Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      126 011
      Quality risk assessment and DoE-based analytical quality by design approach to stability-indicating assay method for acidic degradation kinetic study of apremilast
      P. PRAJAPATI*, H. PATEL, S. SHAH (*Maliba Pharmacy College, Maliba Campus, Uka Tarsadia University, Bardoli, Gujarat 394350, India,

      J. Planar Chromatogr. 33, 231-244 (2020). HPTLC of apremilast on silica gel with toluene - methanol - ethyl acetate 7:2:1. Quantitative determination by absorbance measurement at 241 nm. The hRF value for apremilast was 63. Linearity was between 200 and 1000 ng/zone. Inter-day and intra-day precision were below 1 % (n=3). The LOD and LOQ were 4 and 13 ng, respectively. Recovery rate was between 99.7 and 100.0 %. Apremilast was subjected to acidic, alkaline, oxidative, dry heat, neutral, and photolytic degradation conditions. The method was implemented using a quality risk management and quality by design approach for regulatory requirements.

      Classification: 23e
      100 049
      Comparative study of the retention of s-triazines on octadecylsilica, cyano, and amino HPTLC plates by use of a QSPR model
      Tatjana DJAKOVIC-SEKULIC*, N. PERISIC-JANJIC (*Department of Chemistry, Faculty of Sciences, University of Novi Sad, Trg D. Obradovica 3, 21000 Novi Sad, Serbia;

      J. Planar Chromatogr. 20, 365-371(2007). Estimation of retention data by use of correlation equations and physicochemical properties is a useful tool in liquid chromatography. HPTLC of an homologous series of 9 s-triazines on RP-18, cyano-, and amino phase in unsaturated chambers with aqueous solutions of the organic solvents acetonitrile, tetrahydrofuran, and dioxane. After development the dried plates were examined under UV light at 254 nm.

      Classification: 23e
      107 080
      Stability-indicating HPTLC determination of brimonidine tartrate in bulk drug and pharmaceutical dosage form
      H. BODALWALA*, P. JAIN, R. KHATAL, K. AGRAWAK (*R. C. Patel Institute of Pharmaceutical Education and Research, Karwand Naka, Shirpur, Dist. Dhule 425405 (MS), India)

      62nd Indian Pharmaceutical Congress Abstract No. F-301 (2010). TLC of brimonidine tartrate on silica gel with methanol – toluene – triethylamine 10:35:2. The hRf value was 48. Quantitative determination by absorbance measurement at 247 nm. The method was linear in the range of 100-600 ng/band. The sample was subjected to different stress conditions (acid, base, oxidative, thermal and photolytic). With the proposed method all the degradation products were well resolved from the drug.

      Classification: 23e
      107 097
      TLC densitometric fingerprint development and validation of berberine as markers in poly-herbal Unani formulations
      S. SHUKLA*, Swarnlata SARAF, S. SARAF (*University Institute of Pharmacy, Pt. Ravishankar Shukla University, Raipur, Chhattisgarh, India)

      Der Pharma Chemica 2(3), 8-18 (2010). HPTLC of berberine on silica gel with methanol – acetic acid – water 8:1:1. The band corresponding to berberine showed an hRf value of 74. Quantitative determination by absorbance measurement at 350 nm. The method was linear in the range of 100-500 ng/band. Different samples analysed by the proposed method were found to contain 11.8-12.5 mg/g berberine. The recovery was between 98.0-100.3 %.

      Classification: 23e
      116 061
      Influence of the anionic part of 1-alkyl-3-methylimidazolium-
      based ionic liquids on the chromatographic behavior of piperazine in RP-HPTLC
      D. MIESZKOWSKI, W. SROKA, M. MARSZALL* (*Department of Medicinal Chemistry, Collegium Medicum in Bydgoszcz, Jurasza 2, 85-094 Bydgoszcz, Poland,

      J. Liq. Chromatogr. Relat. Technol. 38, 1499-1506 (2015). RP-HPTLC of piperazine in pharmaceutical formulations on RP-18 with acetonitrile - water 3:2 modified with 1.5 % tetrafluoroborate. Quantitative determination by absorbance measurement at 247 nm. The hRF value for piperazine was 43. Linearity was in the range of 0.8-2.2 μg/zone. LOD and LOQ were 0.11 and 0.34 μg/zone. The intermediate precision was below 3.5 % (n=3). Recovery was between 99 and 103 %. Significant changes and improvements regarding the hRF value were observed when tetrafluoroborate was added to the mobile phase.

      Classification: 23e
      62 166
      Synthesis and anticandidal properties of polyoxin L analogues containing a-amino fatty acids
      R.K. KHARE*, J.M. BECKER, F.R. NAIDER, (*Dep. of Chemistry, Coll. of Staten Island, City Univ. of New York, Staten Island, New York 10301)

      J.of Medicinal Chemistry 31, 650-656 (1988). TLC of polyoxins on silica with 1-butanol - acetic acid - water 4:1:2. Detection under UV or by spraying with ninhydrin in butanol.

      Classification: 23e
      67 124
      Identification, qualitative and quantitative analysis of uric acid, creatine and creatinine together with carbohydrates in biological material
      R. KLAUS, (Fichtestrasse 25, D-6100 Darmstadt, FRG)

      Proc. 6th Int. Symp. Instrum. Planar Chromatogr., (Interlaken 1991), Inst. Chromatogr., Bad Dürkheim, FRG, 157-173 (1991). Determination of title substances on HPTLC-NH2 plates. Qualitative analysis in human urine and serum, 2-fold development with 1-propanol - nitromethane - water - glacial acetic acid 30:30:10:1. Detection under UV or by heating at 150°C. Quantitative analysis of uric acid, creatine, creatinine and glucose in human urine; two-fold development with 1) acetonitrile - water 70:30, 2) ethyl acetate - pyridine - water - acetic acid - propionic acid 50:50:10:5:5. Quantitative analysis of glucose, creatinine and uric acid in serum; two-fold development in 1) acetonitrile - water 80:20, 2) ethyl acetate - pyridine - water - glacial acetic acid - propionic acid 50:50:10:5:5. Quantitative determination by fluorescence 366/>400 nm.

      Classification: 18, 23e
      75 105
      A study of the retention of azines and diazines in RPTLC with bonded alkyl stationary phases
      I. BARANOWSKA, S. SWIERCZEK, (Dept. of Anal. and Gen. Chem., Silesian Techn. Univ., 9 Kuczewskiego Street, 44-101 Gliwice, Poland)

      J. Planar Chromatogr. 7, 399-405 (1994). Investigation of retention of azines and diazines in RP-TLC with RP-2, RP-8 and RP-18 material and methanol - water eluents; the practical usefulness of the retention model employed was established for pyrazine, quinoxaline, pyridine, quinoline, c-picoline, 2-methylquinoxaline, for their dehydrocondensation products, and for their sulfur derivatives. Visualization with Dragendorff's reagent, followed by additional spraying with sulfuric acid.

      Classification: 23e