Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      59 065
      Hydrolysis of all- gangliosides including GM1 and GM2 on thin-layer plates by vibrio cholerae neuraminidase
      J. PORTOVKALIAN, B. BOUCHON, (Lab. Immuno., Cent. Leon Berard, F-69373 Lyon)

      J. Chromatogr. 380, 386-392 (1986). TLC of humanmelanoma gangliosides on silica with chloroform - methanol - 0.2 % calcium chloride 60:35:8. Hydrolysis with 0.5 unit neuraminidase in 5 ml buffer maintained on plate for 18 h. Detection of the products specific to gangliosides GM2 and CD2 by an immunoperoxidase staining system after treatment with monoclonal antigangliotetraosylceramide.

      Classification: 11
      69 158
      Comparison of induced vapor phase fluorescent responses of four polycyclic ether antibiotics and several lipid classes on RP-18 and silica gel HPTLC plates
      R.J. MAXWELL*, J. UNRUH, (Dept. of Agric., Agric. Res. Service, Eastern Reg. Res. Center, 600 East Mermaid Lane, Philadelphia, PA 19118, USA)

      J. Planar Chromatogr. 5, 35-40 (1992). HPTLC of lasalocid sodium, monensin sodium, narasin sodium, salinomycin sodium on silica and RP-18 with ethyl acetate – water 100:3 resp. with methanol – 5% aqueous acetic acid 9:1 (2 x). Lipids (i.a. L-a-phospatidylcholine-ß-linoleoyl-y-palmitoyl, dipalmitoyl L-a-phosphatidylethanolamine, triolein, oleic acid, L-a-dipalmitoyl phosphatidylcholine) were chromatographed with cyclohexane – ether – acetic acid 90:10:1 on silica, with chloroform on RP-18. VPF resposes on silica and RP-18 have been compared for both classes of compounds: the respose of the polycyclic ether antibiothics narasin and salinomycin on RP-18 plates was three times greater than on silica; lipids with the exception of cholesterol could be detected only on silica plates. Quantification by fluoro densitometry at 366/>400 nm.

      Classification: 11, 28
      78 057
      (Simultaneous separation of the metablins of amino acids, organic acids and nucleosides in clinical chemistry by two-dimensional thin-layer chromatography
      Y. WU (Wu Youguang), B. KUANG (Kuang Bohai), F. LONG (Long Fei), (Jiangxi Med. Coll., Nanchang 330006, P.R. China)

      Chromatogr. (Sepu) 14, 259-263 (1996). Two dimensional TLC of 30 amino acids, 40 organic acids and 20 nucleosides and related compounds on cellulose - silica with 1) isopropanol - ethyl acetate - acetone - methanol - para-amyl alcohol - NH3 - water 9:3:3:1:1:3:3, butanol - isopropanol - acetone - formic acid - water 18:8:8:3:6, 2) tert-butanol - ethanol - NH3 - water 5:6:1:3, isopentanol - petrol ether - ethanol - formic acid - propionic acid - water 45:100:25:20:1:1, 3) isopropanol - ethyl acetate - methanol - NH3 - water 5:3:1:3:1, isopropanol - saturated (NH4)2SO4 - water 4:77:19, for both direction, respectively. Detection under UV 254 nm, by spraying with 0.1 % acridine in ethanol, by spraying with ninhydrin-cadmium acetate reagent. Detection limit 10-10 - 10-11 mol, 2x10-8 - 5x10-8 mol, and 1x10-8 - 3x10-8 mol, respectively.

      Classification: 11, 18a
      87 034
      Highly-substituted benzhydrylamine resin
      R.S.H. CARVALHO, A.H. STRAUS, H.K. TAKAHASHI*, C.R. NAKAIE, (*Dept. Biochem. Univ. Fed. Sao Pauolo, Rua Batucatu 862, 04023-900, Sao Paulo, SP, Brazil)

      Chromatographia 52, (5/6), 363-366 (2000). Purification by liquid chromatography using the highly-substituted benzhydrylamine resin as stationary phase. Analysis of different fractions by TLC on silica gel with chloroform - methanol - aqueous CaCl2. Detection by spraying with ocinol - sulfuric acid reagent, and resorcinol - sulfuric acid reagent.

      Keywords:
      Classification: 4d, 11
      102 026
      TLC and GC-MS probes into the fatty acid composition of some Lycoperdaceae mushrooms
      D. NEDELCHEVA, D. ANTONOVA, S. TSVETKOVA, I. MAREKOV, S. MOMCHILOVA, Boryana NIKOLOVA-DAMYANOVA*, M. GYOSHEVA (*Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences, 1113 Sofia, Bulgaria; bmd@orgchm.bas.bg)

      J. Liq. Chromatogr. Relat. Technol. 30, 2717-2727 (2007). Identification of lipid classes, e. g. fatty acid methyl esters, and polar lipids (presumably phospholipids), free fatty acids, sterols, triacylglycerols, fatty acid esters, by TLC on silica gel with n-hexane - acetone 25:4. Detection by spraying with 50 % ethanolic sulfuric acid and heating at 200 °C. The mushrooms contained a characteristic group of three isomeric hexadecenoic fatty acids (double bond in positions 6-, 9-, and 11-) which are resolved and determined separately for the first time.

      Classification: 11a
      105 014
      Comparison of methods for calculation of the partition coefficients of selected aliphatic compounds
      Anna NIESTROJ (Silesian University, Institute of Chemistry, 9 Szkolna Street, 40-006 Katowice, Poland; annaniestroj@wp.pl)

      J. Planar Chromatogr. 23, 198-200 (2010). Proposition of new methods for calculation of the partition coefficients of aliphatic compounds from experimental Rf values and the numerical values of selected topological indexes. The experimental partition coefficient (log Pexp) of cetyl alcohol was determined for the n-octanol-water system. Numerical values obtained were compared with theoretical values from a database (AlogPs, AC_logP, AB/LogP, ALOGP, milogP, and XLOGP2). HPTLC of cetyl alcohol, stearyl alcohol, palmitic acid, stearic acid, alpha-hydroxypalmitic acid, and 12-hydroxystearic acid on RP18 with methanol and with methanol - water 19:1 in a horizontal chamber at room temperature. Detection after visualization in iodine vapor.

      Classification: 6, 11a
      106 056
      Development and validation of HPTLC method for determination of betulinic acid in Helicteres isora root extract
      K. PAGI*, S. LAHIRI, G. YADAV, Mamta SHAH (*Dept. of Phytochemistry and Pharmacognosy, L.M. College of Pharmacy, Navarangpura, Ahmedabad, Gujarat 380009, India, mbshah2007@rediffmail.com)

      International Journal of ChemTech Research 2(2), 851-855 (2010). Defatted powdered roots of Helicteres isora (Sterculiaceae) were extracted with ethyl acetate. TLC on silica gel with toluene - acetone - formic acid 25:5:2. The hRf value was 43. Densitometric evaluation at 540 nm. The method was linear in the range of 100-500 ng/band. Recovery was 98.4-99.9 %.

      Classification: 11a
      106 075
      Application of TLC-densitometry method for simultaneous estimation of telmisartan and amlodipine besylate in pharmceutical dosage form
      N. VEKARIYA*, G. PATE, H. BHATT, M. PATEL, R. DHOLAKIYA, G. RAMANI (*Shree Dhanvantary Pharmacy College, Kim, Dist Surat, Gujarat, India, Smt B.N.B. Swaminarayan Pharmacy College, Salvav Dist. Valsad, Gujarat, India)

      International Journal of PharmTech Research 1(4), 1644-1649 (2009). TLC of telmisartan and amlodipine besylate on silica gel with tetrahydrofuran - dichloromethane - methanol - 25 % ammonia 30:10:5:1. The hRf value for telmisartan was 22 and for amlodipine 45. Densitometric evaluation in absorbance mode at 326 nm. The method was linear in the range of 1200-7200 ng/band for telmisartan and 400-1400 ng/band for amlodipine. The average recovery was 100.7-101.5 %.

      Classification: 11a