Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      62 167
      2-Trichloromethylbenzimidazole, a new selective chromogenic reagent for the detection of some azines on thin-layer plates
      L. KONOPSKI*, B. JERZAK, (Inst. Indus. Org. Chem., Annopol 6, 03-236 Warsaw, Poland)

      J. Chromatogr. 363, 394-396 (1986). TLC of azines on silica with acetone, or ethyl acetate - methanol - water 5:3:1. Detection by spraying with 1 % 2-tri chloromethylbenzimidazole in acetone with or without heating at 105 °C for 1 min. Detection limits, 10-100 ng.

      Classification: 23e
      67 138
      Determination of the enantiomeric composition of 2-methoxy-3-(1'-methylpropyl)pyrazine from Galbanum oil using achiral and chiral lanthanide shift reagents
      S. MIHARA, H. MASUDA, O. NISHIMURA, H. TATEBA, (Ogawa & Co., Ltd., 6-329 Akabanemishi, Kita-ku, Tokyo 115, Japan)

      J. Agric. Food Chem. 38, 465-467 (1990). Analytical and preparative TLC of 2-methoxy-methyl-popyl-pyrazine on silica with acetone - hexane 1:9 and dichloromethane - ethyl acetate 6:1.

      Classification: 23e
      75 106
      (Determination of N-(ß-naphthyl)carbazole and N-(a-naphthyl)carbazole from photoinduced SRN1 reaction by thin-layer chromatography
      Y. FENG (Feng Yulin), ZH. ZHANG (Zhang Zhao), L. CHEN (Chen Liang), (Cent. Anal. & Test., Shanxi Univ., Taiyuan 030006, (Chinese)

      Chinese J. Instr. Anal. (Fenxiceshixuebao) 14, 73-75 (1995). TLC of the title compounds on silica with 1,2-dichloromethane - cyclohexane 1:4. Identification of the separated spots by IR. Quantification by densitometry at 288 nm.

      Classification: 23e
      93 075
      (Comparative study of extraction combination isolated from ingredients of Jiaotai pills by semi-bionic extraction
      X. ZHANG (Zhang Xuelan)*, ZH. ZHANG (Zhang ZHAOWANG) (*Shangdong Univ. TCM, Jinan 250014, P. R. China)

      J. Chinese Trad. Patent Med. (Zhongchengyao) 25 (7), 526-529 (2004). TLC on silica gel with benzene - ethyl acetate - methanol - isopropanol - conc. ammonia 20:10:5:5:1. Detection of berberine chloride under UV 365 nm. Identification by standard comparison. Quantification by densitometry at 342 nm. GC of volatile oil and HPLC of cinnamyl aldehyde. Discussion of the optimization of the extraction methods of combined ingredients of the medicine.

      Classification: 4d, 22, 23e
      100 052
      Chemical and analytical screening of some edible mushrooms
      U. MALLAVADHANI*, A. SUDHAKAR, K. SATYANARAYANA, A. MAHAPATRA, W. LI, R. BREEMEN. (*Center for Herbal Drugs, Regional Research Laboratory, Orissa, India, uvmavadani@yahoo.com)

      Food Chem. 95, 58-64 (2006). HPTLC of nicotinic acid (1) and pyrazole-3(5)-carboxylic acid (2) of Volvariella volvacea on silica gel with chloroform – methanol 17:3 with one drop of formic acid added. Quantitative determination by absorbance measurement at 190 nm for (1) and 262 nm for (2). The hRf values for (1) and (2) were 30 and 40, respectively. Linearity was between 400 and 7000 ng/zone (1) and 200 and 2500 ng/zone for (2). The limits of detection and quantification were 50 and 400 ng/zone for (1) and 20 and 200 ng/zone for (2). Recoveries of both compounds were between 96 and 102 %.

      Classification: 23e
      107 082
      Development and validation of TLC-densitometry method for the estimation of anti-psychotic drug in bulk and tablet formulation
      S. KATHIRVEL*, A. SUNEETHA, S. SUJANI (*Hindu College of Pharmacy, Amaravati Rd., Guntur-522002, India)

      62nd Indian Pharmaceutical Congress Abstract No. F-13 (2010). HPTLC of risperidone in bulk and pharmaceutical dosage form on silica gel with dichloromethane – methanol – ethanol – triethylamine 120:120:60:1. Quantitative determination by absorbance measurement at 280 nm. The linearity was obtained in the range 4-8 µg/spot (r2 =0.9989). The limit of detection and the limit of quantification for risperidone were 98 ng/zone and 599 ng/zone, respectively. The recovery was 99.5 %.

      Classification: 23e
      107 100
      Development and validation of HPTLC method for simultaneous estimation of hydrochlorothiazide and irbesartan in combined dosage form
      M. TRYAMBAKE*, S. SHINDE, A. CHABUKSWAR, S. JAGDALE (*MAEER’s Maharashtra Institute of Pharmacy, Kothrud, Pune 411038 (MS), India)

      62nd Indian Pharmaceutical Congress Abstract No. F-343 (2010). TLC of hydrochlorothiazide (HCTZ) and irbesartan (IRBE) on silica gel with toluene – acetic acid – methanol 70:2:50. Quantitative determination by absorbance measurement at 264 nm. The hRf values were 15 for HCTZ and 45 for IRBE. The linearity was in the range of 90-540 ng/band and 180-900 ng/band with r2= 0.9989 for HCTZ and IRBE. The recovery of HCTZ was 95.3-97.7 % and of IRBE 95.2-98.7 %.

      Classification: 23e
      119 046
      Antifungal amide alkaloids from the aerial parts of Piper flaviflorum and Piper sarmentosum
      Y. SHI (Shi Yan-Ni), F. LIU (Liu Fang-Fang), Melissa R. JACOB, X. LI (Li Xing-Cong), H. ZHU (Zhu Hong-Tao), D. WANG (Wang Dong), R. CHENG (Cheng Rong-Rong), C. YANG (Yang Chong-Ren), M. XU (Xu Min)*, Y. ZHANG (Zhang Ying-Jun)** (*/**Kunming Institute of Botany, Chinese Academy of Sciences, China; *xumin@mail.kib.ac.cn; **zhangyj@mail.kib.ac.cn)

      Planta Medica 83(01/02), 143-150 (2017). Preparative TLC on silica gel H to purify amide alkaloids from column chromatography apolar subfractions of aerial part methanolic extracts of: a) Piper flaviflorum: decenoylpiperidide (petroleum ether – acetone 10:1), N-methoxycinnamoyl-pyrrolidine, dihydropiperyline, stigmalactam, chingchengenamide A (petroleum ether – ethyl acetate 8:1); and b) P. sarmentosum: methylenedioxyphenyl-undecadienoyl/undecatrienoyl-pyrrolidine (petroleum ether – acetone 1:2), cinnamoyl-hydroxypyrrolidine and deacetylsarmentamide B (chloroform – methanol 9:1); detection with Dragendorffʼs reagent.

      Classification: 8b, 17c, 22, 23e, 32e