Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      96 021
      Coupling development and elution, a new thin-layer chromatography technique J
      J. HAN (Han Jing), D. WANG (Wang Dongyuan)*, D. WANG (Wang Dan), Y. WANG (Wang Yuping), M. ZHOU (Zhou Mi), L. LI (Li Ledao), H. ZHANG (Zhang Hongxia) (*Department of Analytical Chemistry, Shenyang Pharmaceutical University, 103 Wenhua Road, Shenyang 110016, China)

      Chromatogr. A 1002 (1-2), 213-219 (2003). Three methods of coupling development and elution were studied in this paper. (1) A new mode of solvent supplementation and eluate collection was developed for descending development. By using a new distributor and collector in descending development, components can be separated and eluted continuously. (2) The same effect can be realized with a slope distributor [Su et al., J. Planar Chromatogr. 14 (2001) 203] and a collector by horizontal development. (3) In-situ elution can be used to treat a developed silica plate, which can elute the separated components to the receptor without scraping them off. These three methods can be used individually, and the in-situ elution can be used with other modes of development.

      Keywords:
      Classification: 3g
      51 011
      Two phase, two-dimensional TLC for fingerprinting and confirmation procedures
      T.E. BEESLEY, E. HEILWEIL

      J. Liquid Chrom. 5, 1555-1566 (1982). Two-dimensional TLC on a special plate with two layers (silica and RP-18) of A) morphine with1) methanol - 0.5M NaCl 65:35, 65 °C for 20 minutes, 2) ethyl acetate - methanol - water - 28 % NH3, 170:27:2:1; B) lubricating oil with 1) acetonitrile-water - acetic acid 90:10:1, 2) hexane - chloroform 8:20. Detection of A) with methanolic iodoplatinate reagent and of B) with 5 % phosphomolybdic acid and heating for 5 minutes at 120°C.

      Keywords:
      Classification: 3
      53 011
      Use of various organic modifiers in thin-layer chromatography on chemically bonded phases
      U. BRINKMANN, G. DE TRIES

      J. Chromatogr. 265, 105-110 (1983). Use of various organic modifiers: acetone, dioxane, isopropanol and THF, in thin-layer chromatography on chemically bonded phases. Two classes of compounds have been studied: phthalate esters and isomeric aminophenols. TLC of phthalate esters/isomeric aminophenols on RP-plates with a) acetone - water, b) dioxane-water, c) isopropanol - water, d) THF-water, all with or without 3 % of sodium chloride. Detection by UV 254 nm.

      Keywords:
      Classification: 3
      54 020
      Determination of the lipophilicity of some aniline derivatives by reversed phase thin-layer chromatography
      R. CSERHATI

      Chromatographia 18, 318-322 (1984). The lipophilicity of aniline and 36 ring-substituted aniline derivatives was determined by reversed-phase thin-layer chromatography using methanol, acetone and acetonitrile as the organic phase. Reversed-phase TLC of aniline derivatives on silica, impregnated with 5 % solution of paraffin in hexane, with methanol, acetone, acetonitrile in varying proportions. Detection by UV.

      Keywords:
      Classification: 3
      79 034
      Duennschicht-Chromatographie aktuell
      W. FISCHER, H.E. HAUCK, G. WIELAND, (Merck KGaA, Anal. Chromatogr., 64271 Darmstadt, Germany)

      (Current Thin-Layer Chromatography). LABO June 1997, 56-62 (1997). Short overview of advantages of TLC; i.e. simultaneous determination of more than 70 single substances within 30 min on a single plate; determination of up to 30 single substances per sample using Automated Multiple Development (AMD) techniques; TLC as general method for High Throughput Screening (HTS): more than 1000 samples per day per person; description of plates with spherical particles - available since 1997: developing time shorter by 20%, more compact spots with smaller diameter, therefore lower detection limits, order of elution unchanged.

      Keywords:
      Classification: 3
      58 035
      Sample collection, quantification and identification in preparative anticircular planar chromatography
      A. STUDER, H. TRAITLER

      J. High Resol. Chromatogr. 9, 218-223 (1986). Description of a preparative anticircular chromatography (PACH) apparatus including sampling device; evaluation of sample collection techniques, quantification and evaluation of consistency by UV/VIS scanning after spot-visualization as well as application examples.

      Keywords: preparative TLC
      Classification: 3a
      97 009
      HPTLC method development for pharmacokinetic study of sparfloxacin in plasma
      R. SHAH*, B. SUHAGIA, I. RATHOD, S. SHAH, D. PATEL (*L.M.College of Pharmacy, Ahmedabad-380009, India)

      Indian J. Pharm Sciences 67 (6), 687-690 (2005). HPTLC of sparfloxacin extracted with dichloromethane from plasma. A standard solution was prepared in methanol - dichloromethane 1:1. HPTLC on silica gel with chloroform - toluene - methanol - diethylamine 44:15:2:1. Quantitative determination by absorbance measurement at 301 nm. The method had a linearity range of 80-200 ng/spot with an average recovery of 89.17 %.

      Classification: 3a
      111 011
      Introduction of special HPTLC and TLC plates for coupling with mass spectrometry
      M. SCHULZ*, B. SCHUBACH, Susanne MINARIK, H. GRIESINGER (*Merck KGaA, MM-LER-CP. Frankfurterstr. 250, 64293 Darmstadt, Germany, michael.schulz@merckgroup.com)

      CBS 110, 10-11 (2013). New HPTLC silica gel plates specially suited for coupling with MS and TLC plates for coupling with NMR. These MS-grade HPTLC plates are low in impurities and show less background noise, the layer thickness is 100 µm. HPTLC of human insulin and its secondary components on MS-grade silica gel with 2-butanol - pyridine - ammonia 25 % - water 39:34:10:26, detection under UV 366 nm after treatment with fluorescamine and by elution with the TLC-MS Interface and Q-TOF MS analysis in ESI positive mode, the eluent was acetonitrile - water 19:1. Separation and identification of insulin and desamido insulin was achieved, even though there is only 1 Da mass difference.

      Keywords: HPTLC
      Classification: 3b, 19