Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      132 003
      Development and validation of an assay for the quantification of glycosides using high‑performance thin‑layer chromatography (HPTLC)
      S. SULTANA, K. FOSTER, M. HOSSAIN, L. LIM, C. LOCHER* (*Division of Pharmacy, School of Allied Health, University of Western Australia, Crawley 6009, Australia, connie.locher@uwa.edu.au)

      J. Planar Chromatogr. 36, 179-190 (2023). HPTLC of genistin (1), ononin (2), rutin (3) and luteolin-6-C-glucoside (4) in rutin commercial products on silica gel with ethyl acetate - methanol - glacial acetic acid - formic acid 11:1:1:1. Detection by derivatization with natural products polyethylene glycol reagent. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (4) were 50, 46, 21 and 29, respectively. Linearity was in the range of 60-300 ng/zone for (1) to (4). Intermediate precisions were below 3 % (n=3). LOD and LOQ were 8 and 24 ng/zone for (1), (2) and (4), and 11 and 32 ng/zone for (3). Recovery was between 98.2 and 102.0 % for (1), 100.5 and 100.8 % for (2), 99.8 and 101.6 % for (3) and 99.7 and 100.3 % for (4).

      Classification: 8b, 10
      131 012
      Chemical comparison of monk fruit products processed by different drying methods using High-Performance Thin-Layer Chromatography combined with chemometric analysis
      H. HONG (Hong Huijie), Q. YANG (Yang Qi), Q. LIU (Liu Qiao), F. LEONG (Leong Fong), X. CHEN (Chen Xiaojia)* (*State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau, Macau, Macao SAR, China, XiaojiaChen@um.edu.mo)

      Front. Nutr. 9, 887992 (2022). HPTLC of 13 mogrosides, 1 flavonoid, and 3 sugars in monk fruit products on silica gel with n-butanol - water - ethanol - acetic acid 70:10:10:2. Detection by spraying with 10 % sulfuric acid in ethanol solution, followed by heating at 105 °C for 10 min. Orthogonal partial least square-discriminant analysis (OPLS-DA) was subsequently conducted allowing the identification mogroside V, 11-oxo-mogroside V, isomogroside V, mogroside IV and sucrose to be the characteristic compounds to distinguish the two types of monk fruits.

      Classification: 8a
      131 020
      Iridoid-glycoside isolation and purification from Premna fulva leaves
      F. HE (He Feifan), X. YAN (Yan Xiaojie), N. ZHAO (Zhao Ningtao), X. JIANG (Jiang Xiaohua), Y. WEI (Wei Yulu), F. LU (Lu Fenglai), H. LI (Li Heping), D. LI (Li Dianpeng)*, Y. CHEN (Chen Yueyuan) (*Guangxi Key Laboratory of Plant Functional Phytochemicals and Sustainable Utilization, Guangxi Institute of Botany, Guangxi Zhuang Autonomous Region, P. R. China, phytoldp@hotmail.com)

      J. Sep. Sci. 46, 2300059 (2023). HPTLC of iridoid and iridoid glycoside in Premna fulva on silica gel with ethyl acetate - n-butanol - water 3:1:4. Detection by spraying with 10 % sulfuric acid - ethanol chromogenic agent, followed by heating. The system showed a hRF values from 30 and 70. The method was applied for candidate solvent-system prediction with a generally useful estimate of the solvent systems (GUESS). Further analysis by high-speed counter-current chromatography.

      Classification: 8b
      131 022
      The potential off-target neuroprotective effect of sister gliflozins suggests their repurposing despite not crossing the blood–brain barrier: From bioanalytical assay in rats into theory genesis
      M. HENDY*, S. MOWAKA, E. ELKADY, A. EL-ZAHER, B. AYOUB (*School of Arts and Sciences, Concordia University Irvine (CUI), 1530 Concordia West, Irvine, CA 92612, USA, bassam.ayoub@cui.edu,)

      J. Sep. Sci. 46, 2200921 (2023). Review of the techniques for the analysis of sodium-glucose linked transporter-2 (SGLT-2) inhibitors, including HPTLC for the determination of canagliflozin, dapagliflozin and empagliflozin.

      Classification: 1b, 8a
      131 024
      Two-step isolation of the two major paraconic acids of Cetraria islandica
      E. VILLICAÑA, S. SCHWAIGER*, H. STUPPNER (*Institute of Pharmacy/Pharmacognosy, CMBI, University of Innsbruck, Innrain 80/82, Innsbruck, Austria, Stefan.Schwaiger@uibk.ac.at)

      J. Sep. Sci. 46, 2200805 (2023). HPTLC of paraconic acids in Cetraria islandica on silica gel with cyclohexane - ter-butyl-methyl-ether - formic acid 16:6:1. Detection by exposure to iodine vapor and spraying with a starch solution. Further analysis by LC-MS.

      Classification: 8
      131 009
      Detection of coumarin derivatives of Viola odorata cultivated in Iraq
      Zainab A. ALI*, I. SALEH, W.M.K. ALANI (*College of Pharmacy, Mustansiriah University, Baghdad, Iraq; zaineb-aziz@esraa.edu.iq)

      J Pharm Bioallied Sci 15(Suppl.2), S948-S951 (2023). Sample was the ethyl acetate fraction of an ethanolic extract of Viola odorata aerial parts (Violaceae). Standards were coumarinic compounds: esculetin (1) and umbelliferone (2). TLC and HPTLC on silica gel with toluene – ethyl acetate – formic acid 5:4:1. Visualization under UV 254 nm and 366 nm; densitometric scanning at 366 nm. Both (1) and (2) were found in the extract (hRF values 30 and 53, respectively, in TLC). Alternative mobile phases were also tested (TLC only): toluene – ethyl acetate 1:1 (hRF values 47 and 68) and chloroform – methanol 97:3 (hRF values 20 and 41).

      Classification: 8b, 32e
      131 057
      Analytical method development and validation for the simultaneous estimation of quercetin, berberine, rutin and curcumin in a polyherbal formulation using high‑performance thin‑layer chromatography
      A. KHAINAR, S. LOHIDASAN*, R. DUBEY, S. SANKARAN (*Department of Quality Assurance Techniques, Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune 411038, Maharashtra, India, l.satyanarayan@bharatividyapeeth.edu)

      J. Planar Chromatogr. 36, 63-70 (2023). HPTLC of quercetin (1), berberine (2), rutin (3) and curcumin (4) in a polyherbal formulation on silica gel with toluene - ethyl acetate - methanol - formic acid 10:6:4:1. Quantitative determination by absorbance measurement at 366 nm for (1) to (3) and 425 nm for (4). The hRF values for (1) to (4) were 57, 30, 9 and 66, respectively. Linearity was in the range of 500-3000 ng/zone for (1), 200-700 ng/zone for (2), 1000-6000 ng/zone for (3) and 100-350 ng/zone for (4). Intermediate precisions were below 2 % (n=6). LOD and LOQ were 119 and 362 ng/zone for (1), 33 and 100 ng/zone for (2), 248 and 750 ng/zone for (3) and 14 and 42 ng/zone for (4). Recovery was between 95 and 102 % for (1) to (4).

      Classification: 7, 8a, 8b
      131 057
      Analytical method development and validation for the simultaneous estimation of quercetin, berberine, rutin and curcumin in a polyherbal formulation using high‑performance thin‑layer chromatography
      A. KHAINAR, S. LOHIDASAN*, R. DUBEY, S. SANKARAN (*Department of Quality Assurance Techniques, Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune 411038, Maharashtra, India, l.satyanarayan@bharatividyapeeth.edu)

      J. Planar Chromatogr. 36, 63-70 (2023). HPTLC of quercetin (1), berberine (2), rutin (3) and curcumin (4) in a polyherbal formulation on silica gel with toluene - ethyl acetate - methanol - formic acid 10:6:4:1. Quantitative determination by absorbance measurement at 366 nm for (1) to (3) and 425 nm for (4). The hRF values for (1) to (4) were 57, 30, 9 and 66, respectively. Linearity was in the range of 500-3000 ng/zone for (1), 200-700 ng/zone for (2), 1000-6000 ng/zone for (3) and 100-350 ng/zone for (4). Intermediate precisions were below 2 % (n=6). LOD and LOQ were 119 and 362 ng/zone for (1), 33 and 100 ng/zone for (2), 248 and 750 ng/zone for (3) and 14 and 42 ng/zone for (4). Recovery was between 95 and 102 % for (1) to (4).

      Classification: 7, 8a, 8b