Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

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      97 111
      Immunostimulant activity of Adhatoda vasica, Lawsonia inermis and Alkanna tinctoria, TLC fingerprint profile for identification
      K. JINYVARGHESE, S.T. KARPE AND S.R. KULKARNI* (*Dept. of Pharmacognosy and Phytochemistry, The Bombay College of Pharmacy, Kalina, Mumbai 400098, India)

      Indian Drugs 42 (6), 345-352 (2005). TLC fingerprint identification of methanolic extracts of Adhatoda vasica, Lawsonia inermis and Alkanna tinctoria, on silica gel. For Lawsonia inermis and Alkanna tinctoria the developing solvent toluene - acetone - acetic acid 90:10:1 was used, and for Adhatoda vasica n-hexane - acetone - diethyl ether 3:1:1 for. Detection of alkannin by spraying with 10 % methanolic KOH.

      Classification: 32a
      98 046
      TLC determination of aliphatic polyamines on calcium sulfate layers
      H. A. KHAN (Department of Biochemistry, College of Science, King Saud University, P.O. Box 2455, Riyadh, 11451 Saudi Arabia)

      Chromatographia 64 (7-8), 423-427 (2006). TLC of six polyamines (ornithine, citrulline, putrescine, cadaverine, spermidine and spermine) on calcium sulfate (CaSO4) and silica gel with 11 different mobile phases, using methanol as the solvent to enhance selectivity and produce differential Rf values. On CaSO4 better separation was achieved than on silica gel, no derivatization is needed, and development time is about 1/3 shorter. Quantitative determination by absorbance measurement at 550 nm after extracting substances from the plates and eluting from the coating material. Limit of detection (LOD) was 750 ng, limit of quantification (LOQ) was 1880 ng. Quantitative separation of underivatized polyamines in spiked human urine samples.

      Classification: 17a
      99 147
      Comparison between HPLC and HPTLC densitometry for the determination of icariin from Epimedium koreanum extracts
      O. POZHARITSKAYA, V. KOSMAN, A. SHIKOV*, D. DEMCHENKO, A. ESCHENKO, V. MAKAROV (*Interregional Center “Adaptogen”, St. Petersburg, Russia, alexs79@mail.ru)

      J. Sep. Sci. 30, 708-712 (2007). HPTLC of icariin in the aerial part of Epimedium koreanum Nakai on silica gel with ethyl acetate – glacial acetic acid – formic acid – water 10:1:1:2. Quantitative determination by absorbance measurement at 270 nm. The LOD and LOQ for icariin were 66 and 215 ng/band, respectively. Results did not show statistical significance between HPLC and HPTLC.

      Classification: 32e
      100 080
      Comparative study of mature and immature tubers of Imomoea mauretania by using HPLC and HPTLC analysis
      D.S. CHAUHAN*, P. DHUMAL, R. DANG, K.K. MUEEN AHMED, R. SULTANA (* AL -AMEEN COLLEGE OF PHARMACY, BANGALORE, KARNATAKA, INDIA)

      59th Indian Pharmaceutical congress C-305, 297, (2007). Phytoconstituents of mature and immature tubers of Ipomoea mauritiana (methanolic and aqueous extracts) have been studied. HPTLC on silica gel with chloroform - methanol - formic acid 6:3:1. Detection by spraying with vanilin - sulphuric acid reagent. Densitometric evaluation at 365 nm. Mature tubers were found to contain higher concentration of phytoconstiuents than immature tubers.

      Classification: 32e
      101 058
      Antibacterial and wound healing activity of roots of Sesamum indicum
      S.V. DHUMAL*, S.R. KULKARNI (*Department of Pharmacognosy and Phytochemistry, The Bombay College of Pharmacy, Sunder Nagar, Kalina, Santacruz (E), Mumbai 400098, India)

      Indian Drugs 44 (12), 937-944 (2007). HPTLC of methanolic and ethyl acetate extracts of Sesamum indicum root on silica gel with ethyl acetate - n-hexane 1:9. Densitometric evaluation at 549 nm. The red zones were isolated by preparative TLC and identified by IR as 1,4 naphthoquinone derivatives.

      Classification: 32a
      102 100
      Chemical fingerprinting of Lawsonia inermis L
      Francesca GALLO*, G. MULTARI, M. GIAMBENEDETTI, E. FEDERICI (*Dipartimento del Farmaco, Istituto Superiore di Sanita, Roma, Italy, Francesca.gallo@iss.it)

      using HPLC, HPTLC and densitometry. Phytochem. Anal. 19, 550-559 (2008). HPTLC of the leaves of Lawsonia inermis L., on silica gel with ethyl acetate – formic acid – water 82:9:9 followed by drying at 110 °C for 15 min. Detection by spraying with diphenylborinic acid aminoethylester 0.5 % in ethyl acetate, followed by drying and dipping into macrogol reagent (1 g polyethylene glycol 400 in 20 mL dichloromethane). Quantitative determination by absorbance measurement at 337 nm. Chemical fingerprint was used for quality evaluation of herbal products and detection of adulteration. Comparison with an HPLC method gave comparable results.

      Classification: 32e
      104 154
      Development and validation of a new sensitive method for the quantitative analysis of ranitidine hydrochloride and domperidone in antiulcer combination by using HPTLC
      M. PAI*, Rajashree GUDE, Swati KENY (*Goa College of Pharmacy, Panaji, Goa, India)

      60th Indian Pharmaceutical Congress PA-215 (2008). HPTLC of ranitidine HCl and domperidone in combined dosage form on silica gel with ethyl acetate - methanol - ammonia 100:10:1 in a twin trough chamber saturated for 10 min. Quantitative determination by absorbance measurement at 285 nm. The method was linear in the range of 100-500 ng/µL for both compounds with a recovery of 102.5-100.8 %.

      Classification: 32a
      105 060
      HPLC-PAD and HPTLC methods for quantitative and chromatographic fingerprint analysis of Embella ribes (Vidanga) Churna formulation
      A. BORKAR*, S. MULGUND, A. GAJBHAR, K. JAIN (*Sinhgad College of Pharmacy, Pune, Maharashtra, India)

      Abstract No. F-10, 61st IPC (2009). HPTLC of Embella ribes Churna formulation on silica gel with chloroform - ethyl acetate - formic acid 5:4:1 in a twin trough chamber. Densitometric measurement of embelin at 291 nm. The method was linear in the range of 600-1800 ng/band with recovery value of 99.1-101.2 %. The formulation was also analyzed by HPLC and results were found to be comparable.

      Classification: 32e