Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      62 097
      Reversed-phase thin-layer chromatography of the ecdysteroids
      I.D. WILSON, (Dep. Chem., Univ. Keele, Staffordshire ST5 5BG, GB)

      J. Planar Chromatogr. 1, 116-122 (1988). Reversed- phase TLC of 23 ecdysteroids on 3 different types of octadecyl-bonded silica and on a cyanopropyl bonded silica with methanol - water based solvent systems. Discussion of the differences in chromatographic selectivity between the various TLC plate types and the effect of various functional groups on the chromatographic properties of the ecdysteroids.

      Keywords:
      Classification: 13e
      92 001
      Thin-layer chromatography of phytoecdysteroids
      M. BATHORI*, H. KALASZ, G. JANICSAK, Z. PONGRACZ, J. VAMOS, (*Dept. of Pharmacogn., Univ. of Szeged, Eötvös utca 6, H-6720 Szeged, Hungary)

      J. Liq. Chrom. & Rel. Technol. 26, 2629-2649 (2003). Review of planar chromatography of ecdysteroids. Separation of various ecdysteroids is detailed using both straight-phase and reversed-phase thin-layer chromatography. The generally used special techniques, such as two-dimensional TLC, forced-flow TLC, displacement mode of development, etc., are also specified. The particular behavior of certain ecdysteroids is discussed. Materials and methods frequently used for ecdysteroid separation are described like e.g. stationary phases, mobile phases, detection methods, screening and identification of plant ecdysteroids, analysis of 20-hydroxyecdysone through the vegetation of plants, lipophilicity of ecdysteroids, analysis of ecdysteroids on RP-TLC plates, FF-TLC, AMD, 2D-TLC, displacement TLC, and hyphenated techniques.

      Keywords:
      Classification: 1, 13e
      63 057
      Thin-layer chromatography of ecdysteroids originated from silene otites L
      M. BATHORI*, K. SZENDREI, H. KALASZ, R. LAFONT, J.P. GIRAULT, (*Dep. Pharm., A. Szent-Györgyi Med. Univ., Szeged, Hungary)

      (Wib.). Chromatographia 25, 627-630 (1988). TLC on silica with ethyl acetate - methanol - NH3 85:10:5. Detection under UV 254 nm; densitometry. TLC method used for monitoring the isolation of ecdysteroids by CC and droplet countercurrent chromatography (DCCC) and for controlling the homogeneity of pure products.

      Keywords: densitometry
      Classification: 13e
      95 026
      TLC of ecdysteroids with four mobile phases and three stationary phases
      Mária BÁTHORI*, A. HUNYADI, G. JANICSÁK, I. MÁTHÉ (*Department of Pharmacognosy, University of Szeged, Szeged, Eötvös u. 6, H-6720 Hungary)

      J. Planar Chromatogr. 17, 335-341 (2004). TLC and HPTLC of 29 ecdysteroids (e. g. 20-hydroxyecdysone, polypodine B, 2-deoxyintegristerone, ajugasterone C, isovitexirone, muristerone A, turkesterone, makisterone C, rubrosterone, poststerone, ecdysone, herkesterone) on silica gel, RP-18, and cyano phase with four mobile phases enabling separation of all the ecdysteroids from each other in at least one system. Detection under UV light at 254 nm or by use of vanillin-sulfuric acid spray reagent. After spraying the spots were either observed in daylight or at 366 nm. Quantitative determination by reflectance-absorbance measurement at 254 nm.

      Classification: 13e
      63 061
      Thin-layer chromatography of ecdysone acyl esters and their 2,3-acetonide derivatives
      L. DINAN, (Dep. Biolog. Sci., Univ. Exeter, Perry Road, Exeter, Devon EX4 4QG, UK)

      J. Chromatogr. 411, 379-392 (1987): TLC of ecdysone 22-acyl esters on silica and ethyl-, octyl-, octadecyl- and cyano-bonded silica with solvent systems of different polarity. Detection by fluorescence quenching under UV 254 nm and by spraying with vanillin - sulfuric acid and heating at 110°C for 5 min. Evaluation of various types of TLC systems. Radioscanning.

      Keywords:
      Classification: 13e
      99 026
      Role of preparative rotation planar chromatography in the isolation of ecdysteroids
      H. KALÁSZ, E. LIKTOR-BUSA, G. JANICSÁK, Mária BÁTHORI* (*Department of Pharmacognosy, University of Szeged, Eotovs utca 6, H-6720 Szeged, Hungary; bathori@pharm.u-szeged.hu)

      J. Liq. Chromatogr. & Relat. Technol. 29, 2095-2109 (2006). Analytical and preparative TLC of ecdysteroids (e. g. dacryhainansterone, 20-hydroxy-ecdysone) on silica gel in unsaturated glass chambers with dichloromethane - methanol - benzene 25:5:3 and ethyl acetate - 96% ethanol - water 16:2:1. Detection under UV 254 nm or by spraying with vanillin-sulfuric acid reagent, followed by detection under white light and under UV 366 nm. Densitometric absorbance measurement at 254 nm.

      Classification: 13e
      63 065
      Comparison of non-hydrophobic C18-bonded thin-layer and for high-performace thin-layer chromatography plates for reversed-phase thin-layer chromatography of ecdysteroids
      I.D. WILSON, (Dep. Chem., Univ. Keele, Keele, Staffordshire STS 5BG, UK)

      J. Chromatogr. 438, 419-422 (1988).Reversed-phase and normal phase HPTLC of a number of ecdysteroids on octadecyl-bonded silica and silica with methanol - water systems. Detection by fluorescence quenching under UV 254 nm. Discussion of the effects of varying the water content on Rf values of ecdysone and 20-hydroxyecdysone on both layers.

      Keywords: HPTLC
      Classification: 13e
      64 092
      Steroidhormon- Derivate
      P. PACHALY, (Pharm. Inst. der Univ., Kreuzbergweg 26, D-5300 Bonn 1, FRG)

      Cortison, Cortisonacetat, Dexamethason (Betamethason), Hydrocortison, Hydrocortisonacetat, Prednison, Prednisolon, Testosteronpropinat, Triamcinolon, Triamcinolonacetonid. Steroidhormone derivatives. Cortisone, cortisone acetate, dexamethasone (betamethasone), hydrocortisone, hydrocortisone acetate, prednisone, prednisolone, testosterone propionate, triamcinolone, triamcinolone acetonide.) (German). Deutsche Apotheker Zeitung 129, 1538-1539 (1989). TLC purification of steroidhormone derivatives on silica with dichloromethane - acetone 75:25. Detection under UV 254 nm or by spraying with 20% sulfuric acid in ethanol followed by heating at 110°C for 10 min.

      Classification: 13e