Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      73 172
      (Separation and identification of dyes in municipal wastewater
      SH. DAI* (Dai Shuhui), D. YOU (You Daoxin), M. BAO (Bao Mingliag), X. LI (Li Xiaoxin), G. LEI (Lei Gongmin), H. XIE (Xie Huasheng), T. SHONG (Shong Tiedong), (*Dept. Environ. Sci., Nakai Univ., Tianjin 30007u1, P.R. China)

      Chinese J. Environ. Chem. (Huanjing Huaxue) 12, 225-230 (1993). TLC of 7 dyes on silica with 14 different solvent systems (two for each dye). Identification by comparison colors and Rf values with those of standards. Confirmation and quantification by HPLC.

      Classification: 30a, 37c
      85 092
      OPLC analysis of food dyestuffs
      J.K. ROZYLO, R. SIEMBIDA, (Maria Curie-Sklodowska University, Fac. of Chem., Maria Curie-Sklodowska Sq. 3, 20031 Lublin, Poland)

      Chem. Environ. Res. 6, 49-55 (1997). OPLC of quinoline yellow (E104), sunset yellow (E110), cochineal red A (E124), indigo carmine (E132), tartrazine (E102), amaranth (E123), erythrozine (E127) on silica gel with NH3 - methanol - ethyl acetate 1:3:6 and NH3 - MEK - n-butanol 2:3:5 to 80 mm. Limits of detection are below 0,5 µg. E127 migrates in both solvent systems into the demixing zone. Thus, it could not be determined quantitatively. Significantly decrease in time of chromatographic analysis as compared to conventional TLC.

      Keywords:
      Classification: 30a
      105 050
      Validation of NP-HPTLC and RP-HPTLC methods with videodensitometric detection for analysis of ziprasidone in pharmaceutical formulations
      R. SKIBINSKI*, L. KOMSTA (*Department of Medicinal Chemistry, Medical University of Lublin, Jaczewskiego 4, 20-090 Lublin, Poland, robert.skibinski@am.lublin.pl)

      J. Planar Chromatogr. 23, 23-27 (2010). HPTLC of ziprasidone (5-[2-[4-(1,2-benzothiazol-3-yl)piperazin-1-yl]ethyl]-6-chloro-1,3-dihydroindol-2-one) on silica gel with hexane - dioxane - propylamine 5:45:2 up to 9 cm (under saturated conditions) and on RP8 with tetrahydrofuran - phosphate buffer (pH 9.0) 1:1 up to 4.5 cm (under unsaturated conditions), both in horizontal chambers. Quantitative determination by videodensitometry at 254 nm. Calibration was linear in the range 0.2-1.2 and 0.1-1.1 µg/spot ziprasidone for NP-HPTLC and RP-HPTLC, respectively. The intra-day precisions for 0.4-1.2 µg/spot on NP-HPTLC was 2.0 to 5.2 % and on RP-HPTLC 4.0 to 6.1 %; the respective inter-day precision for NP-HPTLC was 2.0 to 6.7 % and for RP-HPTLC 4.1 to 7.1 %. LOD/LOQ on NP-HPTLC was 0.03/0.09 µg/spot; using RP-HPTLC, LOD/LOQ was 0.02/0.06 µg/spot. The specificity of the methods was confirmed by comparison of hRf values (74 +/- 2 in NP-HPTLC and 36 +/- 1 in RP-HPTLC, n=12).

      Classification: 30a
      117 107
      Quantification of synthetic amino-nitroquinoxaline dyes – an approach using image analysis
      L. DA SILVA, D. DE LIMA, J. SILVA, C. DE MORAIS, B. ALBUQUERQUE, A. BORTOLUZZI, J. DOMINGOS, R. ARAUJO, F. MENEZES, K. LIMA* (*Biological Chemistry Research Group, Institute of Chemistry, Federal University of Rio Grande do Norte, Natal-RN, Brazil, kassiolima@gmail.com)

      J. Braz. Chem. Soc. 27, 1067-1077 (2016). HPTLC for the kinetic study involving the conversion of 2,3-dichloro-6,7-dinitroquinoxaline (1) into 2-chloro-6,7-dinitro-3-pyrrolidinoquinoxaline (2) and then into 6,7-dinitro-2,3-dipyrrolidinoquinoxaline (3) on silica gel through monosubstitution of a chlorine group with one equivalent of pyrrolidine. First, for obtaining calibration sets, 1 μL of solutions containing compounds (2) and (3) in chloroform with concentrations ranging from 1.0 to 8.0 mM were applied separately on chromatographic plates. In the kinetic study, 100 μL of a solution of compound (1) in chloroform (0.32 M) was added to 100 μL of pyrrolidine in chloroform (1 M eq). 10 μL of the reaction media taken at different times (30, 60, 90, 120, 180, 240, 300, 600, 1200 and 1800 s) was applied onto the TLC layer and separated with chloroform. All the final chromatograms were directly scanned to generate their digital image. Detection by absorbance measurement at 411 nm for (2) and 331 nm for (3). Kinetics profile was constructed for reagent (2) consumption and product (3) formation.

      Classification: 30a
      57 028
      A new chromatographic method for the separation of food dye mixtures on thin MgO layers
      J. MASTOWSKA

      Chromatographia 20, 99-101 (1985). TLC of food dyes, indigo carmin, cochineal red, acid amaranth I, orange yellow S and tartrazine G on thin MgO layers with mixtures of 15 % sodium citrate and methanol in proportions from 9:1 to 1:9. The best proportion of the developing solvent mixture was 6:2. It permits the full separation of the dye mixture from a 0.3 mL sample solution with concentrations of 1 x 10 to minus 6 mole/liter.

      Classification: 3b, 30a
      65 145
      (Analysis of hydrolysates of vinyl sulfone reactive dyes by thin-layer chromatography
      G. LI( Li Guizheng), Y. LE (Le Yiming), ZH. ZHU (Zhu Zhenghua), Y. LIU (Liu Yinyi), (East China Inst. Chem. Technol., Shanghai, P.R. China)

      Chinese J. Chromatogr. 7, 285-288 (1989). TLC of vinyl sulfone reactive dyes on silica with chloroform - methanol - acetone 18:3:2. Detection by densitometry. Detection limit 10 ng. Measurement and discussion of the reaction rate constant of hydrolysis of 10 dyes having different constitutions.

      Classification: 30a
      74 104
      Identification of unlawful food dyes by thin-layer chromatography - fast atom bombardment mass spectrometry
      H. OKA*, Y. IKAI, T. OHNO, N. KAWAMURA, J. HAYAKAWA, K. HARADA, M. SUZUKI, (*Aichi Prefect. Inst. Public Health, Tsuji-machi, Kita-ku, Nagoya 462, Japan)

      J. Chromatogr. 674, 301-307 (1994). Identification of the 27 food dyes by TLC on RP-18 with methanol - acetonitrile - 5% aqueous sodium sulfate 1:1:1. Description of a focusing technique for concentrating of diffuse sample spots on the plate. FAB-MS detection in a matrix 1,4-dithiothreitol-1,4-dithioerythritol 3:1.

      Classification: 4e, 30a
      88 071
      HPTLC separation and determination of banned amine isomers, with reference to the German ban on azo dyes
      M.S. NARVEKAR, A.K. SRIVASTAVA*, (*Dept. of Chem., Univ. of Mumbay, Vidyanagari, Santacruz (E), Mumbai 400 098, India)

      J. Planar Chromatogr. 14, 360-363 (2001). HPTLC of 7 amines (p-chloroaniline, o-toluidine, o-anisidine, 2-naphthylamine, 4-chloro-o-toluidine, 2-diaminotoluene, 2-aminio-4-nitrotoluene) on silica gel plates with dichloromethane (developing distance 4.5 cm), drying and development with toluene - tetrahydrofuran 10:1 to a distance of 8.5 cm. Visualization under UV 254 nm. New quantitative very simple, accurate, low-cost, rapid and highly selective method.

      Keywords:
      Classification: 17a, 30a