Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
- Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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- Search by CBS edition: Select a CBS edition and find all related publications
Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. The saved items can be printed to PDF using the print function of your web browser.
J. AOAC Int. 102, 708-713 (2019). TLC of snake bile in 20 species from three families (Elapidae, Colubridae, and Viperidae) on silica gel with xylene – isopropanol – methanol – glacial acetic acid – water 80:40:30:20:3. Detection by spraying with a 10% sulfuric acid ethanol solution, followed by heating at 105 ºC. Qualitative identification under UV light at 366 nm. TLC coupled with quadrupole–time-of-ﬂight–MS analysis of each zone was used for compound identification and evaluation.
J. Liq. Chromatogr. Relat. Technol. 31, 1373-1385 (2008). TLC of cholic acid, glycocholic acid, glycolithocholic acid, deoxycholic acid, chenodeoxycholic acid, glycodeoxycholic acid, and lithocholic acid on silica gel with concentration zone, prewashed with methanol and dried for 24 h at room temperature, in a saturated chamber. Best separation of the bile acids was achieved with n-hexane - ethyl acetate - methanol - acetic acid 20:20:5:2. Detection by dipping for 15 s in sulfuric acid - methanol 1:19, followed by heating at 90 °C for 20 min provided better results than derivatization by spraying with 10 % phosphomolybdic acid in ethanol. Quantitative determination by absorbance measurement between 190 and 800 nm.
J. Planar Chromatogr. 2, 355-361 (1989). Description of the use of SIMS in the direct analysis of samples separated by TLC (bile acids and diuretics). Discussion of the correct selection of extraction/sputtering solvent, the influences of extraction solvent volume and primary ion beam parameters.
J. Planar Chromatogr. 19, 52-57 (2006). TLC and HPTLC of cholesterol, cholic and lithocholic acid, and taurodeoxycholic acid sodium salt on silica gel with methanol - dichloromethane 1:4, and on RP18 with methanol - water 4:1 with chamber saturation. Detection by spraying with phosphomolybdic acid solution and placing the plates in a gravity convection oven. The plates were heated to different temperatures from 40 to 120 °C for different periods of time (from 2 to 40 min). Best conditions for sensitive and robust detection on silica gel and RP18 were low derivatization temperatures around 60 °C and long heating times of more than 15 min.
J. Sep. Sci. 33, 3110-3118 (2010). HPTLC of bile acids and their derivatives on 1) RP-18, 2) RP-18W and 3) cyano phase with methanol - water mixtures. The volume fraction of organic solvent in the mobile phase ranged from 70-90 % for (1), 50-70 % for (2) and 45-65 % for (3). Detection by spraying with a solution of manganese chloride in sulfuric acid, followed by heating at 100-120 °C for 10 min. Quantification by absorbance measurement at 254 nm and 365 nm.
J. Shenyang Pharm. Coll. (Shenyang Yaoxueyuan Xuebao) 6, 197-198 (1989). TLC of bile components on silica with isopentanol - acetic acid - water 18:5:3. Identification by comparing the Rf values with those of standards.
III. Separation on various stationary phases. J. Liq. Chrom. & Rel. Technol. 27, 2613-2623 (2004). TLC of cholic, glycocholic, glycolithocholic, deoxycholic, chenodeoxycholic, glycodeoxycholic, and lithocholic acid on different preparations of silica gel and a mixture of silica gel and Kieselguhr with n-hexane - ethyl acetate - acetic acid in various volume compositions; successful separation was achieved with the compositions 4:4:1 and 22:21:5. Detection by 10 % aqueous sulfuric acid followed by heating at 120 °C for 20 min. Densitometric measurement at 250 nm.
J. Planar Chromatogr. 28, 380-385 (2015). HPTLC of taurocholic acid (1), glycodeoxycholic acid (2) and taurodeoxycholic acid (3) in ten Thai edible plants on silica gel with chloroform - methanol - acetic acid 7:2:1. Quantitative determination by absorbance measurement at 366 nm. Linearity was in the range of 34-2200 ng/zone for (1), 33-2100 ng/zone for (2) and 30-1900 ng/zone for (3). LOD and LOQ were 10 and 50 ng/zone for (1), 20 and 40 ng/zone for (2) and 10 and 50 ng/zone for (3). The intermediate precision was below 1.2 % (n=6). Average recovery for (1) to (3) was 99, 100 and 100 %, respectively.