Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      119 066
      Development and validation of high-performance thin-layer chromatographic
      method for determination of amygdalin
      A. RADOICIC, R. PETRONIJEVIC, F. ANDRIC, Z. TESIC, D. MILOJKOVIC* (*Faculty of Chemistry, University of Belgrade, Belgrade, Serbia, dusankam@chem.bg.ac.rs)

      J. Liq. Chromatogr. Relat. Technol. 40, 297-303 (2017). HPTLC of amygdalin on RP-18 with acetonitrile – water 1:1. Quantitative determination by absorbance measurement at 210 nm. The hRF value for amygdalin was 60. Linearity was between 2.5 and 50 μg/zone. LOD and LOQ were 1 and 4 μg/zone, respectively. The intermediate precision was <2 % (n=3). Recovery rate ranged from 99.9 to 100.6 %.

      Classification: 17
      120 058
      Thin-layer chromatographic separation and a validated high-performance thin-layer chromatography method for the quantifcation of stigmasterol in 48 different extracts of Lasiurus scindicus Henrard (Poaceae)
      N. KAUR*, R. CHAND (*Department of Botany, Punjabi University, Patiala,
      147002, India, navjot21188@gmail.com)

      J. Planar Chromatogr. 30, 495-501 (2017). HPTLC of stigmasterol in Lasiurus scindicus on silica gel with toluene ‒ methanol ‒ formic acid 90:10:3. Detection by spraying with anisaldehyde ‒ sulfuric acid reagent, followed by heating at 150 °C for 5 min. Quantitative determination by absorbance measurement at 530 nm. The hRF value for stigmasterol was 27. Linearity was between 2 and 12 ng/zone. LOD and LOQ were 0.07 and 0.2 ng/zone. Average recovery was 99.3 %.

      Classification: 13c
      121 055
      Validated thin-layer chromatographic method for the identification and monitoring of the effect of the extraction method on the yield and phytochemical constituents of Egyptian Withania somnifera leaves
      R. MAHROUS, H. FATHY, R. EL-KAHIR, A. OMAR (*Department of Pharmacognosy, Faculty of Pharmacy, Alexandria University, Alexandria, Egypt, hodasherif@hotmail.com)

      J. Sep. Sci. 41, 518-524 (2018). HPTLC of withanolide S in the leaves of Withania somnifera on silica gel with dichloromethane – toluene – methanol – acetone 15:2:1:1. Detection by spraying with sulfuric acid reagent (180 mL methanol with 20 mL sulfuric acid) followed by heating at 120 °C for 10 min. Quantitative determination by fluorescence measurement at 365/>400 nm. The hRF value for withanolide S was 7. Linearity was between 15 and 500 μg/mL. LOD and LOQ were 30 and 92 μg/mL. The intermediate/interday/intra-day precisions were below 2 % (n=3). Recovery was in the range of 94.6 and 99.1 %.

      Classification: 13c
      122 044
      Microscopic characterization and HPTLC of the leaves, stems and roots of Fadogia agrestis – an African folk medicinal plant
      V. RAMAN, J. BUDEL, J. ZHAO, J. BAE, B. AVULA, A. GALAL, Z. ALI, I. KHAN* (*National Center for Natural Products Research, School of Pharmacy, The University of Mississippi, University, MS 38677, United States, ikhan@olemiss.edu)

      Braz. J. Pharmacog. 28, 631-639 (2018). HPTLC of 3-O-α-L-rhamnopyranosyl-(1→ 2)-α-L-arabinopyranosyl pomolic acid, 2,4,6-trihydroxy-4-methoxybenzophenone-2-O-β-d-glucoside, hyperoside, geniposidic acid, nicotiflorin, narcissin, randiasaponin IV and rutin in the leaves, stems and roots of Fadogia agrestis on silica gel with chloroform – ethyl acetate – methanol – formic acid 15:30:10:4. Detection by immersion in the anisaldehyde–sulfuric acid reagent, followed by heating at 100 ºC for 3 min. The HPTLC fingerprinting method was suitable for rapid decisive authentication and comparison of differences among samples of identical source.

      Classification: 8a, 14
      62 252
      (Study on aerosol for Bi-syndrome of chest and heart pain
      L. ZHANG (Zhang Lixia), H. LIU (Liu Hong), (Inst. Basic Theory, China Acad. Trad. Chin. Med., Beijing, P.R. China)

      I. Analysis of the aerosol for the cold type symptom.) (Chinese). J. Chinese Herb Med. 19, 105- 107 (1988) (Zhongcaoyao). TLC of four compounds from herbs on silica with chloroform. Quantification by fluorodensitometry. R.S.D. 0.23%.

      Classification: 32e
      93 095
      (An improved method for quick identification of occident ginsengs by thin-layer chromatography
      X. CHENG (Cheng Xiumin)*, J. REN (Ren Jian), Y. GAO (Gao Yanhui) (*Pharm. Coll., Shandong Univ., Jinan, Shandong 250012, P. R. China)

      J. Chinese Trad. Patent Med. (Zhongchengyao) 25 (8), 665-666 (2004) .TLC on silica gel with chloroform - acetone - formic acid 10:5:2. Detection 1) by spraying with 10 % H2SO4 in ethanol and heating at 80 ºC, 2) under UV 365 nm, 3) daylight, and 4) by densitometry at 543 nm. Identification by fingerprint techniques. Running the procedure for 16 ginsengs cultivated in different regions.

      Classification: 32c
      93 147
      (Study of the quality standard of Yupingfeng oral liquid)
      Y. XIA (XIA YUFENG), Q. YANG (YANG QIN), L. XIE (XIE LIQONG), Q. WANG (WANG QIANG) (China Pharm. Univ., Nanjing 210038, P. R. China)

      (Chinese). J. Chinese Trad. Patent Med. (Zhongchengyao) 25 (12), 968-970 (2004). TLC on silica gel with 1) chloroform - methanol - water 13:7:2, 2) toluene - ethyl formate - formic acid 5:4:1, 3) n-hexane - benzene - ethyl acetate 14:3:3. Detection 1) by spraying with 10 % H2SO4 in ethanol and heating at 105 ºC for 5 min, 2) under UV 365 nm, 3) by iodine vapor. Identification by fingerprint techniques. Quantitative determination of astragaloside by HPLC.

      Classification: 4d, 32c
      94 020
      Investigation of the flavonoids in Croatian propolis by thin-layer chromatography
      I. JASPRICA, A. SMOLCIC-BUBALO, A. MORNAR, Marica MEDIC-SARIC* (*Department of Pharmaceutical Chemistry, Faculty of Pharmacy and Biochemistry, University of Zagreb, A. Kvoacica 1, 10 000 Zagreb, Croatia)

      J. Planar Chromatogr. 17, 95-101 (2004). TLC of 15 flavonoids (flavanone, naringenin, flavone, 3-, 6-, 6’-, 7-hydroxyflavone, 3,6-, 3,7-dihydroxyflavone, morin, chrysin, quercetin, galangin, apigenin, kaempferol) and 4 phenolic acids (o-, p-coumaric acid, caffeic acid, ferulic acid) on silica gel after prewashing with methanol with 11 mobile phases. Chloroform - methanol - 98-100 % formic acid 441:30:235 and n-hexane - ethyl acetate - glacial acetic acid 31:14:5 were the most appropriate eluents. Detection under UV light at 254 and 366 nm or after spraying with 1 % methanolic diphenylboryloxyethylamine and 5 % ethanolic poly(ethylene glycol) 4000, and under UV light at 366 nm after spraying with 1 % ethanolic aluminum chloride solution.

      Classification: 8a