Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

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      123 046
      Determination of sugar biomarkers in methanol root extracts of Asparagus species by High-Performance Thin-Layer Chromatography
      M. KAPOOR, R. GUPTA, P. MAWAL*, S. PRADHAN (*Department of Botany, Punjabi University Patiala, Punjab 147002, India,

      J. Planar Chromatogr. 32, 109-114 (2019). HPTLC of fructose (1), glucose (2), maltose (3), raffinose (4) and sucrose (5) in the roots of the seven Asparagus species A. adscendens, A. racemosus, A. retrofractus, A. officinalis, A. densiflorus, A. falcatus, and A. sprengeri on silica gel with propanol - ethyl acetate - water 6:3:1. Detection by spraying with a methanolic solution of diphenylamine, aniline, and ortho-phosphoric acid, followed by heating at 140 °C for 2-3 min. Quantitative determination by absorbance measurement at 600 nm. The hRF values for (1) to (5) were 55, 50, 31, 11 and 46, respectively. Linearity was between 100 and 500 ng for (1) to (5). The intermediate precision was below 2 % (n=3). The LOD and LOQ were 22 and 66 ng for (1), 13 and 40 ng for (2), 51 and 155 ng for (3), 13 and 39 ng for (4) and 76 and 229 ng for (5), respectively. Average recovery was 97.9 % for (1), 99.9 % for (2), 99.3 % for (3), 98.3 % for (4) and 97.8 % for (5).

      Classification: 10a
      100 028
      Two new derivatization reagents for planar chromatographic quantification of sucralose in dietetic products
      Gertrud MORLOCK*, M. A. VEGA-HERRERRA (*University of Hohenheim, Institute of Food Chemistry, Garbenstrasse 28, 70599 Stuttgart, Germany;

      J. Planar Chromatogr. 20, 411-417 (2007). HPTLC of sucralose in dietetic products on silica gel impregnated with 0.1 M dipotassium hydrogen phosphate solution, and on amino phase with acetonitrile - water 17:3. Also a mixture of sucralose, sucrose, glucose, fructose was separated on amino phases with acetonitrile - water 3:1. Detection by dipping in 2-naphthol sulfuric acid reagent and aniline diphenylamine ortho-phosphoric acid reagent, followed by heating at 120 °C. Post-chromatographic derivatization on aluminium-backed amino plates was performed by heating the plate 190 °C for 20 min. Evaluation under UV light at 366 nm. For fluorescence enhancement the amino plate was dipped into a 1:2 solution of paraffin in n-hexane. Densitometric quantification by fluorescence measurement at 366 nm and by absorbance measurement at 500 and 405 nm.

      Classification: 10a
      109 005
      Thin-layer chromatography for the separation and analysis of acidic carbohydrates
      Z. ZHANG (Zhang Zhenqing), Z. XIAO (Xiao Zhongping), R. LINHARDT* (*Rensselaer Polytechnic Institute, Biotechnology Center 4005, 110 8th Street, Troy, NY 12180-3590, USA,

      J. Liq. Chromatogr. Relat. Technol. 32, 1711-1732 (2009). The authors described the TLC methods available for the analysis of acidic monosaccharides, disaccharides, and oligosaccharides derived from natural sources. TLC methods for the separation and visualization of monosaccharides are examined, as well as the successful application of TLC for ganglioside analysis and the application of these separations to neoglycolipids prepared from less tractable oligosaccharides and strong acidic animal polysaccharides, such as glycosaminoglycans.

      Keywords: food analysis review
      Classification: 1, 10a
      118 051
      Compositional evaluation of selected agro-industrial wastes as valuable sources for the recovery of complex carbohydrates
      A. VOJVODIC, D. KOMES, I. VOVK, A. BELSCAK, A. BUSIC (*Faculty of Food Technology and Biotechnology, University of Zagreb, Department of Food Engineering, Pierottijeva 6, 10 000 Zagreb, Croatia,

      Food Res. Int. 89, 565-573 (2016). HPTLC of galacturonic acid (1), galactose (2), glucose (3), mannose (4), arabinose (5), xylose (6) and rhamnose (7) in neutral hydrolysates from 5 plant secondary raw materials (sugar beet pulp, walnut shell, cocoa bean husk, onion peel and pea pods) on silica gel, impregnated by immersion in 0.5 M solution of monosodium phosphate, three times with acetonitrile – water – ethyl acetate – 1-propanol 17:3:4:4. Detection by dipping into diphenylamine-aniline-phosphoric acid reagent (2 % solution of diphenylamine and aniline, each in phosphoric acid – methanol 1:4), followed by heating at 150 ºC for 3 min. Qualitative identification using white light illumination. The hRF values for (1) to (7) were 1, 15, 22, 28, 37, 54 and 83, respectively.

      Classification: 10a
      60 060
      Synthesis of dabsylhydrazine and its use in the chromatographic determination of monosaccharides by thin-layer and high-performance liquid chromatography
      J.-K. LIN, S.-S. WU (Inst. of Biochemistry, Coll. of Med., Nat. Taiwan Univ., Taipei, Taiwan, P.R. China)

      Anal. Chem. 59, 1320-1326 (1987). TLC of monosaccharide dabsylhydrazones on silica with e.g. water saturated n-butanol - triethylamine 30:1, acetonitrile - benzene - ethyl acetate 15:15:1 or benzene - CHCl3 - EtOH 15:15:10. Dabsylhydrazones of D-glucose, palactose, mannose, fructose, arabinose, xylose, ribose, deoxyribose, glycerose.

      Classification: 10a
      67 064
      Analysis of mucin-derived oligosaccharides by medium-pressure gel-permeation and amino-plate thin-layer chromatography conducted in conjunction
      Y. GOSO, K. HOTTA, (Sch. Med., Kitasato Univ., Sagamihara, Japan 228)

      Anal. Biochem. 188, 181-186 (1990). TLC of GPC fractions of NaBH4-labeled oligosaccharides on 3-aminopropyl-bonded silica with acetonitrile - 10 mM triethylamine acetate 3:2. Detection and mapping according to size, anionic charge, and sugar composition. Determination of the distribution of oligosaccharides on bovine submaxillary mucin and rat gastric mucin.

      Classification: 4d, 10a
      80 035
      Thin-layer chromatography of aldopentose and aldohexose derivatives
      S.M. PETROVIC*, E. LONCAR, M. POPSAVIN, V. POPSAVIN, (*Dept. of Anal. Chem., Fac. of Techn., Univ. of Novi Sad, Bul. Cara Lazara 1, P.O. Box 340, 21000 Novi Sad, Yugoslavia)

      J. Planar Chromatogr. 10, 406-410 (1997). To study the relationship between chemical structure and retention behavior in TLC on silica, the retention constants of variously substituted 1,2-O-isopropylidene derivatives of aldohexoses and 1,2-O-cyclohexylidene derivatives of aldopentoses were measured as a function of the composition of eight binary mobile phases. The slopes and intercepts of the linear relationships between the retention constant (RM) and the logarithm of the volume fraction of the polar mobile phase component were calculated and are discussed in relation to solute and mobile phase characteristics. The RF values and relative retention of compounds depend largely on the retention behavior of their substituents.

      Classification: 2c, 10a
      91 019
      Chromatographic and spectroscopic analysis of the fluorescent compounds derived from monosaccharides on HPTLC-NH2 plates
      G. GRYGIERCZYK, W. FISCHER, M. SAJEWICZ, P. KUS, R. WRZALIK, M. CZAJA, M. DZIADEK, T. KOWALSKA*, (*Inst. of Chem., Silesian Univ., 9 Szkolna Str., 40-006 Katowice, Poland)

      J. Planar Chromatogr. 15, 449-453 (2002). Possible explanation of a detection process HPTLC of D-(+)-glucose, D-(+)-galactose, and D-(-)fructose on NH2-phase with 1-propanol - nitromethane - water 5:3:2. Detection after drying for 24 h and heating at 130 - 140°C for 3-4 min and inspection under UV 366 nm. It is suggested that during heating the analytes probably undergo a process which results in a structural transformation possibly analogous to the Maillard reaction.

      Classification: 10a