Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
- Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
- Keyword register: select an initial character and browse associated keywords
- Search by CBS edition: Select a CBS edition and find all related publications
Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.
J. Liquid Chromatogr. 6, 55-62 (1983). TLC of prostanoids (PGF2 alpha, PGE2; 15-keto-PGE2; 15-keto PGF2 alpha l3,14-dihydro-15-keto-GE2; 13,14-dihydro-15-keto-PGF2 alpha; tromboxane B2, arachidonic acid on silica with chloroform - methanol - acetic acid - water 95:5:1:0.2. Detection with iodine vapor. Radioassay.
Microtechniques. J. Planar Chromatogr. 2, 389-391 (1989). HPTLC separation of neutral lipids, cholesteryl esters, and phospholipids on silica with carbon tetrachloride - propanol - ethyl acetate - chloroform - methanol - ethanol - 43 mM potassium chloride 23:23:29:11:12 or chloroform - methyl acetate - ethyl acetate - methanol - hexane 2000:15:30:30:15 as mobile phases; detection by spraying with phosphomolybdic acid or copper(II)sulfate reagent followed by heating at 100-150 °C for 2-5 min. The methods described allows the determination of 21 different components within 15 min.
J. Planar Chromatogr. 5, 87-91 (1992). Comparison of ANS (8-anilo-1-naphthalene sulfonate, ammonium salt), rhodamine B, nile red, dichlorofluorescein with hematoporphyrin; visual comparison under UV 366 nm. Limits of (visual) detection (LOD) were 10-20 ng for the cationic surfactants, and 5 and 10 ng, respectively, for the phospholipids (sphingomyelin and lecithin) and cholesterol.
J. Planar Chromatogr. 10, 128-130 (1997). HPTLC of the lipid composition of a fresh-water snail. The major neutral lipids and their mean percentage net weight were triacylglycerols (0.107%), free sterols (0.496%), and free fatty acids (0.180%). The major phospholipids were phosphatidylcholine (0.451%) and phosphatidyl-ethanolamine (0.335%). HPTLC of neutral lipids on silica with petrol ether - ether - acetic acid 40:10:1 after equilibration for 10 min. Detection by spraying with 5% ethanolic phosphomolybdic acid and heating for 15 min 115°C. Quantification by densitometry at 700 nm. HPTLC of phospholipids on silica with chloroform - methanol - water 65:25:4. Detection as black spots by spraying the dried plate with a 10% solution of cupric sulfate in 8% phosphoric acid and heating at 160°C for 10 min. Densitometry at 370 nm.
J. Chromatogr. B, 757 (2), 317-324 (2001). Description of a non-radioactive micro-assay for the cyclic phosphodiesterase reaction catalyzed by Bacillus cereus phosphatidylinositol-specific phospholipase C, involving HPTLC on silica gel to resolve the substrate (myo-inositol 1,2-cyclic phosphate and the product (myo-inositol 1-phosphate), followed by detection with a lead tetraacetate-fluorescein stain. Quantitation by analysis of the fluorescent plate image with a commercial phosphoimager and associated software, for sample in the rage of 0.1 to 50 nmol.
Part II. Nicotinic acid and its esters. J. Liq. Chromatogr. Relat. Technol. 30, 2419-2433 (2007). TLC and HPTLC of nicotinic acid and methyl nicotinate, ethyl nicotinate, isopropyl nicotinate, butyl nicotinate, and benzyl nicotinate on RP-18 (prewashed with methanol) with methanol - water and dioxane - water in 10 % volume ratio steps from 100:0 to 0:100 in a chamber saturated for 30 min. TLC on aluminium oxide (prewashed with methanol) with acetone - n-hexane 1:4 provided the optimum conditions for complete separation. Quantitative determination by absorbance measurement at 254 nm.
Asian Journal of Chemistry 23(1), 469-470 (2011). Several herbal formulations were analyzed for gallic acid contents. Tablets were powdered, subjected to hydrolysis by refluxing with 10 % HCl, filtrated and extracted with chloroform. Acidic aqueous extracts were concentrated and the residue was taken up in methanol. TLC on silica gel with ethyl acetate - formic acid 85:11. Gallic acid was observed at an hRf value of 89. Densitometric quantification of gallic acid at 272 nm. The method was linear in the range of 100-3000 ng/band. The method was suitable for analysis of formulations without interference from excipients. Gallic acid contents of different tablet samples varied from 0.06-0.15 % w/w.
International Journal of Pharmaceutical Sciences Review and Research 2(2), 35-39 (2010). TLC on silica gel with methanol - chloroform 1:6. The hRf value was 38 and 68 for ramipril and telmisartan respectively. Densitometric evaluation at 210 nm. The method was linear in the range of 300-3000 ng/band and 500-4000 ng/band for ramipril and telmisartan respectively. The recovery was 98-102 %. The sample was subjected to different stress conditions (acid, base, oxidative, heat, photolytic) and all the degradation products were well separated from drug.