Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      109 023
      Development and validation of a novel HPTLC method for simultaneous estimation of beta-sitosterol-D-glucoside and withaferin-A
      Supriya JIRGE*, Pratimaa TATKE, SATISH GABHE (*C. U. Shah College of Pharmacy, SNDT Woman University, Mumbai-400049, India)

      International Journal of Pharmacy & Pharmaceutical Sciences 3(2), 227-230 (2011). TLC of beta-sitosterol-D-glucoside and withaferin-A in Withania somifera formulations on silica gel with chloroform - methanol 4:1. The hRf value of beta-sitosterol-D-glucoside was 21 and of withaferin-A 59. Quantitative absorbance measurement at 207 nm. The method was linear in the range of 50-500ng/band for beta-sitosterol-D-glucoside and in the range of 5-50 ng/band for withaferin-A.

      Classification: 8b
      116 028
      Isolation, cytotoxic evaluation, and
      simultaneous quantification of eight bioactive secondary metabolites from Cicer
      microphyllum by high-performance thin-layer chromatography
      A. DAR, S. RATH, A. QAUDRI, B. SINGH, S. TASDUQ, A. KUMAR, P. SANGWAN* (*Bio-organic Chemistry Division, CSIR-Indian Institute of Integrative Medicine (CSIR-IIIM),
      Jammu Tawi, India, plsangwan@iiim.ac.in)

      J. Sep. Sci. 38, 4021-4028 (2015). HPTLC of eight natural products viz. stigmasterol (1), oleanolic acid-3-acetate (2), oleanolic acid (3), biochanin A (4), genistein (5), pratensein (6), chrysoeriol (7), and luteolin (8) in Cicer microphyllum on silica gel with n-hexane - ethyl acetate - formic acid 90:65:8. Detection by dipping into a solution of cerric ammonium sulfate reagent, followed by heating at 105 °C for 5 min. Quantitative determination by absorbance measurement at 366 nm. The hRF values for compounds (1) to (8) were 98, 89, 78, 70, 63, 42, 33 and 4, respectively. Linearity was in the range of 100-800 ng/zone for (1) to (8). LOD and LOQ were 60 and 90 ng/zone for (1), (5) and (8), 50 and 90 ng/zone for (2), 90 and 110 ng/zone for (3), 70 and 100 ng/zone for (4) and (6) and 80 and 110 ng/zone for (7). The intermediate precision was below 1.5 % (n=3). Recovery was in the range of 98-100 %.

      Classification: 8b, 13c
      120 003
      A review of methods for the chemical characterization of cannabis natural products
      A. LEGHISSA, Z. HILDENBRAND, K. SCHUG* (*Department of Chemistry and Biochemistry, The University of Texas at Arlington, Arlington, TX, USA, kschug@uta.edu)

      J. Sep. Sci. 41, 398-415 (2018). Review of analytical methods for the analysis of cannabinoids and their metabolites in cannabis, including the application of TLC and HPTLC. The review highlighted the use of automated multiple development (AMD) and optimum performance (or over-pressure) layer chromatography (OPLC) as considerable improvements to the use of classic TLC for cannabis analysis.

      Classification: 1, 8b
      57 052
      Quantitative analysis of mutagenic components by thin-layer chromatography
      H. KANAMORI, I. SAKAMOTO, M. MIZUTA, O. TANAKA

      Chem. Pharm. Bull. 32, 4942-4945 (1984). TLC of 7 mutagenic xanthones on silica. Quantification by densitometry. Investigation of the conditions of the analysis. The relationship between xanthone content and mutagenicity is discussed.

      Classification: 8b, 32e
      61 068
      Fate of ingested aristolochic acids in Battus archidamas
      A. URZUA*, R. RODRIGUEZ, B. CASSELS, (*Depart. de Quimica, Facultad de Ciencia, Univ. de Santiago de Chile, Casilla 5659, Santiago-2, Chile)

      Biochemical Systematics and Ecology 15, 687-689 (1987). TLC of aristolochic acids on silica with chloroform - methanol 85:15 or 2:1. Quantification by spectrophotometry at 254 nm.

      Classification: 8b
      66 049
      A-type proanthocyanidins from stem-bark of Pavetta owariensis
      A.M. BALDE, L.A. PIETERS, A. GERGELY, H. KOLODZIEJ, M. CLAEYS, A.J. VLIETINCK*, (*Dep. Pharm. Sci., Univ. Antwerp (U.I.A.), B-2610 Antwerp, Belgium)

      Phytochemistry 30, 337-342 (1991). TLC of various proanthocyanidins on silica with ethyl acetate – formic acid – acetic acid – water 140:2:1:59 or on cellulose with water. Detection under UV or by spraying with vanillin – sulfuric acid or anisaldehyde – sulfuric acid reagents. TLC of acetate derivatives on silica with toluene – acetone 2:1. Also column chromatography and droplet counter-current chromatography (DCCC).

      Classification: 8b
      70 007
      Retardation behavior and prediction of Rf values in TLC using the „PRISMA“ model
      P. HÄRMÄLÄ, (Pharmacognosy Div., Dept. of Pharm., Univ. of Helsinki, SF-001 70 Helsinki, Finland)

      I. Regular part of the model. J. Planar Chromatogr. 4, 460-466 (1991). Manual examination of the retardation behavior of 16 apolar, closely related coumarins in normal phase TLC using the regular part of the three-dimensional „PRISMA“ model. The results show a highly significant second order dependency between the retardation factor (Rt) and the solvent strength (vertical correlation), as well as between the retardation factor and the selectivity point (horizontal factor).

      Classification: 2e, 8b
      75 044
      Characterization of oxygen-containing adamantane derivatives by thin-layer chromatography
      J. TRISKA*, E.P. BUTKUS, (*Lab. of Anal. Chem. and Biochem., Inst. of Landscape Ecology, Czech Acad. of Sci., Branisovska 31, Ceske Budejovice, Czech Republic)

      J. Planar Chromatogr. 8, 243-344 (1995). TLC of 15 oxygen-containing adamantanes on alumina with chloroform - acetone - methanol 36:12:1, chloroform - acetone 6:1, carbon tetrachloride - acetone 30:7 or chloroform - acetone 18:6 or on silica with chloroform - methanol 50:3 or 14:1. Detection by exposure to iodine vapor.

      Classification: 5b, 8b