Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      96 012
      Comparison of adsorption in liquid-solid chromatography on the basis of different models of retention
      Barbara Oscik-Mendyk (Faculty of Chemistry, M. Curie-Sklodowska University, M. Curie-Sklodowska Sq. 3, 20-031 Lublin, Poland)

      J. Planar Chromatogr. 18, 199-202 (2005). Evaluation of two models of retention in liquid adsorption chromatography. Terms related to adsorption from two equations based on different retention models were compared. The terms were calcutated for selected substances in four chromatographic systems with a different polar modifier. Analysis of the data has proved the comparability of the terms and that they can be used interchangeably to describe adsorption phenomena. TLC of e.g. nitroanilines, nitrotoluidines, nitrophenols on silica gel in horizontal chambers with heptane - ethyl acetate, heptane - 1,4-dioxane, heptane - tetrahydrofuran and heptane - ethylene chloride. Visualization with iodine vapor, detection by scanning.

      Keywords:
      Classification: 2b
      107 022
      Correlation between structure, retention and activity of cholic acid derived cis-trans isomeric bis-steroidal tetraoxanes
      S. SEGAN, F. ANDRIC, A. RADOICIC, D. OPSENICA, B. SOLAJA, M. ZLATOVIC, D. MILOJKOVIC-OPSENICA* (*Institute of Chemistry, Technology, and Metallurgy, University of Belgrade, 11158 Belgrade, Serbia, dusankam@chem.bg.ac.rs)

      J. Sep. Sci. 34, 1-9 (2011). Quantitative structure-retention (QSRR) and quantitative structure-activity relationship (QSAR) studies were performed to correlate the molecular characteristics of seven pairs of cis-trans isomeric bis-steroidal tetraoxanes with their reversed-phase thin-layer chromatography retention and their antiproliferative activity. TLC on 1) RP-18 with mobile phases of 0-14 vol% water in methanol (increment 2 %), 10-30 vol% water in acetone (increment 5 %) and 10-35 vol% water in dioxane (increment 5 %) and on 2) cyano phase with mobile phases of 10-30 vol% water in methanol (increment 5 %), 10-40 vol% water in acetone (increment 5 %). Detection by spraying with sulfuric acid 50 %, followed by heating. In all instances, it was found that the retention of the investigated compounds decreased with increasing concentrations of the organic modifier in the mobile phase.

      Classification: 2c
      114 001
      Lipophilicity study of salicylic and acetylsalicylic acids
      using both experimental and calculations methods
      M. DOLOWY, Alina PYKA (*Department of Analytical Chemistry, Faculty of Pharmacy, Medical University of Silesia in Katowice, 4 Jagiellonska Street, PL-41-200 Sosnowiec,
      Poland, apyka@sum.edu.pl)

      J. Liq. Chrom. Rel. Tech. 38, 485-491 (2015). HPTLC of (1) salicylic acid and (2) acetylsalicylic acid on RP-18W with mixtures of methanol and water of pH 2.6; the content of methanol in the mobile phase was gradually varied by 10 % from 20–100 % (v/v). The method allowed the estimation of the lipophilicity of (1) and (2).

      Classification: 2c
      117 019
      Optimization of the thin-layer chromatography method for the separation of ziprasidone and its impurities
      D. OBRADOVIC, S. FILIPIC*, K. NIKOLIC, D. AGBABA (*Department of Pharmaceutical
      Chemistry, Faculty of Pharmacy, University of Belgrade, Vojvode Stepe 450, Belgrade, Serbia, sfilipic@pharmacy.bg.ac.rs)

      J. Planar Chromatogr. 29, 239-246 (2016). HPTLC of ziprasidone and its 5 impurities on silica gel with toluene – methanol – glacial acetic acid 15:1:1. Qualitative analysis by absorbance measurement at 250 and 320 nm. The hRF values of ziprasidone and its impurities were 19, 11, 16, 7, 41 and 33, respectively. The retention behavior of ziprasidone and its five impurities was investigated by employing the experimental design and quantitative structure–retention relationship. See also J. Liq. Chromatogr. Relat. Technol. 39, 271-276 (2016).

      Classification: 2c
      121 015
      Reversed-phase and normal-phase thin-layer chromatography and their application to the lipophilicity prediction of synthetic pyrethroids based on quantitative structure–retention relationships
      J. NOWAKOWSKA, K. CIURA*, P. KAWCZAK, B. WIELGOMAS, T. BACZEK (*Department of Physical Chemistry, Medical University of Gda?sk, Faculty of Pharmacy, Al. Gen. J. Hallera 107, 80-416 Gda?sk, Poland, krzesimir.ciura@gmail.com)

      J. Planar Chromatogr. 31, 99-104 (2018). HPTLC of synthetic pyrethroids (allethrin, cyfluthrin, cyhalothrin, cypermethrin, deltamethrin, fenvalerate, and permethrin) on silica gel and RP-18 with the following systems: a) RP-TLC with acetone – water in the ratio of 20 % to 80 %, acetonitrile – water 50 % to 100 %, tetrahydrofuran – water 50 % to 100 %; b) NP-TLC with acetone – petroleum ether 20 % to 100 %, tetrahydrofuran – petroleum ether 20 % to 80 %, and acetonitrile – petroleum ether 0 % to 100 % (v/v). The best chromatographic system to predict log P is RP-TLC and a mixture of tetrahydrofuran and water.

      Classification: 2c
      56 108
      High-performance thin-layer chromatography of metal complexes of meso-tetrakis (p-tolyl) porphyrin on cellulose and silica gel
      M. KOBAYASHI, K. SAITOH, N. SUZUKI

      Chromatographia 18, 441-444 (1984). Studies on the migration behaviour of metal complexes of meso-tetrakis (p-tolyl) porphyrin in HPTLC systems with cellulose and silica gel and various solvents of relatively low polarity. TLC on silica with a carbon disulfide - m-xylene mixture is recommended for the separation of the complexes.

      Keywords:
      Classification: 2c, 23a
      58 017
      Chromatographic behaviour of diastereoisomers, VIII) Solvent selectivity effects in separation on silica
      L.R. SNYDER, M. PALAMARERA, B. KURTEV, L. VITEVA, J. STEFANOVSTY

      J. Chromatogr. 354, 107-118 (1986). TLC of 20 diastereoisomeric compounds on silica with 46 different mobile phases. Detection by spraying with iodine - ether solution.

      Keywords:
      Classification: 2c
      63 005
      Relationships between retention behavior and structure of N-substituted 1,2,4-triazoles in thin-layer chromatography on silica gel
      TH. JAQUES, (Lab. Chim., Fac. Sci. Tech., 37200 Tours, France)

      J. Chromatogr. 404, 73-85 (1987). Study of the relationships between the structure of NC1)- or NC4)-substituted 1,2,4-triazoles and their TLC behavior on silica. Linear correlations between RM and the logarithm of the molar fraction of strong solvent in 8 binary solvent systems for 5 pairs of positional isomers. Relationship between the retention order and the adsorption mechanisms of the molecules and the alkalinities of the triazole nuclei.

      Keywords:
      Classification: 2c, 23