Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

      131 077
      In-process quality control of wine by planar chromatography versus micro planar chomatography
      S. KIRCHERT, R. KAISER, Gertrud MORLOCK* (*Institute of Nutritional Science, Chair of Food Science, and Interdisciplinary Research Center, Justus Liebig University Giessen, 35392 Giessen, Germany, gertrud.morlock@uni-giessen.de)

      J. Chromatogr. A. 1588, 137-149 (2019). HPTLC of sugars (1), amino acids (2), gluconic acid (3) and glycerol (4) in 20 wine samples on silica gel with i-propanol - n-butanol - boric acid solution (200 mg/10 mL) - acetic acid 14:6:3:1 for (1), 2-butanol - ammonia solution (25 %) - pyridine - water 19:5:17:13 for (2), methanol - water 7:3 for (3) and acetonitrile - boric acid solution (200 mg/10 mL) 4:1 for (4). Detection of (3) by heating at 190 °C for 20 min, followed by densitometric evaluation at 366 nm. Further detection by dipping into: 1) diphenylamine-aniline-phosphoric acid reagent, followed by heating at 120 °C for 10 min; 2) vanillin-sulfuric acid reagent, followed by heating at 135 °C for 20 min; 3) ninhydrin reagent, followed by heating at 110 °C for 5 min; 4) bromophenol blue, followed by heating at 110 °C for 10 min. Derivatized plates were documented in white light and under UV light at 366 nm. Quantification of (4) was performed using a deuterium/tungsten lamp at 380 nm. Micro planar chromatography was performed using a device, where the HPTLC foil was covered by a thick glass plate with a hole in the center, through which the mobile phase was supplied. Further analysis by mass spectrometry. 

       

      Classification: 4d, 6
      125 032
      Effect directed detection of Rhodiola rosea L. root and rhizome extract
      H. NIKOLAICHUK, M. STUDZINSKI, Irena CHOMA* (*Department of Chromatography, Faculty of Chemistry, Institute of Chemical Sciences, Maria Curie Sklodowska University, Lublin, Poland, irena.choma@poczta.umcs.lublin.pl)

      J. Liq. Chromatogr. Relat. Technol. 43, 361-366 (2020). HPTLC of the dried root and rhizome of Rhodiola rosea on silica gel with ethyl acetate - methanol - water 77:13:10. Detection by spraying with 1) a solution of p-anisaldehyde (0.5 mL in 85 mL methanol, 10 mL acetic acid and 5 mL sulfuric acid), followed by heating at 105 ºC for 5-7 min, 2) a solution of 2-isopropyl-5-methylphenol (0.5 g in 95 mL ethanol and 5 mL sulfuric acid), followed by heating at 120 ºC and 3) NP solution (1 g diphenylboryloxyethylamine in 100 mL methanol) and PEG solution (5 g PEG-4000 in 100 mL ethanol). Detection under UV 254 and 366 nm. Effect directed detection was performed using 1) DPPH* radical reagent assay: spraying with 0.2 % 2,2-diphenyl-1-picrylhydrazyl solution in methanol, 2) AChE assay: spraying with the enzyme solution (20 units of AChE and 150 mg BSA in 150 mL 0.05 M TRIS buffer, pH 7.8), follwed by incubation at 37 ºC for 20 min and spraying with 50 mg Fast Blue B salt diluted in 100 mL of water and 3) Bacillus subtilis bioassay: dipping into bacterial suspension for 8 s, followed by incubation at 37 ºC for 17 h and spraying with 0.2 % MTT aqueous solution. The bioautographic tests showed presence of both antioxidants (DPPH assay) and antibacterials (Bacillus subtilis assay) in the methanolic plant extract, however no acetylcholinesterase inhibitors were found. As marker compound, rosavin was detected.

      Classification: 6, 8a
      119 026
      Five new triterpenoid saponins from the rhizomes of Panacis majoris and their antiplatelet aggregation activity
      M. LI (Li Min), F. LIU (Liu Fen), Y. JIN (Jin Yong-Ri), X. WANG (Wang Xiao-Zhong), Q. WU (Wu Qian), Y. LIU (Liu Ying), X. LI (Li Xu-Wen)* (*College of Chemistry, Jilin University, Changchun, China; xwli@jlu.edu.cn)

      Planta Medica 83(03/04), 351-357 (2017). Acid hydrolysis of five new dammarane-type saponosides extracted from Panax japonicus var. major rhizomes for 5 h in methanol – HCl 1:1 in sealed capillary at 80°C, then TLC on silica gel with n-butanol – acetic acid – water 5:1:4 (upper phase) and with chloroform – methanol – water 16:8:1. After derivatization with aniline phthalic acid reagent, sugar moieties were identified as glucose units by comparison to standards. Note that in the title, by ignorance of the Latin grammar, the authors wrote “Panacis majoris” instead of the nominative “Panax major”. In the names of the compounds, the –ane or –ene ending was often also omitted.

      Classification: 4e, 6, 9, 14, 32e
      63 022
      (Paper and thin-layer chromatography in food laboratories) (Hungarian)
      Z. JESZENSZKY, (OBI, H-1027 Budapest, Bem tér 2., Hungary)

      Borgazdaság 36, 21-24 (1988). TLC of sorbitol in table wine on silica with isopropanol - 0.1N boric acid 85:15. Detection by spraying with 0.1M sodium metaperiodate reagent and benzidine - ethanol - acetone - water - hydrochloric acid reagent. Detection limit, 100 mg/L sorbitol.

      Classification: 6
      102 011
      QUANTITATIVE ANALYSIS OF PROPRANOLOL HYDROCHLORIDE BY HIGH PERFORMANCE THIN LAYER CHROMATOGRaPHY
      G. Bhavar*, V. Chatpalliwar (*Dept. of Pharmaceutical Chemistry, R. C. Patel College of Pharmacy, Karvad Naka, Shirpur 425405, India)

      Ind. J. Pharm. Sci. 70 (3), 395 - 398 (2008). TLC of propranolol hydrochloride on silica gel with isopropanol - ethyl acetate - ammonia 2:17:1. Quantitative determination by absorbance measurement at 290 nm. The linearity of the method was between 200 and 2000 ng/spot. The method was successively applied for tablets, wherein, no interference from tablet excipients was observed.

      Classification: 6
      119 032
      Trypanocidal activity of flavokawin B, a component of Polygonum ferrugineum Wedd
      D.F. RODRIGUES, D.A. MANISCALCO, Flavia A. J. SILVA, Bruna G. CHIARI, María V. CASTELLI, Vera L. B. ISAAC, Regina M. B. CICARELLI, Silvia N. LÓPEZ* (*Facultad de Ciencias Bioquímicas y Farmacéuticas, Universidad Nacional de Rosario, Rosario, Argentina; slopez@fbioyf.unr.edu.ar)

      Planta Medica 83(03/04), 239-244 (2017). HPTLC of flavokawin B (purity checked by TLC, followed by sulfuric acid detection) and a hexane maceration of Polygonum ferrugineum aerial parts on silica gel, twice in the same direction with n-hexane – ethyl acetate 4:1 (humidity 33 %). Detection of flavokawin B by densitometry at 366 nm (without derivatization). The hRf value was 53. The content of flavokawin B was 13.6 % in the hexane extract and 1.0 % in the dried plant.

      Classification: 6, 7, 9, 32e
      67 045
      Determination of the average degree of hydroxy-propylation by thin-layer chromatography
      P. SALLAY*, L. FARKAS, I. RUSZNAK, (Dep. of Organic Chemistry Technology, Technical University, H-1521 Budapest, Müegyetem rkp.2., Hungary)

      Acta Chimica 127, 95-58 (1990). TLC of hydroxy-propylated dodecyl alcohol and dodecyl alcohol on silica with acetone - methanol - water 50:50:1.

      Classification: 6
      105 014
      Comparison of methods for calculation of the partition coefficients of selected aliphatic compounds
      Anna NIESTROJ (Silesian University, Institute of Chemistry, 9 Szkolna Street, 40-006 Katowice, Poland; annaniestroj@wp.pl)

      J. Planar Chromatogr. 23, 198-200 (2010). Proposition of new methods for calculation of the partition coefficients of aliphatic compounds from experimental Rf values and the numerical values of selected topological indexes. The experimental partition coefficient (log Pexp) of cetyl alcohol was determined for the n-octanol-water system. Numerical values obtained were compared with theoretical values from a database (AlogPs, AC_logP, AB/LogP, ALOGP, milogP, and XLOGP2). HPTLC of cetyl alcohol, stearyl alcohol, palmitic acid, stearic acid, alpha-hydroxypalmitic acid, and 12-hydroxystearic acid on RP18 with methanol and with methanol - water 19:1 in a horizontal chamber at room temperature. Detection after visualization in iodine vapor.

      Classification: 6, 11a