Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      66 005
      Lipophike character of cardiac glycosides
      G.L. BLAGI*, A.M. BARBORO, M.C. GUERRA, P.A. BOREA, M. RECANATINI, (*Inst. Farm., Univ. Bologna, Bologna, Italy)

      RM values as lipophilicity parameters. J. Chromatogr. 504, 163-178 (1990). Measurement of RM values for a series of 41 cardiac glycosides and aglycones. Calculation of the RM values for 19 compounds by means of the D RM values. Discussion of the correlation of the measured RM values with literature-reported values, HPLC data and octanol- water partition coefficients (log p).

      Keywords:
      Classification: 2d, 14
      70 005
      Determination of kinetic parameters for precoated silica gel thin layer chromatography plates by forced flow development
      W.P.N. FERNANDO, C.F. POOLE*, (*Dept. of Chem., Wayne State University, Detroit, MI 48202, USA)

      J. Planar Chromatogr. 4, 278-287 (1991). Identification of the kinetic contributions to band broadening for TLC and HPTLC plates precoated with silica, (and porous particle-loaded membrane sheets (EmporeTM)) from plate height measurements over a wide velocity range using forced flow development. The Foley-Dorsey peak shape model was used to calculate plate height parameters; plate height and velocity data were fitted to the van Demter and Knox equations yielding realistic values for the equation coefficients.

      Keywords:
      Classification: 2d
      74 007
      Determination of lipophilicity by means of reversed-phase thin-layer chromatography II
      G.L. Biagi*, A.M. Barbaro, A. Sapone, M. Recanatini, (*Dip. di Farm., Univ. di Bologna, Via Irnelio 48, 40 126 Bologna, Italy)

      Influence of the organic modifier on the slope of the thin-layer chromatographic equation. J. Chromatogr. 669, 246-253 (1994). Determination of the RM values of a series of steroids. Investigation of the influence of the organic solvent in the mobile phase on the slopes of the TLC equations. Analysis of the equation correlating slopes and intercepts in different solvent systems. Proposal of a TLC method to be considered as a general procedure for the determination of lipophilicity.

      Keywords:
      Classification: 2d, 13
      79 012
      The influence of electric field on chromatographic process in TLC
      I. MALINOWSKA, (Fac. of Chem., M. Curie-Sklodowska Univ., Pl. M. Curie-Sklodowskiej 3, 20-032 Lublin, Poland)

      Proc. 9th Internat. Symp. Instr. Chromatogr., Interlaken, April 9.-11., 179-186 (1997). In chromatographic systems containing weak monocomponent mobile phases and polycyclic hydrocarbons as solutes on silica no differences between retention parameters and analysis time were observed. In the case of aluminium oxide as stationary phase the electric field evidently influenced the chromatographic parameters of non-active solutes and the migration velocity of solvents.

      Keywords:
      Classification: 2d
      85 011
      Effect of thermodynamic quality of the mobile phase on the behavior of macromolecules in adsorption chromatography
      L. LITVINOVA*, N. BEL'NIKEVICH, E. TYIHAK, (*Inst. of Macromolecular Compounds of the Russian Acad. of Sci., Bolshoi pr. 31, 199004 St. Petersburg, Russia)

      J. Planar Chromatogr. 13, 149-151 (2000). TLC of polystyrene of average molecular weights of 117, 240 and 460 kDa on silica gel by one-dimensional single development in an N-type unsaturated chamber with cyclohexane - toluene - methyl ethyl ketone or cyclohexane - toluene. Details and detection as described in J. Planar Chromatogr. 11, 114-118 (1998).

      Keywords:
      Classification: 2d
      94 004
      Densitometric comparison of the performance of Stahl-type and sandwich-type planar chromatographic chambers
      M. SAJEWICZ, A. PIENIAK, R. PIETKA, K. KACZMARSKI, T. KOWALSKA* (*Institute of Chemistry, Silesian University, 9 Szkolna Street, 40-006 Katowice, Poland)

      J. Liq. Chrom. Rel. Technol. 27, 2019-2030 (2004). Comparison of the N-type and S-type chambers in terms of mobile phase flow rate, the Rf values obtained, and the densitometrically established concentration profiles of the test analytes. Selected were several phenyl-substituted alcohols and acids, low activity adsorbents (e. g. cellulose powder), and low-polarity solvents (n-octane and decalin) as the components of the chromatographic systems investigated. The overall conclusion from the results obtained is that the physico-chemical performance of the S-chamber is comparable with that of the N-chamber, and that the only indisputable superiority of the S-chamber is the more economical use of the mobile phase.

      Keywords: densitometry
      Classification: 2d, 2a
      115 008
      Chromatographic-densitometric analysis of chosen fluoroquinolones on TLC plates using mobile phases with different viscosity
      J. KRZEK*, Barbara ZUROMSKA, Urszula HUBICKA, Marta KACZMARSKA (*Department of Inorganic and Analytical Chemistry, Faculty of Pharmacy, Jagiellonian University Medical College, 9 Medyczna Street, 30-688 Kraków, Poland, jankrzek@cm-uj.krakow.pl)

      J. Liq. Chromatogr. Relat. Technol. 38, 1113-1120 (2015). HPTLC of orbifloxacin (1), danofloxacin (2), ciprofloxacin (3), norfloxacin (4), enrofloxacin (5), marbofloxacin (6), difloxacin (7) and ofloxacin (8) on silica gel with 1,4-dioxane - ammonia - tetrahydrofuran 6:3:2. Quantitative determination by absorbance measurement at 320 nm. The hRF value was 19 for (4), 23 for (3), 30 for (2), 37 for (8), 40 for (6), 44 for (5), 56 for (1) and 59 for (7). Linearity was in the range of 159-513 ng/zone for (1), 99-238 ng/zone for (2), 97-244 ng/zone for (3), 69-163 ng/zone for (4), 63-170 ng/zone for (5), 103-250 ng/zone for (6), 84-251 ng/zone for (7) and 94-260 ng/zone for (8). LOD and LOQ were 53 and 159 ng/zone for (1), 32 and 98 ng/zone for (2), 32 and 97 ng/zone for (3), 23 and 69 ng/zone for (4), 21 and 63 ng/zone for (5), 34 and 103 ng/zone for (6), 28 and 84 ng/zone for (7) and 31 and 94 ng/zone for (8), respectively. Selection of appropriate viscosity of the mobile phase may be important in obtaining optimal chromatographic separation.

      Classification: 2e, 32a
      68 181
      An improved densitometric determination of equine estrogens
      J. NOVAKOVIC, J. KUBES, I. NEMEC*, (*Fac. of Natural Sci., Dept. of Anal. Chem., Albertov 2030, 12840 Prague, CSFR)

      J. Planar Chromatogr. 3, 521-526 (1990). HPTLC of estrone, equilin, equilenin and their 17a-diols on silica with cyclohexane - chloroform - methanol - triethylamine 16:18:2:3 and, after drying, chloroform - dioxan - triethylamine 40:3:2 (same direction). Mestranol was used as internal standard and densitometric measurement was made in the reflectance mode at 282 nm. Also study of the relationship between structure and retention.

      Classification: 2e, 32e