dioxane, acetonitrile, and tetrahydrofuran) and two stationary phases (RP-8 and RP-18) were used. Correlations of calculated log P values and log kw with carbon number confirm the usefulness of chromatographic techniques for studying the hydrophobicity of organic compounds. TLC on RP-18 with buffer - methanol mixtures in saturated sandwich chambers. Detection under UV light at 254 nm.
J. Chromatogr. A 1458, 136–144, (2016). The soil-water partition coefficient normalized to the organic carbon content (KOC) influences the fate of organic compounds in the environment. This paper proposes a RP-TLC method for KOC determination as a simpler, yet equally accurate method as the official HPLC method. TLC on different systems, including RP-18 and cyano phases developed with methanol – water and acetonitrile – water mixtures. 50 different compounds such as phenols, benzodiazepines, triazine herbicides, and polyaromatic hydrocarbons were selected. A calibration set of 29 compounds with known logKOC values was used to build simple univariate calibrations, Principal Component Regression (PCR) and Partial Least Squares (PLS) models between logKOC and TLC retention parameters. The models exhibit good statistical performance and indicate that the cyano phase contributes better to logKOC modeling than the RP-18 phase. Comparison of the proposed TLC methods, the official HPLC method, and four in silico estimation approaches by using the non-parametric Sum of Ranking Differences(SRD) approach. The best estimations of logKOC values were achieved by simple univariate calibration of TLC retention data from cyano phase developed with 40–50 % methanol. In a Linear Solvation Energy Relationship study it was found that the more polar cyano phase in combination with methanol – water mixtures is the key to better modeling of logKOC through significant diminishing of dipolar and proton accepting influence of the mobile phase as well as enhancing molar refractivity in excess of the chromatographic systems.
Phytochemistry 28, 87-981 (1989). TLC of pisatin and maackiain on silica with chloroform - methanol 4:1. Detection with vanillin - HCl reagent. Determination of RM: TLC on RP-18 254 plates activated by heating at 120°C for 15 min. with acetonitrile - water 13:7. Visualization under UV and by exposing to iodine vapor.
J. Chromatogr. 543, 195-2000 (1991). Measurement of the RM values of arylsulfonylalkanoic and arylsulfonylcycloalkane carboxylic acids by TLC on polyamide. Analysis of the RM vs. Rekker hydrophobicity relation. Excellent correlations, esp. within strictly congeneric sub-series, were established.
Acta Chromatographica 1, 81-90 (1992). Introduction of a new thermodynamic definition of the Rf coefficient and furnish of empirical evidence to support it. Concept is the mental division of the multicomponent mobile phases into the individual liquid moieties. Practical example: Solute : methyl undecyl ketone; stationary phases : RP-2, RP-8, RP-18; mobile phases : methanol : water, binary mixtures in varying proportions.
A linear free energy relationship analysis. J. Chromatogr. A 749, 201-209 (1996). Presentation of a linear free energy relationship to analyze the RMw values determined on RP-18 silica with aqueous methanol mobile phases and give a equation, involving the solute descriptors such as excess molar refraction, dipolarity/polarizability overall or effective hydrogen-bond acidity and basicity, and McGowan characteristic volume etc. Comparison of the coefficients in the equation with those for the correlation of water - octanol partition coefficients. Discussion of the limitation of the equation in its application.
J. Planar Chromatogr. 12, 446-451 (1999). Determination of the lipophilicity and the specific hydrophobic surface area of seven monotetrazolium and nine ditetrazolium salts by RP TLC with ethanol, THF and dioxane as organic modifiers. The nature of the organic modifier significantly influenced the specific hydrophobic surface area. TLC of tetrazolium salts on alumina, also on alumina impregnated by overnight predevelopment in n-hexane - paraffin oil 19:1. After drying visualization under UV and under visible light.
Proc. Intern. Symp. on Planar Separations Plan. Chrom. 13-23 (2003). TLC of newly synthesized benzanilides, benzamide and a group of pesticides on RP-18 with aqueous solutions of acetonitrile or methanol with different organic modifier concentrations. Visualization under UV 254 or 366 nm.