Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      109 102
      Development of analytical methods (RP-HPLC and HPTLC) for the fast analysis of glabridin in crude drug and Unani formulations
      R. PARVEEN*, Y.T. KAMAL, M. SINGH, E.T. TAMBOLI, S. RAHMAN, S. AHMAD, F.J. AHMAD (*Department of Pharmaceutics, Faculty of Pharmacy, Hamdard University, Hamdard Nagar, New Delhi, India-110062)

      Planta Med. 77, 548 (2011). HPTLC of glabridin (4-[(3R)-8,8-dimethyl-3,4-dihydro-2H-pyrano[6,5-f]chromen-3-yl]benzene-1,3-diol) on silica gel with toluene - dichloromethane - ethyl acetate 1:1:1. Detection under UV light at 286 nm.

      Classification: 32e
      109 124
      Determination of novel plant growth promoting diterpenes in Callicarpa macrophylla by HPLC and HPTLC
      R. VERMA, A. SINGH, P. SRIVASTAVA, K. SHANKER, A. KALRA, M. GUPTA* (*Analytical Chemistry Division, Central Institute of Medicinal and Aromatic Plants, Lucknow–226015, India, guptammg@rediffmail.com)

      J. Liq. Chromatogr. Relat. Technol. 32, 2437-2450 (2009). HPTLC calliterpenone (1) and calliterpenone monoacetate (2) in the leaves of Callicarpa macrophylla on silica gel with methanol - water 9:11. Quantitative determination by absorbance measurement at 210 nm. The hRf values of (1) and (2) were 43 and 73, respectively. Linearity was between 1-5 µg/zone for (1) and (2). LOD and LOQ were 230 and 780 ng/zone for (1) and 220 and 730 ng/zone for (2). Intra-day and inter-day precisions ranged between 1.3-1.7 % for (1) and 1.1-1.7 % for (2). Recoveries (by standard addition) were between 97.5-100.8 % for both.

      Classification: 32e
      110 019
      Preparation and characterization of some ethyl-phenyl modified stationary phases
      Olivia MARUTOIU, C. TIGAE, C. MARUTOIU*, I. KACSO, I. BRATU, Ioana PERHAITA (*Babe-Bolyai University Cluj-Napoca, Faculty of Orthodox Theology, 18 Piaba Avram Iancu Square, Cluj-Napoca, Romania, cmarutoiu@yahoo.com)

      J. Planar Chromatogr. 25, 548-553 (2012). New modified stationary phases obtained by chemical modification of diatomaceous earth from Filia and silica gel with trimethoxyethylphenylsilane. Separations on ethyl-phenylmodified adsorbents are similar to the separation on C8.

      Classification: 3b
      110 041
      Qualitative and quantitative analysis of hyaluronan oligosaccharides with high-performance thin layer chromatography using reagent-free derivatization on amino-modified silica and electrospray ionization-quadrupole time-of-flight mass spectrometry couplin
      M. ROTHENHÖFER, ROSMARIE SCHERÜBL, G. BERNHARDT, J. HEILMANN*, A. BUSCHAUER (*Lehrstuhl für Pharmazeutische Biologie, Universität Regensburg, Universitätsstr. 31, 93040 Regensburg, Germany)

      J. of Chromatogr. A 1248, 169-177 (2012). Purified oligomers of hyalobiuronic acid are indispensable tools to elucidate the physiological and pathophysiological role of hyaluronan degradation by various hyaluronidase isoenzymes. Establishment and validation of a novel sensitive, convenient, rapid, and cost-effective HPTLC method for the qualitative and quantitative analysis of small saturated hyaluronan oligosaccharides consisting of 2–4 hyalobiuronic acid moieties. HPTLC on amino phase with 1-butanol - formic acid - water 3:5:2 or 3:4:1. Detection 1) by spraying with orcinol in various concentrations of sulfuric acid; 2) by dipping into the reagent of orcinol in 10 % sulfuric acid and Morgan–Elson reagent; 3) by illuminating with white light and UV 366 nm after heating. The simple reagent-free in situ derivatization of 3) resulted in a detection limit of 7–19 pmol/band and LOQ of 37–71 pmol/band depending on the analyzed saturated oligosaccharide. Identification of the analytes by TLC-ESI-MS. The validated HPTLC method, as an alternative to sequential techniques such as HPLC and CE, can easily be automated and is applicable to the analysis of multiple samples in parallel.

      Classification: 17
      110 060
      Application of high-performance thin-layer chromatography for determination of nicotine in different brands of cigarettes
      J. BADR*, F. BAMANE, N. EL-SHAER (*Department of Pharmacognosy, Faculty of Pharmacy, Suez Canal University, Ismailia 41522, Egypt, jihanbadr2010@hotmail.com)

      J. Liq. Chromatogr. Relat. Technol. 35, 1213-1221 (2012). HPTLC of nicotine in cigarettes on silica gel with n-hexane - methylene chloride - methanol 4:16:3. Quantitative determination by absorbance measurement at 254 nm. Linearity was in the range of 0.1-1 mg/mL. Precision was estimated with an %RSD below 2.0. Limits of detection and quantification were 0.008 mg/mL and 0.02 mg/mL, respectively. The method provides acceptable intra-day and inter-day precision for nicotine. Recovery was between 97.5 and 98.4 %, respectively.

      Classification: 32d
      110 091
      Differentiating the gum resins of two closely related indian Gardenia species, Gardenia gummifera and Gardenia lucida, and establishing the source of dikamali gum resin using high-performance thin-layer chromatography and ultra-performance liquid chromato
      S. LAKAVATH, B. AVULA, Y. WANG, C. RUMALL, S. GANDHE, A. BELVOTAGI, P. ACHANTA, R. KUMAR, I. KHAN, A. NARASIMHA* (*Kakatiya University, University College of Pharmaceutical Sciences, Department of Pharmaceutical Chemistry, Warangal-506009, Andhra Pradesh, India, avnapparao@yahoo.com)

      J. AOAC Int. 95, 67-73 (2012). HPTLC fingerprint of four cycloartanes dikamaliartane-A (1) and dikamaliartane-B (2) and gummiferartane-1 (3) and gummiferartane-2 (4) in the gum resin from the leaf buds of Gardenia lucida or G. gummifera on silica gel with toluene – acetone 11:9. Detection by dipping in anisaldehyde reagent (anisaldehyde 0.5 % in methanol – acetic acid – sulfuric acid 17:2:1), followed by heating at 100 °C for 5 min. The hRf of compounds (1) to (4) were 60, 80, 90 and 70, respectively.

      Classification: 32e
      110 125
      A simple and sensitive HPTLC method for simultaneous analysis of tolperisone hydrochloride and etodolac in combined fixed-dose oral solid formulation
      M. PATEL*, A. PATEL, C. PATEL, R. BADMANABAN (*Quality Assurance Department, Shree Sarvajanik Pharmacy College, Nr. Arvind Baug, Mehsana, Gujarat 384001, India, mitpatel23@gmail.com)

      J. Planar Chromatogr. 25, 85-88 (2012). HPTLC of tolperisone hydrochloride (1) and etodolac (2) in combined dosage form on silica gel with toluene - ethylacetate - ethanol 12:3:5. Quantitative determination by absorbance measurement at 260 nm. The hRf of (1) and (2) were 40 and 58, respectively. Linearity was in the range of 75-450 ng/band for (1) and 200-1200 ng/band for (2). Limits of detection and quantification were 1 and 4 ng/band for (1) and 2 and 5 ng/band for (2), respectively. The intermediate/inter-day/intra-day precision was below 2 % (n=3). Recovery was between 98.1 and 100.9 %.

      Classification: 32a
      110 158
      Densitometric determination of mebhydrolin napadisylate in tablets
      L. WULANDARI, M. YUMONO, G. INDRAYANTO* (*Faculty of Pharmacy, Airlangga University, Dharmawangsa Dalam, Surabaya 60286, Indonesia, gunawanindrayanto@yahoo.com)

      J. Planar Chromatogr. 25, 60-64 (2012). HPTLC of mebhydrolin napadisylate in tablets on silica gel with methanol - ethyl acetate 1:1. Quantitative determination by absorbance measurement at 287 nm. Linearity was in the range of 600-1600 ng/zone. Limits of detection and quantification were found to be 19 and 56 ng/zone, respectively. The intermediate/inter-day/intra-day precision was below 2 %. Recovery (by standard addition) was in the range of 99.3-100.8 %.

      Classification: 32a
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