Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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J. of Chromatogr. A 1534, 170-178 (2018). HPTLC of flavonoid aglycones in eleven commercial Cistus incanus herbal teas using three independent methods (multi-development on amino phase and two two-dimensional developments on silica gel phase). HPTLC on silica gel with chloroform - methanol - ethyl acetate 15:3:2. Detection at UV 254 and 366 nm and by derivatization with aluminium chloride (1 % methanolic solution), ferric chloride (0.5 g FeCl3 in 2.5 mL water and 47.5 mL ethanol), NP-PEG (0.5 % methanolic NP solution, and after drying, 5 % ethanolic PEG solution), PABA (0.5 g PABA in 18 mL glacial acetic acid diluted with 20 mL water, plus 1 mL o-phosphoric acid and 60 mL acetone), or DPA reagents (1 g aniline and 1 g diphenylamine in 100 mL acetone and 10 mL o-phosphoric acid, heated for 5 min at 110°C). Confirmation of the presence of glucose by HPTLC on amino phase with in situ acid hydrolysis: incubation in HCl vapor followed by heating at 100°C, pre-development with acetonitrile, drying, development with acetonitrile - water 7:3, heating for 20 min at 170°C and dipping in paraffin - n-hexane 1:2 follwed by drying. TLC-direct bioautography by immersion of the developed and dried plates in a bacterial cell suspension of either Bacillus subtilis or Aliivirio fischeri strains. Analysis of the compounds isolated from the bioactive zones by HPLC-diode array detector (DAD)-electrospray ionization (ESI)-MS. The presented TLC/HPTLC platform allowed identification of the antibacterial components apigenin, kaempferide, cis- and trans-tiliroside, and the isomers of the p-coumaric acid-conjugated tiliroside, all of them inhibiting both B. subtilis and A. fischeri.
Int. J. Morphol. 37, 1164-1171 (2019). HPTLC of transresveratrol in traditional fermented soybean seed coat on silica gel with chloroform - ethyl acetate - formic acid 25:10:1. Qualitative identification under UV light at 254 and 366 nm. The hRF value for transresveratrol was 64.
Rev. Bras. Farmacogn. 29, 177-181 (2019). HPTLC of chlorogenic acid (1), 3,4-O-dicaffeoylquinic acid (2), and 3,5-O-dicaffeoylquinic acid (3) in the leaves of Pluchea indica on silica gel with ethyl acetate - water - formic acid - toluene 20:2:2:1. Quantitative determination by absorbance measurement at 326 nm. The hRF values for (1) to (3) were 34, 63 and 79, respectively. Linearity was between 100 and 400 ng/zone for (1) to (3). Intermediate precisions were below 3 % (n=3). The LOD and LOQ were 9.9 and 30.1 ng/zone for (1), 17.6 and 53.3 ng/zone for (2) and 6.7 and 20.2 ng/zone for (3), respectively. Recovery rate was 99.0 % for (1), 97.5 % for (2) and 99.6 % for (3).
J. of Chromatogr. A 1533, 180-192 (2018). HPTLC-UV/Vis/FLD-(bio)assay-HRMS of polar (phenolics) and nonpolar (tanshinones) extracts of Salvia miltiorrhiza Bunge root (Danshen), followed by streamlined scale-up to preparative layer chromatography with 1H-NMR. For phenolics, HPTLC on silica gel first with toluene - chloroform - ethyl acetate - methanol - formic acid 4:6:8:1:1 and second development with petroleum ether - cyclohexane - ethyl acetate 25:14:11. Confirmation of the acetylcholinesterase inhibitors salvianolic acid B (1), lithiospermic acid (2), rosmarinic acid (3), cryptotanshinone (4) and 15,16-dihydrotanshinone I (5). In the polar extracts, compounds (1), (2) and (3) exhibited free radical scavenging activity in the 2,2-diphenyl-1-picrylhydrazyl assay (DPPH* radical reagent), (4) and (5) were active against Bacillus subtilis and Aliivibrio fischeri (LOD of 12 ng/zone for (4), and 5 ng/zone for (5). For the first time, the unidentified, most active zone of the nonpolar Danshen extract was identified as a co-eluting zone of 1,2-dihydrotanshinone and methylenetanshinquinone 2:1.
J. Planar Chromatogr. 32, 447-451 (2019). HPTLC of Fritillaria cirrhosa on silica gel with ethyl acetate - methanol - ammonia solution - water 180:20:10:1. Bioautography by dipping into a 0.15 mg/mL solution of substrate Gly-Pro-p-nitroanilide hydrochloride in 50 % of ethanol, followed by ethanol removal in the hood and dipping into a 10 U/L DPP IV enzyme solution in TrisHCl buffer (pH 8.2, 70 mM), followed by incubation at 37°C for 40 min. Detection by dipping into a solution of 0.5 % sodium nitrite in 1.2 M hydrochloric acid, followed by drying slightly for 5 min and dipping into 0.05 % N-(1-naphthyl)ethylenediamine dihydrochloride solution. Further analysis by mass spectrometry using a TLC interface. The hRF value for the dipeptidyl peptidase IV inhibitor was 58.
J. Planar Chromatogr. 32, 467-474 (2019). HPTLC of quercetin in the fresh fruits of Benincasa hispida on silica gel with toluene - ethyl acetate - formic acid 25:20:1. Quantitative determination by absorbance measurement at 262 nm. The hRF value for quercetin was 39. Linearity was between 100 and 1200 ng/zone. Intermediate precision was below 2 % (n=6). The LOD and LOQ were 20 and 60 ng/zone. Recovery rate was 94.3 %.
J. Planar Chromatogr. 32, 461-465 (2019). HPTLC of betulinic acid (1), oleanolic acid (2) and lupeol (3) on silica gel with benzene - ethyl acetate - formic acid 679:227:94 for (1), n-hexane - ethyl acetate - glacial acetic acid 40:20:1 for (2) and n-hexane - ethyl acetate 4:1 for (3). Detection by spraying with anisaldehyde sulfuric acid, followed by heating at 105-110 ºC for 5-10 min. Quantitative determination by absorbance measurement at 530 nm. The hRF values for (1) to (3) were 79, 46 and 44, respectively. Intermediate precision was below 2 % (n=3).
J. Planar Chromatogr. 32, 379-384 (2019). HPTLC of trigonelline (1) and diosgenin (2) in the seeds of Trigonella foenum-graecum L. on silica gel with acetonitrile - water 3:1. Quantitative determination by absorbance measurement at 267 nm for (1) and at 430 nm after derivatization with vanillin - sulfuric acid for (2). The hRF values for (1) and (2) were 29 and 17, respectively. Linearity was between 200 and 1400 ng/zone for (1) and 50 and 300 ng/zone for (2). Intermediate precision was below 2 % (n=6). The LOD and LOQ were 7 and 1 ng/mL for (1) and 7 and 19 ng/mL for (2), respectively. Recovery rate was between 97.8 and 99.1 % for (1) and 98.2 and 99.3 % for (2), respectively.