Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      130 116
      Agar‑free high‑performance thin‑layer chromatography–bioautography method for the qualitative estimation of α‑amylase inhibitor in Syzygium cumini seed extract and formulation
      S. BHUJBAL*, B. CHAWALE, M. KALE, R. BHUJBAL (*Department of Pharmacognosy, Dr. D. Y. Patil Institute of Pharmaceutical Sciences and Research, Sant. Tukaram Nagar Pimpri, Pune, Maharashtra 411018, India, santosh.bhujbal@dypvp.edu.in)

      J. Planar Chromatogr. 35, 501-507 (2022). HPTLC of β-sitosterol the seeds of Syzygium cumini on silica gel with toluene - ethyl acetate - methanol - glacial acetic acid 6:3:2:1. Detection by dipping into anisaldehyde sulfuric acid solution for 3 s, followed by heating at 80-100 °C for 2-3 min. The assessment of α-amylase inhibitors was performed by dipping into enzyme solution (10 mg α-amylase enzyme in 20 mL of sodium acetate buffer and stored at 2–8 °C) for 2–3 seconds, followed by 90 min humidification in a desiccator and the dipping into a 1 % starch solution as a substrate and put in a humid environment for additional 20–30 min to allow the enzyme–substrate interaction to occur. After a 2–5-min time, the plate was washed or dipped in Gram’s iodine blue, which revealed anti-diabetic activity as blue stains on a white background. The hRF value for β-sitosterol was 87. Further analysis by high‑resolution mass spectrometry.

      Classification: 13c
      130 117
      Combination of high‑performance thin‑layer chromatography and liquid chromatography–quadrupole time‑of‑flight–tandem mass spectrometry analysis: a promising analytical tool for discrimination between oleo‑gum resin of raw and purified Commiphora wightii
      V. CHARDE, C. JAGTAP, Y. GANDHI, R. VERMA, S. MISHRA, V. KUMAR*, R. ACHARYA (*Department of Ayurveda, Central Ayurveda Research Institute, Jhansi, Uttar Pradesh 284003, India, vijaychem99@gmail.com)

      J. Planar Chromatogr. 35, 481-490 (2022). HPTLC of oleo‑gum resin of raw and purified Commiphora wightii on silica gel with chloroform - ethyl acetate - formic acid - acetic acid
      30:9:2:2. Detection by spraying with anisaldehyde sulfuric acid reagent, followed by heating at 105 °C until the development of visible zones. The plate was analyzed under UV light at 254 and 366 nm, and after derivatization at 541 nm. 

      Classification: 32e
      130 118
      A validated method for the thin‑layer chromatography in situ densitometric quantitation of capsaicinoids in Habanero pepper (Capsicum chinense Jacq.)
      A. CORDOVA, M. MONFORTE, A. ROZETE, N. ESTRADA, F. VAZQUEZ* (*Unidad de Bioquímica y Biología Molecular de Plantas, Centro de Investigación Científica de Yucatán, 97205 Mérida, Yucatán, Mexico, felipe@cicy.mx)

      J. Planar Chromatogr. 35, 473-479 (2022). HPTLC of capsaicin and dihydrocapsaicin as capsaicinoids in Habanero pepper pods on silica gel with cyclohexane - chloroform - acetic acid 7:2:1. Quantitative determination by absorbance measurement at 254 nm. The hRF value for capsaicinoids was 29. Linearity was between 0.5 and 4.0 µg/zone. Interday and intra-day precisions were below 6 % (n=6). The LOD and LOQ were 251 and 750 ng/zone, respectively. 

      Classification: 17c
      130 119
      Development of an identification method for fern extracts using high‑performance thin‑layer chromatography (HPTLC)
      Melania ENOT*, R. SABESAJE, G. PRESORES, G. BARBOSA, A. ANG, R. BAUTISTA, R. DE LA CRUZ (*Tuklas Lunas Development Center, Central Mindanao University, University Town, Musuan, 8714 Bukidnon, Philippines, melaniaenot@cmu.edu.ph)

      J. Planar Chromatogr. 35, 491-500 (2022). HPTLC of gallic acid in fern species Drynaria
      quercifolia, Diplazium esculentum, and Asplenium nidus
       on silica gel with ethyl acetate - formic acid - acetic acid - water 120:11:11:26. Detection by heating at 100 °C for 3 min, followed by dipping into NP reagent (1.0 g of 2-aminoethyl diphenyl borate in 200 mL of ethyl acetate and stored at 4 °C).
      Quantitative determination by absorbance measurement at 366 nm. The hRF value for gallic acid was 82. Interday and intra-day precisions were below 1 % (n=3). 

       

      Classification: 7
      130 120
      Detection of diazepam in spiked drink using thin‑layer chromatography
      A. KAMBLE, J. KENNADY, A. BADIYE, N. KAPOOR* (*Department of Applied Chemistry, Karunya Institute of Technology and Sciences, Coimbatore, Tamil Nadu, India, neeti.kapoor86@gmail.com)

      J. Planar Chromatogr. 35, 543-546 (2022). HPTLC of diazepam in spiked lemon juice drink on silica gel with chloroform - acetone 4:1 (system 1) and chloroform - methanol - ethyl acetate 14:3:1 (system 2). Detection under UV light at 254 nm. The hRF values for diazepam in systems 1 and 2 were 72 and 88, respectively. 

      Classification: 32d
      130 121
      High‑performance thin‑layer chromatography method development and validation for quantification of naringin in different extracts of Citrus sinensis L. and its antioxidant activity
      I. GUPTA, S. ADIN, M. AQIL*, M. MUJEEB (*hytomedicine Laboratory, Department of Pharmacognosy & Phytochemistry, School of Pharmaceutical Education &Research, Jamia Hamdard, New Delhi 110062, India, aqilmalik@yahoo.com)

      J. Planar Chromatogr. 35, 463-471 (2022). HPTLC of naringin in the peels of Citrus sinensis on silica gel with glacial acetic acid - chloroform - water - methanol 10:30:1:5. Detection by heating at 60 °C for 5 min. Quantitative determination by absorbance measurement at 296 nm. The hRF value for naringin was 45. Linearity was between .04 and 2.0 µg/zone. Interday and intra-day precisions were below 1 % (n=3). The LOD and LOQ were 6 and 19 ng/zone. Average recovery was 99.4 %.

      Classification: 8a
      130 123
      Enantioresolution of three β‑blockers using l‑glutamic acid as chiral selector by thin‑layer chromatographic methods
      R. VYAS, V. VASHISTHA, A. SHARMA, R. KUMAR, S. BHARDWAJ, J. MEENA, H. GUPTA, H. NAGAR* (*School of Applied Sciences, Suresh Gyan Vihar University, Jaipur, Rajasthan 302017, India, hariomnagariitr@gmail.com)

      J. Planar Chromatogr. 35, 533-541 (2022). HPTLC of three β-blockers, namely, (RS)-pindolol (1), (RS)-alprenolol (2), and (RS)-sotalol (3) on silica gel mixed with L-Glu as chiral selector, and methanol - acetonitrile - water - dichloromethane 9:3:4:1 as mobile phase. Detection by exposure to iodine vapor. The hRF values for (1) to (3) were 48, 44 and 55, respectively. The LOD was found within 1.3-1.7 µg/zone for (1) to (3). Recovery was between 96.3 and 98.7 % for the enantiomers.

      Classification: 38
      130 124
      Development and validation of a high‑performance thin‑layer chromatographic method for the simultaneous estimation of berberine, gallic acid, mangiferin, and quercetin in Amritamehari churnam
      S. MENON, P. TATKE* (*MET Institute of Pharmacy, Bandra West, Mumbai, India, drpratimatatke@gmail.com)

      J. Planar Chromatogr. 35, 453-461 (2022). HPTLC of mangiferin (1), berberine (2), gallic acid (3), and quercetin (4) in Amritamehari churnam on silica gel with toluene - ethyl acetate - formic acid - methanol 5:4:1:1. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (4) were 13, 32, 49 and 64, respectively. Linearity was between 50 and 1000 ng/zone for (1), 100 and 1000 ng/zone for (2), 1200 and 2600 ng/zone for (3) and 100 and 800 ng/zone for (4). Interday and intra-day precisions were below 3 % (n=3). Average recovery was 93.7 % for (1), 91.2 % for (2), 94.5 % for (3) and 99.0 % for (4).

      Classification: 8a
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