Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
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      117 083
      Determination of common triterpenoids and phytosterols in vegetable waxes by HPTLC-densitometry and HPTLC-image analysis
      M. MARTELANC, K. NAUMOSKA, Irena VOVK* (*National Institute of Chemistry, Hajdrihova 19, 1000 Ljubljana, Slovenia, irena.vovk@ki.si)

      J. Liq. Chromatogr. Relat. Technol. 39, 312-321 (2016). HPTLC of lupeol in waxes of different cabbage varieties on RP-18 with ethyl acetate – acetonitrile 5:1. Detection by dipping into the anisaldehyde reagent (16 mL sulfuric acid were dropwise added to a cooled mixture of 20 mL glacial acetic acid and 170 mL methanol, then 1 mL of anisaldehyde was added), followed by heating at 110 °C for 30 s. Quantitative determination by absorbance measurement at 535 nm. The hRF of lupeol was 40. Linearity was in the range of 30-150 ng/zone. The LOD and LOQ were 7 and 20 ng/zone, respectively. Intermediate precisions were below 10 %. Recoveries were between 90.3 and 93.1 %.

      Classification: 14
      117 114
      (Study of the method for the quality control of Shengxinfa Jiaonang capsules) (Chinese)
      W. FAN (Fan Weifeng), SH. WANG (Wang Shiyong)*, D. HE (He Danxuan), ZH. YE (Ye Zhiwen), Q. LI (Li Qin) (*Yulin Pharm. Group Co. Ltd., Guangxi, Yulin 537001, China)

      Chinese J. of Inform. on TCM 20 (7), 59-61 (2013). Shengxinfa Jiaonang capsule is a herbal TCM preparation for treatment of hair loss caused by blood deficiency and kidney essence deficiency, scalp pruritus, alopecia areata, and postpartum alopecia. For quality control, TLC on silica gel (1) for Fallopia multiflora (Thunb.) Harald, with toluene – ethyl acetate – formic acid 15:2:1, detection in daylight; (2) for Psoralea corylifolia Linn., with n-hexane – ethyl acetate 4:1, detection by spraying with 10 KOH in methanol and viewing under UV 366 nm; (3) for Gastrodia elata Bl., with chloroform – ethyl acetate 1:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C until the zones are visible. Quantification of 2,3,5,4'-tetrahydroxy stilbene-2-Ο-β-D-glucoside by HPLC.

      Classification: 32e
      118 019
      Trilinear analysis of thin-layer chromatography retention of 35 model compounds chromatographed on nine adsorbents with 20 pure solvents
      L. KOMSTA*, R. SKIBINSKI, N. BEZPALKO, A. MIELNICZEK, B. STEPKOWSKA (*Department of Medicinal Chemistry, Medical University of Lublin, Jaczewskiego 4, 20–090 Lublin, Poland, lukasz.komsta@umlub.pl)

      J. Sep. Sci. 39, 4258-4262 (2016). TLC of 35 model compounds on RP-2, RP-8, RP-18, alumina, cellulose, cyano, diol, amino phase, and silica gel with 20 pure solvents (acetone, acetonitrile, 1-butanol, 1-chlorobutane, chloroform, cyclohexane, 1,2-dichloroethane, dichloromethane, dioxane, ethanol, ethyl acetate, heptane, hexane, methanol, isooctane, 1-propanol, 2-propanol, t-butyl methyl ketone, tetrahydrofuran, and toluene). Parallel factor analysis was used to study the retention phenomena in quantitative manner.

      Classification: 2c
      118 055
      Tabebuia roseoalba - in vivo hypouricemic and anti-inflammatory effects of its ethanolic extract and constituents
      Zilma Schimith FERRAZ-FILHA, Marcela Carolina de PAULA MICHEL ARAÚJO, Fernanda Cristina FERRARI, Iális Paiva Andrade RODRIGUES DUTRA, Dênia Antunes SAÚDE-GUIMARÃES* (*School of Pharmacy, Federal University of Ouro Preto, Ouro Preto, Minas Gerais, Brazil; saudeguima@gmail.com)

      Planta Medica 82 (16), 1395-1402 (2016). The hexane – ethyl acetate subfraction of the ethyl acetate fraction of an ethanolic Tabebuia roseoalba leaf percolation extract was subfractioned on a silica gel column with 42500 mL of a gradient of hexane, ethyl acetate, and methanol. For monitoring, TLC on silica gel with hexane – ethyl acetate 1:1, detection with anisaldehyde sulfuric acid reagent. Two fractions that gave only one visible zone on TLC, were identified by NMR as mixtures of stigmasterol and sitosterol, and of alpha- and beta-amyrins, respectively.

      Classification: 13c, 15a, 32e
      118 080
      Determination of dantrolene sodium in the presence of its process-related impurity by high-performance thin-layer chromatography–spectrodensitometry
      N.S. ABDELWAHAB, M.T. ELSAADY, A.G. KORANY*, M.A. HGAZY (*Medicinal Chemistry, Faculty of Pharmacy, Beni-Suef University, Beni-Suef, Egypt, Amalgaber1989@gmail.com)

      J. Planar Chromatogr. 29, 462-468 (2016). HPTLC of dantrolene sodium (1) and its process-related impurity 5-(4-nitrophenyl)-2-furaldehyde (2) on silica gel with chloroform – ethyl acetate – glacial acetic acid 1000:500:1. Quantitative determination by absorbance measurement at 380 nm. The hRF values for (1) and (2) were 22 and 83, respectively. Linearity ranged between 100-1500 ng/zone for (1) and 100-2000 ng/zone for (2). The intermediate precisions were below 0.3 % (n=3). The LODs and LOQs were 33 and 99 ng/zone for (1) and 32 and 96 ng/zone for (2), respectively. Average recoveries were 99.5 % for (1) and 100.2 % for (2).

      Classification: 32a
      119 009
      Chromatographic behavior of selected dyes on silica and cellulose micro-TLC plates – Potential application as target substances for extraction, chromatographic, and/or microfluidic systems
      E. WLODARCZYK, P. ZARZYCKI (*Department of Environmental Technologies and Bioanalytics, Faculty of Civil Engineering, Environmental, and Geodetic Sciences, Koszalin University of Technology, Koszalin, Poland, pkzarz@wp.pl)

      J. Liq. Chromatogr. Relat. Technol. 40, 259-281 (2017). Research communication on chromatographic properties of 18 colorants including amaranth, black PN, bromophenol blue, bromocresol green, bromocresol purple, bromothymol blue, carmine, dimethyl yellow, erythrosine, fluorescein, methyl red, naphthalene black, patent blue, phenol red, Sudan II, Sudan III, Sudan IV, and p-xylenol blue. The paper presents a comprehensive retention database for designing 1D and 2D planar separations systems.

      Classification: 1, 30a
      119 050
      Simultaneous quantification of carbohydrates and metabolites in multicomponent fermentation broths by means of high-performance thin-layer chromatography
      S. COSTA, I. RUGIERO, P. PEDRINI, T. BERNADI, Elena TAMBURINI* (*Department of Life Science and Biotechnology, University of Ferrara, via L. Borsari, 46, 44121 Ferrara,
      Italy, tme@unife.it)

      J. Planar Chromatogr. 30, 170-174 (2017). HPTLC-overpressured layer chromatography of monosaccharides (glucose, xylose, rhamnose, and arabinose) as substrates and sugar alcohols (xylitol, sorbitol and arabitol) as metabolites, to follow the fermentation of the yeast Candida tropicalis DSM 7524 on silica gel with acetonitrile – acetic acid – water 63:33:5. Detection by dipping for 9 s into a reagent containing 5 mL of solution I (2 % basic acetate of lead (IV) in glacial acetic acid) and 5 mL of solution II (0.2 % 2,7-dichlorofluorescein in 100 mL ethanol) made up to 200 mL with toluene, followed by heating at 105 °C for 3 min. Quantitative determination by absorbance measurement at 366 nm.

      Classification: 10a
      119 075
      Separation of a mixture of eleven alkaloids by 2D-TLC on multi-K CS5 plates and identification of analytes in Thalictrum foetidum root extract by TLC and HPLC–DAD
      T. TUZIMSKI*, Anna PETRUCZYNIK, Justyna MISIUREK (*Department of Physical Chemistry, Chair of Chemistry, Medical University in Lublin, 4a, Chodzki Street, 20-093 Lublin, Poland, tomasz.tuzimski@umlub.pl)

      J. Planar Chromatogr. 30, 142-147 (2017). 2D-HPTLC of eleven alkaloids: allocryptopine (1), berberine (2), boldine (3), chelidonine (4), glaucine (5), papaverine (6), emetine (7), columbamine (8), magnoflorine (9), palmatine (10), and coptisine (11) on bilayer Multi-K CS5 with methanol – water 4:1 containing 0.05 mL (volume not clear) diethylamine in the first dimension, followed by drying at 110 ºC for 40 min and developing in the second dimension with methanol – acetone – diisopropyl ether – ammonia 18:18:63:1. Quantitative determination at UV 366 nm. The LOD and LOQ were 25 and 63 μg/zone for (2), 14 and 42 μg/zone for (9).

      Classification: 22
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