Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

Page
      130 127
      Simultaneous quantitative analyses of five constituents in crude and salt‑processed Cuscutae Semen using a validated high‑performance thin‑layer chromatography method
      Y. SHI (Shi Yun), J. JIN (Jin Junjie), C. XU (Xu Changli), Y. LIANG (Liang Yusha), X. LIU (Liu Xiao), X. GAO (Gao Xun), K. QIN (Qin Kunming)*, W. LI (Li Weidong) (*School of Pharmacy, Jiangsu Ocean University, Lianyungang 222005, People’s Republic of China, qinkm123@126.com)

      J. Planar Chromatogr. 35, 421-430 (2022). HPTLC of rutin (1), chlorogenic acid (2), hyperin (3), isoquercitrin (4) and astragalin (5) on silica gel with ethyl acetate - formic acid - water - toluene 18:2:2:1. Quantitative determination by absorbance measurement at 318 nm. Linearity was between 33 and 1139 ng/zone for (1), 13 and 1048 ng/zone for (2), 14 and 1110 ng/zone for (3), 1 and 298 ng/zone for (4) and 2 and 711 ng/zone for (5). The LOD and LOQ were 4 and 14 ng/zone for (1), 3 and 13 ng/zone for (2), 3 and 14 ng/zone for (3), 1 and 5 ng/zone for (4) and 2 and 9 ng/zone for (5), respectively. Average recovery was 100.0 % for (1), 98.6 % for (2), 96.6 % for (3), 94.7 % for (4) and 98.1 % for (5).

      Classification: 8a
      130 129
      High‑performance thin‑layer chromatography chemical fingerprinting: a modern technique for comparative assessment of a multivariate chromatogram analysis of Padina boergesenii
      M. HAKIM*, I. PATEL (*Department of Life Sciences, Hemchandracharya North Gujarat University, Patan, Gujarat 384265, India, hakim.masuma1@gmail.com)

      J. Planar Chromatogr. 35, 395-402 (2022). HPTLC of Padina boergesenii on silica gel with toluene - ethyl acetate 93:7. Detection by spraying with different reagents: anisaldehyde‒sulfuric acid reagent, vanillin‒sulfuric acid reagent, methanolic‒sulfuric acid reagent and Liebermann‒Burchard reagent (1 mL concentrated sulfuric acid, 20 mL acetic anhydride and 100 mL chloroform). Fingerprint analysis under UV light at 254 and 366 nm.

      Classification: 32e
      130 130
      Validated simultaneous high‑performance thin‑layer chromatography‒mass spectrometry method for analysis of citalopram prochlorperazine, midazolam, and chlorodiazepoxide in urine for forensic analysis
      P. CHOUDHARY*, K. VERMA, D. KALRA (*Regional Forensic Science Laboratory, Govt. of NCT of Delhi, Chankyapuri, New Delhi 110021, India, pallavi.choudhary23@gmail.com)

      J. Planar Chromatogr. 35, 363-373 (2022). HPTLC of midazolam (1), prochlorperazine (2), citalopram (3) and chlorodiazepoxide (4) in urine on silica gel with cyclohexane - toluene - diethylamine 14:3:3. Quantitative determination by absorbance measurement at 229 nm for (1), 257 nm for (2), 240 nm for (3) and 275 nm for (4). The hRF values for (1) to (4) were 31, 79, 63 and 7, respectively. Linearity was between 3 and 7 µg/zone for (1) to (4). Interday and intra-day precisions were below 5 % (n=3). The LOD and LOQ were 0.5 and 1.6 µg/zone for (1), 0.7 and 2.1 µg/zone for (2), 0.5 and 1.6 µg/zone for (3) and (4).  Average recovery was 95.5 % for (1), 90.5 % for (2), 95.9 % for (3) and 92.5 % for (4).

      Classification: 32d
      130 131
      Development of a new chromogenic spray reagent for the detection and identification of synthetic pesticide carbaryl in biological material by high‑performance thin‑layer chromatography
      U. PAWAR, D. PANSARE*, R. SHELKE, C. PAWAR, A. PATHAN, V. THAKRE, B. DOBHAL, R. PARDESHI (*Regional Forensic Science Laboratories, Aurangabad, Maharashtra, India, dattatraya.pansare7@gmail.com)

      J. Planar Chromatogr. 35, 431-434 (2022). HPTLC of carbaryl in biological material on silica gel with hexane - acetone 4:1. Detection by spraying with reagent A (4 g sodium hydroxide in 100 mL water), waiting for 10 min, followed by spraying with reagent B (2 g vanillin in 100 mL acetone). Brown-colored zone with white background was clearly visible. The hRF values for carbaryl were 22 and 54.

      Classification: 29c
      130 132
      A validated method for the thin‑layer chromatographic in situ autofluorescence densitometric quantitation of the benzylisoquinoline alkaloids berberine and sanguinarine
      N. ESTRADA, M. MONFORTE, Z. ESCOBAR, A. CORDOVA, F. VASQUEZ* (*Unidad de Bioquímica y Biología Molecular de Plantas, Centro de Investigación Científica de Yucatán, 97205 Mérida, Yucatán, Mexico, felipe@cicy.mx)

      J. Planar Chromatogr. 35, 375-381 (2022). HPTLC of benzylisoquinoline alkaloids sanguinarine (1) and berberine (2) in Argemone mexicana on silica gel with benzene - ethanol 47:3 for (1) and n-butanol - water - ammonia 8:1:1 for (2). Quantitative determination by absorbance measurement at 365 nm. The hRF values for (1) and (2) were 36 and 32, respectively. Linearity was between 10 and 40 ng/zone for both (1) and (2). Interday and intra-day precisions were below 1 % (n=3). The LOD and LOQ were 1 and 4 ng/zone for both (1) and (2). Recovery was between 92.7 and 93.5 %.

      Classification: 22
      130 133
      A developed high‑performance thin‑layer chromatography method for the determination of baicalin in Oroxylum indicum L. and its antioxidant activity
      S. ADIN*, I. GUPTA, A. AHAD, M. AQIL, M. MUJEEB (*Phytomedicine Laboratory, Department of Pharmacognosy & Phytochemistry, School of Pharmaceutical Education & Research, Jamia Hamdard, New Delhi 110062, India, aqilmalik@yahoo.com)

      J. Planar Chromatogr. 35, 383-393 (2022). HPTLC of baicalin in the stem barks of Oroxylum indicum on silica gel with acetone - ethyl acetate - water - formic acid 4:20:1:1. Quantitative determination by absorbance measurement at 318 nm. The hRF value for baicalin was 49. Linearity was between 0.2 and 1.0 µg/zone. Interday and intra-day precisions were below 1 % (n=3). The LOD and LOQ were 56 and 188 ng/zone. Average recovery was 99.2 %.

      Classification: 8a
      130 134
      High‑performance thin‑layer chromatography evaluation of the counterfeiting of vanilla flavoring
      A. HOSU, Claudia CIMPOIU* (*Department of Chemistry, Faculty of Chemistry and Chemical Engineering, Babes-Bolyai University, 11
      Arany Janos Street, 400028 Cluj-Napoca, Romania, ccimpoiu@yahoo.com)

      J. Planar Chromatogr. 35, 281-285 (2022). HPTLC of vanillin (1) and ethyl vanillin (2) in flavoring agents on silica gel with toluene - chloroform - acetone 7:8:2. Detection under UV light at 254 and 366 nm. The hRF values for (1) and (2) were 46 and 55, respectively.

      Classification: 7
      130 135
      Applications of the solvation parameter model in thin‑layer chromatography
      C. POOLE (Department of Chemistry, Wayne State University, Detroit,
      MI 48202, USA, cfp@chem.wayne.edu)

      J. Planar Chromatogr. 35, 207-227 (2022). The paper discussed the applications of the solvation parameter model in TLC, as a transfer model for biphasic systems in which isotropic interactions in each phase are responsible for the preferential solvation of a solute in one phase over the other. The model emphasizes the importance of water in the mobile phase and the general contributions of mobile phase interactions on the retention mechanism. In addition, the selected solvation of the stationary phase in contact with the mobile phase makes an important contribution to system selectivity. System constants for reversed-phase separations on chemically bonded silica gel HPTLC layers with different mobile phases compositions were also discussed and applied to construct correlation diagrams to facilitate the comparison of selectivity for different layers with the same mobile phase composition or different mobile phase compositions for the same layer.

      Keywords: HPTLC
      Classification: 2c
Page