Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. The saved items can be printed to PDF using the print function of your web browser.

      105 021
      Determination of aloe vera gel in cosmetics
      J. GEISSER*, Evamaria KRATZ (*Chemical and Veterinary Investigation Laboratory (CVUA), Weissenburger Str. 3, 76187 Karlsruhe, Germany, Juergen.Geisser@cvuaka.bwl.de)

      CBS 104, 13-15 (2010). HPTLC of aloeverose, glucose and galactose in aloe vera products on silica gel (impregnated with NaH2PO4) with acetone - iso-propanol - 0.1 M formic acid 221 (double development for products with high glucose content). Detection by immersion in 4-aminobenzoic acid reagent (1 g 4-aminobenzoic acid in 36 mL acetic acid, with 40 mL water, 2 mL 85 % phosphoric acid and 120 mL acetone), followed by heating at 100 °C for 10 min. Densitometric evaluation by fluorescence measurement at 366 nm. The limit of quantification was approx. 3 % in aloe vera products. RSD for polynomial calibration is 2.1 % for mannose in the range of 8-80 ng/band and 4.0 % using matrix calibration.

      Keywords: hptlc
      Classification: 10b
      59 051
      Analysis of branched cyclodextrins by high-performance liquid and thin-layer chromatography
      K. KOIZUMI*, T. UTAMURA, T. KUROYANAGI, S. HIZUKURI, J. ABE, Women's Univ., 4-16 Edagawa-cho, Nishinomiya 663, Japan)

      J. Chromatogr. 360, 397-406 (1986). TLC of 6-o-alpha-D-glucosyl-, 6-0-alpha-maltosyl and 6-o-alpha-maltotriosyl derivatives of alpha, beta- and gamma cyclodextrin (CD) and of 6,6'-di-o-alpha-D-glucocyl-beta-CD on 4 kinds of plates with different solvent systems. Chromatography on silica with 1-propanol - ethyl acetate - water, 25 % NH3 3121, on NH2-bonded silica with acetonitrile - water 32, on Si 50000 silica with 1-butanol - pyridine - water 643. TLC is a more convenient method than HPLC for the analysis of CDS.

      Classification: 10b
      98 040
      Direct microextraction and analysis of rough-type lipopolysaccharides by combined thin-layer chromatography and MALDI mass spectrometery
      H. THERISOD, V. LABAS, M. CAROFF* (*Equipe “Endotoxines”, UMR 8619 du Centre National de la Recherche Scientifique, Biochimie, Universitè de Paris-Sud, F-91405 Orsay, France)

      Anal. Chem. 73, 3804-3807 (2001). TLC of lipopolysaccharides from intact bacteria on silica gel with chloroform – methanol – water – triethylamine 12610.04. Detection by spraying with 10 % sulphuric acid in ethanol followed by heating at 150 °C for 5 min. For the non-destructive visualization the plates were pre-washed twice with propanol – water 11 and developed in methanol – water 11 which made the products appear as dull white spots on a bright background. Zones containing lipopolysaccharides or lipid A molecular species were isolated from the plate and analyzed by MALDI mass spectrometery.

      Keywords:
      Classification: 10b
      105 022
      Concise synthesis of the pentasaccharide O-antigen corresponding to the Shiga toxin producing Escherichia coli O171
      P. MANDAL, A. MISRA* (*Division of Molecular Medicine, Bose Institute, A.J.C. Bose Birth Centenary Campus, Kolkata, India, akmisra69@gmail.com)

      Bioorg. Chem. 38, 56-61 (2010). TLC of 4-methoxyphenyl glycoside on silica gel with acetonitrile - methanol - water 421. Detection by spraying with warm 2 % ceric sulphate in 2N sulfuric acid. The hRf of 4-methoxyphenyl glycoside was 30.

      Classification: 10b
      60 059
      Schleimpolysaccharide auf Wollblumen
      R. KLAUS, G. FRANZ

      (Mucopolysaccharides of cotton flowers). Dtsch. Apoth. Ztg. 127, 665-669 (1987). After acidic hydrolysis, TLC on silica with acetonitrile - water 8515. Staining with aniline - diphenylamine - phosphoric acid reagent. The following sugars were identified D-galacturonic acid, D-glucoronic acid, D-galactose, D-glucose, D-mannose, L-arabinose, D-xylose and L-rhamnose.

      Classification: 10b
      105 023
      Transglycosylation properties of maltodextrin glucosidase (MaIZ) from Escherichia coli and its application for synthesis of a nigerose-containing oligosaccharide
      K. SONG, J. SHIM, J. PARK, S. KIM, Y. KIM, W. BOOS, K. PARK* (*Department of Biology, University of Incheon, Incheon, Republic of Korea, parkkh@incheon.ac.kr)

      Biochem. Biophys. Res. Commun. 397, 87-92 (2010). Preparative TLC of the hydrolysis reaction of maltodextrin glycosidase on various substrates (maltotriose, alpha-, beta-, gamma-cyclodextrins and cycloamylose) on silica gel with ethyl acetate - methanol - acetic acid - water 12331. The structure of the products was determined by MALDI-TOF/MS, 13C NMR, and enzymatic analysis.

      Classification: 10b
      61 075
      (Thin-layer chromatography of unsaturated sulfated disaccharides)
      CH. ZHANG (Zhang Chunling), Y. ZHANG, (Zhang Yingshan), (Inst. Cardiovasc. Dis., Chin. Acad. Sci., Beijing, P.R. China)

      (Chinese). Chinese J. Adv.in Biochem.& Biophys. 2, 64-66 (1987) (Shengwu Huaxue Yu Shengwu Wuli Jinzhan). TLC on cellulose with n-butanol - acetic acid - 2M NH4OH 231. Detection under UV at 260 nm. Identification by comparison of Rf values to standards.

      Classification: 10b
      105 024
      Use of HPTLC to differentiate among the crude polysaccharides in six traditional chinese medicines
      C. YANG (Yang Cheng), J. GUAN (Guan Jia), J.-S. ZHANG (Zhang Jiang-sheng), S.-P. LI*(Li Shao-ping) (*Institute of Chinese Medical Sciences, University of Macau, Macau SAR, China; lishaoping@hotmail.com)

      J. Planar Chromatogr. 23, 46-49 (2010). HPTLC of polysaccharides (with galactose, glucose, mannose, arabinose, ribose, xylose, rhamnose, galacturonic acid, and glucuronic acid as standards) before and after hydrolysis on silica gel with chloroform - n-butanol - methanol - water - acetic acid 9251033 with chamber saturation for 30 min at room temperature. Detection by spraying with aniline - diphenylamine - phosphoric acid reagent and heating at 130 °C for 10 min. Quantitative determination by absorbance measurement at 380 nm. Ninhydrin reagent was used for detection of other compounds.

      Classification: 10b