Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      117 038
      Tracking and identification of antibacterial components in the essential oil of Tanacetum vulgare L
      Ágnes M. MÓRICZ*, T.T. HÄBE, Andrea BÖSZÖRMÉNYI, P.G. OTT, Gertrud E. MORLOCK (*Plant Prot. Inst., Centre for Agr. Res., Hungarian Acad. of Sci., Herman O. Str. 15, 1022 Budapest, Hungary)

      by the combination of high-performance thin-layer chromatography with direct bioautography and mass spectrometry. J. of Chromatogr. A 1422, 310-317 (2015). Investigation of two tansy (Tanacetum vulgare L.) essential oils, obtained by steam distillation of the capitula with subsequent liquid-liquid extraction (oil 1) or with use of an auxiliary phase for the trapping of the steam components (oil 2), against Bacillus subtilis F1276, B. subtilis spizizenii (DSM 618), Xanthomonas euvesicatoria, Pseudomonas syringae pv. maculicola, Ralstonia solanacearum strain GMI1000 and Aliivibrio fischeri by using the coupling of HPTLC to direct bioautography (HPTLC-DB). Oil 2 was richer in components and provided more inhibition zones due to the advanced extraction process. Identification of the main bioactive components by scanning HPTLC-direct analysis in real time mass spectrometry (HPTLC-DART-MS) and solid-phase microextraction GC electron impact MS (SPME-GC-EI-MS) as cis- and trans-chrysanthenol as well as trans-chrysanthenyl acetate. The results indicated that cis-chrysanthenol exhibited antibacterial effects against all tested bacteria. Trans-chrysanthenol inhibited B. subtilis, R. solanacearum and A. fischeri, and trans-chrysanthenyl acetate was an inhibitor for X. euvesicatoria, R. solanacearum and A. fischeri. However, the ionization characteristics and the recorded mass spectra showed that DART is a softer ionization technique than EI and more affected by ambient conditions and thus prone to additional oxidation products, although HPTLC-DART-MS resulted in a comparable fragmentation.

      Classification: 4e, 32e
      117 058
      Development and validation of a high-performance thin-layer chromatographic–densitometric method for the quantification of apigenin in Ocimum basilicum L
      N. PARIKH, C. KOTHARI* (*Department of Pharmaceutical Analysis, Institute of Pharmacy, Nirma University, Ahmedabad, Gujarat, India, charmyshah@gmail.com)

      seed (Takhmaria). J. Planar Chromatogr. 29, 216-220 (2016). HPTLC of apigenin in the seeds of Ocimum basilicum on silica gel with toluene – acetone – formic acid 5:4:1. Quantitative determination by absorbance measurement at 340 nm. The hRF value of apigenin was 71. Linearity was in the range of 100-600 ng/zone. Intermediate precisions were below 0.5 %. The LOD and LOQ were 4 and 12 ng/zone. Recovery was between 98.5 and 100.6 %.

      Classification: 8a
      117 077
      Effect of dietary complex lipids on the biosynthesis of piglet brain gangliosides
      M.M. REIS*, E.N. BERMINGHAM, M.G. REIS, S. CHOUDHURY, A. MACGIBBON, B. FONG, P. MCJARROW, R. BIBILONI, S.A. BASSETT, N.C. ROY (*Food Nutrition & Health Team, Food & Bio-Based Products Group, AgResearch Grasslands, Palmerston North 4442, New Zealand, marlon.m.reis@agresearch.co.nz.)

      J. Agric. Food Chem. 64, 1245-1255 (2016). Preparative HPTLC of gangliosides in the frontal lobe of piglets on silica gel with chloroform – methanol – calcium chloride 50:42:11. Fractions were subjected to a series of reactions to obtain sialic acid, glucose, galactose, N-acetyl-galactosamine, and fatty acid derivatives.

      Classification: 11e
      117 094
      Quantification of nicotine in liquids for electronic cigarettes
      Tiên DO (CAMAG, Sonnenmattstrasse 11, 4132 Muttenz, Switzerland, tien.do@camag.com)

      CBS 116, 13-15 (2016). HPTLC of nicotine in e-liquids on silica gel with chamber saturation (with filter paper) for 20 min with toluene – acetone –diethylamine 10:10:1 to the migration distance of 70 mm. Detection under UV 254 nm. Quantitative determination by absorbance measurement at 260 nm. Elution of the zones with methanol (with 0.1 % formic acid) into a single quadrupole MS and detection in positive ionization mode. The hRf value of nicotine was 56 and separation from other ingredients (propylene glycol, glycerol, flavors) was good. Visual evaluation of the samples for presence of nicotine was confirmed with MS and UV spectra.

      Classification: 22
      117 119
      Identification of herbal slimming drugs and screening for adulteration by HPTLC
      S. MEDHE*, K. DODTALE, S. BHARUCHA, K. JAYACHANDRAN, P. HANDE, T. THITE (*Anchrom Testlab Pft. Ltd., A-101, Shree Aniket Apt. Navgar Road, 400 081, Mulund (E) Mumbai, India, hptlc@anchrom.in)

      CBS 116, 9-10 (2016). HPTLC of herbal slimming drugs and the standard orlistat on silica gel with toluene – ethyl acetate 4:1 with chamber saturation (with filter paper) to the migration distance of 70 mm. Detection by dipping in phosphomolybdic acid reagent (5 g in 100 mL ethanol) and heating at 110 °C for 5 min. Evaluation under UV 254 nm, 366 nm and white light. Quantitative determination by absorbance measurement at 195 nm before derivatization to detect illegally added orlistat in the herbal drugs. The LOD of orlistat standard was 70 ng/band.

      Classification: 32c
      118 019
      Trilinear analysis of thin-layer chromatography retention of 35 model compounds chromatographed on nine adsorbents with 20 pure solvents
      L. KOMSTA*, R. SKIBINSKI, N. BEZPALKO, A. MIELNICZEK, B. STEPKOWSKA (*Department of Medicinal Chemistry, Medical University of Lublin, Jaczewskiego 4, 20–090 Lublin, Poland, lukasz.komsta@umlub.pl)

      J. Sep. Sci. 39, 4258-4262 (2016). TLC of 35 model compounds on RP-2, RP-8, RP-18, alumina, cellulose, cyano, diol, amino phase, and silica gel with 20 pure solvents (acetone, acetonitrile, 1-butanol, 1-chlorobutane, chloroform, cyclohexane, 1,2-dichloroethane, dichloromethane, dioxane, ethanol, ethyl acetate, heptane, hexane, methanol, isooctane, 1-propanol, 2-propanol, t-butyl methyl ketone, tetrahydrofuran, and toluene). Parallel factor analysis was used to study the retention phenomena in quantitative manner.

      Classification: 2c
      118 047
      High-performance thin-layer chromatographic analysis for the simultaneous quantification of gallic acid, vanillic acid, protocatechuic acid, and quercetin in the methanolic fraction of Limonia acidissima L
      S. VERMA, A. GUPTA, M.V. RAMANA, A.K.S. RAWAT* (*Pharmacognosy and Ethnopharmacology Division, CSIR – National Botanical Research Institute, Lucknow 226 001, India, rawataks@rediffmail.com)

      fruits. J. Planar Chromatogr. 29, 356-360 (2016). HPTLC of gallic acid (1), vanillic acid (2), protocatechuic acid (3), and quercetin (4) in the fruits of Limonia acidissima on silica gel with toluene – ethyl acetate – formic acid 5:4:1. Quantitative determination by absorbance measurement at 254 nm. The hRF values of (1) to (4) were 30, 47, 37 and 42, respectively. Linearity was between 100 and 600 ng/zone for (1) to (4). The intermediate precisions for (1) to (4) were below 1.6 % (n=3). The LODs and LOQs were 30 and 91 ng/zone for (1), 25 and 76 ng/zone for (2), 33 and 100 ng/zone for (3) and 28 and 85 ng/zone for (4). Recoveries were between 98.0 and 100.1 % for (1) to (4).

      Classification: 8a
      118 068
      Assessment of preservative potential of Cinnamomum zeylanicum Blume essential oil against food borne molds, aflatoxin B1 synthesis, its functional properties and mode of action
      S. KIRAN, A. KIJUR, B. PRAKASH* (*Department of Food Protectants and Infestation Control, CSIR-Central Food Technological Research Institute, Mysore 570020, India, bhanubhu08@gmail.com)

      Innov. Food Sci. Emerg. Technol. 37, 184-191 (2016). HPTLC of aflatoxin B1 in Aspergillus flavus isolates on silica gel with toluene – isoamyl alcohol – methanol 90:32:2. Qualitative determination under UV light at 360 nm.

      Classification: 28b
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