Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

      90 022
      Two types of oxidative dimerization of the black tea polyphenol theaflavin
      T. TANAKA, K. INOUE, Y. BETSUMIYA, C. MINE, I. KOUNO*, (*School of Pharm. Sci., Nagasaki Univ., 1-14 Bunkyo-machi, Nagasaki 852-8521, Japan)

      J. Agric. Food Chem. 49, 5785-5789 (2001). TLC of bistheaflavin A, theanaphthoquinone, theaflavin on silica gel with benzene - ethyl formate - formic acid 1:7:1 or chloroform - methanol - water 14:6:1. Detection under UV and by spraying with 2% ethanolic iron(III)chloride solution or 10% sulfuric acid reagent, followed by heating.

      Keywords:
      Classification: 8a
      94 021
      A rapid TLC method for analysis of external flavonoid aglycones in plant exudates
      M. NIKOLOVA*, S. BERKOV, S. IVANCHEVA (*Dep. Appl. Botany, Inst. Botany, Bulgarian Acad. Sci., Acad. G. Bonchev Str. 23, 1113 Sofia, Bulgaria)

      Acta Chromatographica 14, 110-114 (2004). TLC of external flavonoid aglycones on silica gel with toluene - dioxane - acetic acid 95:25:4 for Veronica exudates, and toluene - acetic acid 2:1 for Artemisia exudates. Detection by spraying with “Naturstoffreagenz A” reagent. Documentation of apigenin and quercetin under UV 366 nm by digital camera. Quantitative determination by comparison with the peak areas of the standards. Evaluation of suitability of the method for routine assays with large number of samples.

      Classification: 8a
      98 033
      HPTLC, with UV and MS detection, and preparative-layer chromatography for analysis and purification of synthesis products
      P. K. SALO, A. ESSÉN-SUURONEN, H. SALOMIES, R. A. KETOLA, R. KOSTIAINEN* (*Faculty of Pharmacy, Division of Pharmaceutical Chemistry, P. O. Box 56, FIN-00014 University of Helsinki, Finland)

      J. Planar Chromatogr. 19, 371-377 (2006). HPTLC of five isoflavone products and 2-phenylchromone as reference standard on silica gel, pre-washed with acetonitrile, in an unsaturated chamber, twice with chloroform or dichloromethane. Determination by absorbance measurement at 280 nm. Preparative layer chromatography on silica gel. A new device for isolation of sythesis products in sub-milligram amounts was successfully employed.

      Classification: 8a
      106 035
      Development of HPTLC method for estimation of wedelolactone, quercetin and jatamansone in polyherbal formulation
      R. THORAT*, V. JADHAV, V. KADAM, S. KAMBLE & K. SALASKAR (*Dept. of Q. A., Bharati Vidyapeeth’s College of Pharmacy, Sector 8, CBD Belapur, Navi-Mumbai 400614, India, drvmjadhav_bvcop@rediffmail.com)

      International Journal of ChemTech Research 1(4), 1079-1086 (2009). TLC of wedelolactone, quercetin, and jatamansone in a polyherbal formulation. The formulation (oil) was extracted with methanol, the supernatant was concentrated under vacuum and used for chromatographic analysis. TLC on silica gel with toluene - acetone - formic acid 11:6:1 for wedelolactone, toluene - ethyl acetate - methanol 44:50:6 for quercetin and petroleum ether - acetone 3:1 for jatamansone. The hRf value of jatamansone was 34, of wedelolactone 56, and of quercetin 47. Densitometric evaluation at 254 nm, 285 nm and 366 nm for quercetin, jatamansone, and wedelolactone respecticely. The method was linear in the range of 500-2500 ng/band for wedelolactone, 3000-8000 ng/band for quercetin and 2000-6000 ng/band for jatamansone. The polyherbal oil formulation contained 1.62 %, 0.24 % and 0.11 % of wedelolactone, quercetin, and jatamansone respectively.

      Classification: 8b
      114 017
      A stability-indicating assay of biomarker bergenin in the aerial parts of Flueggea virosa by a validated high-performance thin-layer chromatographic–densitometric method
      P. ALAM*, A. AL-REHAILY, N. SIDDIQUI, E. AL-SHEDDI, F. SHAKEEL (*Department of
      Pharmacognosy, College of Pharmacy, King Saud University, Riyadh, Kingdom
      of Saudi Arabia, alamperwez007@gmail.com)

      J. Planar Chromatogr. 28, 54-60 (2015). HPTLC of bergenin in the aerial parts of Flueggea virosa on silica gel with dichloromethane – methanol 17:3. Quantitative determination by absorbance measurement at 220 nm. The hRF value of bergenin was 29. Linearity was between 100 and 800 ng/zone. The intermediate intra-day and inter-day precisions were below 2 % (n=6). The LOD and LOQ for bergenin were 18 and 53 ng/zone, respectively. Recoveries were in the range of 99-100 %.

      Classification: 8b
      118 038
      Quantitative analysis of phytochemicals from
      Inula cappa roots
      J. KALOLA, R. SHAH, M. SHAH* (*Department of Pharmacognosy, L. M. College of
      Pharmacy, Navarangpura, Ahmedabad, 380 009, Gujarat, India, mbshah2007@rediffmail.com)

      J. Planar Chromatogr. 29, 336-340 (2016). HPTLC of isoalantolactone (1), germacranolide (2), β-sitosterol (3), and lupeol (4) in the roots of Inula cappa on silica gel with toluene ‒ methanol 47:3. Detection by dipping into anisaldehyde reagent followed by heating at 105 ºC until colored bands appeared. Quantitative determination by absorbance measurement at 525 nm. Linearity ranged from 10-70 μg/mL for (1), 10-60 μg/mL for (2), 8-48 μg/mL for (3) and 15-90 μg/mL for (4). The intermediate precisions were below 0.9 % (n=7). The LODs and LOQs were 5 and 10 μg/mL for (1), (2) and (4) and 2 and 6 μg/mL for (3). Average recoveries were between 98.3 and 99.0 % for (1) to (4).

      Classification: 8b, 14
      121 039
      Synthetic modification of 9?- and 9?-hydroxyparthenolide by Heck or acylation reactions and evaluation of cytotoxic activities
      A. EL BOUAKHER, B. JISMY, H. ALLOUCHI, E. DUVERGER, L. BARKAOUI, A. EL HAKMAOUI, R. DANIELLOU, G. GUILLAUMET, M. AKSSIRA* (*Laboratoire de Chimie Physique & de Chimie Bioorganique, Université Hassan II Casablanca, Mohammedia, Morocco; akssira@fstm.ac.ma)

      Planta Med. 83(07), 661-671 (2017). Structural modifications of 9α- and 9β-hydroxyparthenolide (isolated from Anvillea radiata aerial parts) were performed either by Heck’s reaction (a palladium(II) acetate treatment in presence of triethylamine and iodoaryl in dimethylformamide), or by acylation (here, addition of aroyl chlorides and/or acetic anhydride in dichloromethane and pyridine). TLC for reaction monitoring of the 21 derivatives on silica gel with petroleum ether – ethyl acetate in various proportions (3:2; 1:4; 1:1). Detection under UV or under white light after spraying with 5 % phosphomolybdic acid in ethanol, followed by heating.

      Classification: 8b, 15a, 32e
      58 166
      Determination of phenolic compounds in colladonia triquetra L
      M. SIMOVA, E. TOMOV, T. PANGAROVA, N. PAVLOVA

      J. Chromatogr. 351, 379-382 (1986). TLC of plant extracts containing the xanthone-C-glycoside mangiferin on silica with ethyl acetate - formic acid - water 67:13:20. Densitometric determination at 366 nm. Also TLC of colladin and colladonin with benzene - MEK - formic acid 9:1:1. Comparison with HPLC. Method suitable for the quantitative determination of other xanthone glycosides and coumarins in plant extracts.

      Classification: 8b, 32e