Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      89 025
      Isolation of flavonoid aglycones from propolis by a column chromatography method and their identification by GC-MS and TLC methods
      W. MACIEJEWICZ, (Dept. of Inorg. and Anal. Chem., Med. Univ., Staszica 6, 20-081 Lublin, Poland)

      J. Liq. Chrom. & Rel. Technol. 24, 1171-1179 (2001). TLC of genkwanin, tectochrysin, galangin, apigenin, pilloin, chrysin, kaempferol, pinocembrin, 5-hydroxy-4',7-dimethoxyflavone, and pinostrobin chalcone on silica gel with hexane - dichloromethane and dichloromethane - ethyl acetate in different proportions. Visualization under UV 254 and 366 nm and in day light after spraying with 1% methanolic iron(III) chloride solution or 1% methanolic aluminium chloride solution.

      Keywords:
      Classification: 8a
      92 028
      Separation of some flavonoids by use of the Prisma model and forced-flow planar techniques
      I. MALINOWSKA, M. KRAUZE-BARANOWSKA*, (*Dept. of Pharmacogn., Med. Univ. of Gdansk, Gen. J. Hallera str. 107, 80-416-Gdansk, Poland)

      Proc. Intern. Symp. on Planar Separations Plan. Chrom. 305-307 (2003). TLC of flavonoids (7-O-glucoside luteolin, 7-O-glucoside apigenine, 5'-O-glucoside tricetin, 3-O-rhamnoside quercetin, 3-O-rhamnoside kaempferol, luteolin, quercetin, kaempferol, isoginkgetin, ginkgetin) on silica gel in a sandwich chamber, in a Personal OPLC chamber, and by planar electrochromatography method with 11 monocomponent, 8 binary phases in different concentration, and ternary and quaternary mobile phases. The best separation of flavonoids, biflavones, aglycones, glycosides was obtained with ethanol - ethyl acetate -dioxane - hexane (as solvent strength modifier).

      Keywords:
      Classification: 8a
      96 031
      Use of reversed-phase and normal-phase preparative thin-layer chromatography for isolation and purification of coumarins from Peucedanum tauricum Bieb
      Magdalena Bartnik*, K. Glowniak, A. Maciag, M. Hajnos (*Department of Pharmacognosy with Medicinal Plant Laboratory, Skubiszewski Medical University, Chodzki 1, 20-093 Lublin, Poland)

      leaves. J. Planar Chromatogr. 18, 244-248 (2005). Analytical and preparative TLC of coumarins from Peucedanum tauricum with bergapten, scopoletin, and coumarin A and B as standards on silica gel and on RP-2 with water - methanol 3:2 in horizontal chambers. Detection under UV light at 366 nm and densitometry at UV 366 and 320 nm. Re-chromatography with more selective mixtures of dichloromethane and acetonitrile 99:1 and 39:1. Identification by analytical co-chromatography with standards using mixtures of cyclohexane - ethyl acetate 3:1 and dichloromethane - acetonitrile 39:1.

      Keywords: herbal densitometry
      Classification: 8a
      100 023
      Densitometric determination of flavonoids in methanolic and aqueous extracts of Epilobii angustifolii herba by use of HPTLC
      Agnieszka BAZYLKO*, A.K. KISS, J. KOWALSKI (*Department of Pharmacognosy, Faculty of Pharmacy, Medical University of Warsaw, 1 Banach Street, 02-097 Warsaw, Poland; oklyzab@farm.amwaw.edu.pl)

      J. Planar Chromatogr. 20, 53-56 (2007). HPTLC of flavonoids (quercetin glucuronide, hyperoside, isoquercitrin, quercetin galloyl galactoside, quercitrin) on silica gel with ethyl acetate - formic acid - water 136:5:6 in a horizontal chamber. Densitometric quantitfication of flavonoids at 350 nm.

      Classification: 8a
      109 025
      Standardization of ashokarista formulation by TLC method
      S. PARIHAR, S.MISRA, H. SINGH, A. RATHORE* (*NRI Institute of Pharmaceutical Sciences, 3 Sajjansingh Nagar, Raisen Road, Bhopal,(M.P.), Bhopal, India, pariharsandeep85@gmail.com)

      International Journal of PharmTech Research 2(2), 1427-1430 (2010). Ashokarista formulations contain ashoka (Saraca indica) as the main ingredient. Its markers are catechin, (+)catechole, and (-)epicatechin. TLC of extracts and (+)catechin on silica gel with toluene - ethyl acetate - formic acid - methanol 15:15:4:0.1. Quantitative determination by densitometry in absorbance mode at 278 nm. For identification of the stem-bark of Saraca indica the fingerprint is evaluated after detection with anisaldehyde-sulphuric acid. The hRf value of (+)catechin was 54.

      Classification: 8a
      114 023
      HPTLC screening of taro hybrids (Colocasia esculenta (L
      V. LEBOT*, L. LEGENDRE (*CIRAD-AGAP, P.O. Box 946, Port-Vila, Vanuatu, lebot@vanuatu.com.vu)

      Plant Breeding 134, 129-134 (2015). HPTLC screening of flavonoids in more than 1800 taro hybrids (Colocasia esculenta (L.) Schott) on silica gel with ethyl acetate - methanol - acetic acid - formic acid - water 30:1:2:1:3. Detection by heating at 100 °C for 3 min, followed by dipping with natural product reagent. Qualitative determination by absorbance at 366 nm. Scoring of the absence and presence of a selection of 8 zones for each track followed by statistical retreatment permitted to sort samples per family. This method contributed to taro genetic improvement.

      Classification: 8a
      115 035
      Adulteration in commercial buchu dietary supplements
      V. RAMAN*, S. SAGI, A. GALAL, B. AVULA, A. VILJOEN, I. KHAN (*National Center for Natural Products Research, School of Pharmacy, University of Mississippi, University, MS 38677, USA, vraman@olemiss.edu)

      S. Afr. J. Bot. 100, 122-131 (2015). HPTLC fingerprint of Agathosma betulina and Agathosma crenulata on silica gel with toluene - ethyl acetate - methanol - acetonitrile - formic acid 10:3:3:2:2. Qualitative identification at UV 366 nm. The hRF values of rutin, chlorogenic acid and kaempferol were 15, 25 and 65.

      Classification: 8a
      118 034
      High-performance thin-layer chromatographic analysis for the simultaneous quantification of lupeol and ursolic acid in the methanolic fraction of four different species of Bauhinia
      A. GUPTA, S. VERMA, A.K.S. RAWAT*, H. DWIVEDI (*Pharmacognosy and Ethnopharmacology Division, CSIR-National Botanical Research Institute, Lucknow, India, rawataks@rediffmail.com)

      J. Planar Chromatogr. 29, 423-428 (2016). HPTLC of lupeol (1) and ursolic acid (2) in the leaves of Bauhinia purpurea L., Bauhinia variegata L., Bauhinia acuminata L., and Bauhinia tomentosa L. on silica gel with toluene – ethyl acetate – formic acid 80:20:1. Detection by dipping into anisaldehyde – sulfuric acid reagent followed by heating at 40 °C for 3 min. Quantitative determination by absorbance measurement at 550 nm for (1) and 522 nm for (2). The hRF values for (1) and (2) were 46 and 68, respectively. Linearity was between 100 and 600 ng/zone for (1) and (2). The intermediate precisions were below 1.5 % (n=3). The LODs and LOQs were 40 and 100 ng/zone for (1) and 35 and 100 ng for (2). Recoveries were between 97.1 and 100.0 % for (1) and 98.0 and 99.2 % for (2).

      Classification: 8a