Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
- Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
- Keyword register: select an initial character and browse associated keywords
- Search by CBS edition: Select a CBS edition and find all related publications
Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.
Biomed. Chromatogr. 11, 280-285 (1997). Discussion of impregnation of methods of impregnation of thin-layer materials with a variety of reagents and the role of impregnating reagents in resolving compounds on the layers with special reference to main/basic approaches of impregnation as applied to direct enantiomeric resolution. Discussion of advantages of TLC over other chromatographic methods in efficiency and quantitation. TLC may serve as method for daily routine process in various laboratories to determine enantiomeric purity with a great ease and speed, and serve as pilot methods for large scale separation of therapeutics etc.
J. Chromatogr. B 737 (1/2), 71-77 (2000). Description of a fast and effective three-step purification procedure for a fragment of FKBP52, consisting of affinity chromatography, anion-exchange and gel-permeation chromatography. Verification of the purity of the products by SDS-PAGE.
J. Planar Chromatogr. 19, 278-281 (2006). Discussion of the deviation from the strict vertical of the migration tracks of chiral compounds during TLC on silica gel. Focus is put on possible crystalline asymmetry of the silica gel used in TLC. Description of an attempt to verify the hypothesis by means of circular dichroism spectroscopy. TLC of S-(+)-ibuprofen and S-(+)-naproxen on silica gel with acetonitrile - methanol - water 5:1:1 for S-(+)-ibuprofen and 10:2:3 for S-(+)-naproxen. Quantitative determination by absorbance measurement at 210 nm.
J. Planar Chromatogr. 21, 129-134 (2008). TLC of racemic metoprolol, propranolol, carvedilol, bisoprolol, salbutamol, and labetalol on silica gel impregnated with optically pure L-Glu with acetonitrile - methanol - water - dichloromethane 10:3:1:2 or 10:3:3:2 (for propanolol), and on silica gel impregnated with L-Asp, with acetonitrile - methanol - water - dichloromethane 5:3:1:3, or acetonitrile - methanol - water - glacial acetic acid 50:10:5:7. Detection with iodine vapor; the detection limits were 0.23, 0.1, 0.27, 0.25, 0.2, and 0.2 µg for each enantiomer, respectively.
J. Chromatogr. A 1218 (19), 2737-2744 (2011). Investigation of new cellulose tribenzoate/gypsum layers in the ratio up to 8:1 (w/w) for the chiral resolution of closely related aromatic ketones (e.g. tetralones and indanones), alcohols (e.g. benzhydrols) and racemates or enantiomers of other compound classes (e.g. dinitrophenyl amino acids). 16 racemates were baseline or partially resolved by eluting with methanol or 2-propanol/water mixtures on 4:1 (w/w) layers among 22 investigated compounds. The study provided better understanding of the retention and resolution mechanisms on this chiral stationary phase, however, some results were unexpected and confirmed the complexity of enantioseparation mechanisms. Evidence from experimental tests is necessary. Quantification of the investigated compounds by densitometry in the visible region of cellulose tribenzoate/gypsum plates after their exposure to iodine vapours.
J. Planar Chromatogr. 29, 184-189 (2016). HPTLC of (±)-etodolac mixed with L-Trp 1:1 as chiral inducing reagent on silica gel with acetonitrile – dichloromethane – methanol 3:1:2. Detection by using iodine vapor. The hRF values for (-)- and (+)-etodolac were 33 and 62, respectively.
J. Chromatogr. 452, 323-330 (1988). Evaluation of the use of partially substituted hydroxypropyl-ß-cyclodextrin and hydroxyethyl-ß-cyclodextrin as chiral mobile phase additives for TLC resolution of racemic benzyl-z-oxazolidinone, 5-(4-methyl-phenyl)-5- phenylhydantoin, mephenytoin and several dansyl and ß-naphtylamide amino acids and diastereomeric compounds including steroid epimers and alkaloids.
Chromatogr. Sci. 55, 541-591 (1991). A review with 146 references on the versatile applicability and separation mechanisms of TLC for the separation of enantiomers. The summary contains Rf values and separation conditions for numerous classes of racemic compounds.