Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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JAOAC Int. 83, 675-678 (2000). TLC of mono- and disaccharides (with D(-)-fructose and D(+)-sucrose as standards) before and after hydrolysis - (30 min with 1 % oxalic acid in a boiling water bath) - on silica gel with acetonitrile-diluted phosphate buffer solution pH 5.5 17:3. Detection by immersion of the plate for 1 s into a solution of 2 mL aniline and 2 g of diphenylamine in 100 mL methanol and 15 mL o-phosphoric acid (85 %) and heating for 10 min at 120°C. Quantitation by densitometry at 560 nm in absorption/transmission mode. Improved and simple method for the determination of fructan inulin in yoghurts, honey cakes and chocolates.
J. Chromatogr. A 1110 (1-2), 214-221 (2006). Presentation of a rapid, simple and inexpensive method for the analysis of fructooligosaccharides as feed additives (prebiotics) in complicated biological samples with minimal pre-treatment. TLC of fructooligosaccharides in dietetic products and in samples from intestinal tract of monogastric animals on silica gel (impregnated with sodium acetate) with butanol - ethanol - water 5:3:2 with chamber saturation. Detection by spraying with diphenylamine - aniline - phosphoric acid in acetone. Quantitative determination by absorbance measurement at 370 nm.
Acta Chimica 110, 197-202 (1982). TLC of ferric-fructose (FeCl3), ferric-fructose (FeNO3), ferric-sorbose (FeCl3 ) on silica with butanol - acetone - HCl - acetylacetone - water 60:40:1:0.5:20. Detection with 10 % sulfuric acid and 2 % K4FeCN9.
nauk. SSSR, serija chimicheskaja 2400-2402 (1983). (Russian) (Synthesis of 3,4-di-o-benzyl-1,2,-o- (1-cyano)-ethylidcine-alpha -D-xylopyranose.) TLC of the title compound on silica with a) ether - benzene 1:1, 1:2; b) chloroform - methanol 93:7. Detection with 25 % sulfuric acid.
J.A.O.A.C. 72, 27,29 (1989). TLC separation of polysorbates (20, 40, 60, 65, 80) on silica with chloroform - methanol - acetic acid - water 68:12:12:3, propanol - chloroform - methanol - NH3 10:10:5:2. Visualization with cobalt thiocyanate reagent.
Var. australis (Diels) Rehd.) (Chinese). Chinese J. Herb Med. (Zhongcaoyao) 24, 563-566(1993). Preparative TLC of saponins and monosaccharides on silica with the lower phases of a) chloroform - methanol - water 16:5:1, and b) a solution of 9 mL of the above mixture blended with 1 mL acetic acid. Detection by spraying with 50% sulfuric acid in methanol for saponins and with naphthyl alcohol - sulfuric acid reagent for saccharides. Identification by MS and NMR.
J. Planar Chromatogr. 18, 285-289 (2005). HPTLC of glucose - after hydrolyis of starch using alpha-amylase and amyloglucosidase - on silica gel, pre-washed with methanol, treated by immersion in a 0.1 M solution of di-potassium hydrogen phosphate in methanol and activated for 30 min at 120 °C. Three-fold development was performed in a horizontal development chamber with acetonitrile - water 17:3. Detection by dipping in aniline-diphenylamine reagent, densitometry at 520 nm. Calibration was linear between 100 and 300 ng with a coefficient of determination r2 of 0.9959. The limits of detection and quantification for starch as glucose were 0.26 and 0.51 g/100 g, respectively.
as a leading compound for quantification in raw material and finished product. J. Liq. Chromatogr. Relat. Technol. 33, 996-1004 (2010). TLC of xylose with acetonitrile - water 9:1 with chamber saturation at ambient temperature. Detection by dipping into 4-aminobenzoic acid reagent for 1 to 2 s followed by heating at 110 °C for 10 min. The hRf of xylose was 56. Quantitative determination by densitometric evaluation at 366 nm. The linearity determination coefficient was r2 = 0.9999. The recovery of xylose was between 102 and 106 %. The precision of a six-time preparation was 1.6 %.