Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

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      107 067
      Thin-layer chromatographic method for the determination of ternary mixture containing salbutamol sulphate, bromhexine hydrochloride and etofylline
      H. DAVE*, Rajeshree MASHRU, A. PATEL (*Centre of Relevance and Excellence in Novel Drug Delivery Systems, Pharmacy Dept., G. H. Patel Bldg., Dono’s Plaza, The M. S. University, Baroda, Fatehgung, Vadodara, Gujarat, India 390002, India, rajshreemashru_msu@yahoo.com)

      J. Pharm. Sci. & Res. 2(2), 143-148 (2010). TLC of salbutamol sulphate (SS), bromhexine hydrochloride (BH), and etofylline (ET) in fixed dose formulation on hand-made silica gel plates with methanol – n-hexane 2:1. All three compounds were well separated with hRf values of 25 for SS, 71 for ET and 91 for BH. Detection at 254 nm as well as by exposure to iodine vapors. For spectophotometric quantification the bands of the selected drug in sample and standard mixture were scraped off, suspended in methanol, and the absorbance was measured at the maximum absorbance wavelength of each compound.

      Classification: 17a
      107 086
      Simultaneous estimation of risperidone and trihexyphenidyl hydrochloride in tablets by HPTLC
      Kranti MALPURI*, S. YAMUNA, R. VIJAYAGEETHA, Shantha ARCOT (*Final year B. Pharmacy, Faculty C. L. Baid Matha College of Pharmacy Chennai, India)

      62nd Indian Pharmaceutical Congress Abstract No. F-249 (2010). TLC of risperidone and trihexyphenidyl hydrochloride on silica gel with methanol – chloroform – glacial acetic acid 160:40:0.1. Quantitative determination by absorbance measurement at 254 nm. The linearity was in the range of 20-60 µg/band and 10-30 µg/band for risperidone and trihexyphenidyl hydrochloride, respectively. The recovery was 99.4-99.9 % for both drugs.

      Classification: 23e
      107 109
      Application of a stability-indicating HPTLC method for quantitative analysis of amtolmetin guacil in a pharmaceutical dosage form
      V.K. BHUSARI*, M.V. MAHADIK, S.R. DHANESHWAR (*Bharati Vidyapeeth Univ., Poona Coll. of Pharm., Dep. of Pharm. Chem., Pune, Maharashtra, India 411038)

      Acta Chromatographica 21(2), 299-317 (2009). HPTLC of amtolmetin guacil on silica gel with toluene – ethyl acetate 2:3. Identification and quantification by densitometric analysis in absorbance mode at 320 nm. The samples were subjected to acidic and alkaline hydrolysis, oxidation, dry heat treatment, and photo-degradation. The method was suitable for stability studies and to study the kinetics of degradation of amtolmetin guacil.

      Classification: 32c
      107 129
      Simultaneous HPTLC analysis of aspirin, atorvastatin calcium and clopidogrel bisulphate in the bulk drug and in capsules
      S.V. LONDHE*, S.V. MULGUND, R.S. DESHMUKH, K. S. JAIN (*Sinhgad College of Pharmacy, Dep. of Pharm. Chem., Vadgaon, Pune 411041, India)

      Acta Chromatographica 22 (2), 297-305 (2010). Description of a simple, precise, and accurate method for simultaneous quantification of aspirin, atorvastatin calcium and clopidogrel bisulphate by HPTLC on silica gel with toluene – methanol - formic acid 65:35:1. The hRf values were 26, 47, and 78 for aspirin, atorvastatin calcium, and clopidogrel bisulphate, respectively. Quantification by densitometry at 254 nm. The precision intra-day and inter-day was in the ranges of 0.2–0.7 %RSD and 0.5–1.0 %RSD for aspirin, 0.4–0.9 %RSD and 0.4–0.6 %RSD for atorvastatin calcium, and 0.3–0.7 %RSD and 0.4–0.9 %RSD for clopidogrel bisulphate.

      Classification: 32e
      107 150
      (Study of the quality standard for Cishushi suppository) (Chinese)
      X. WEN* (Wen Xianmin), M. YANG (Yang Miannan) (*Res. Cent. of Natural Drugs, Yunnan Mingyang Pharm. Co., Kunming 650200, China)

      Yunan J. of Chinese Trad. Med. & Pharm. 31(10), 58-60 (2010). TLC of extracts of Cishushi suppository: 1) for Panax notoginseng, on silica gel with chloroform – methanol – water 14:6:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 ºC; 2) for Fructus Cnidii, on silica gel with petroleum ether (60-90 °C) – ethyl acetate 7:3, detection under UV 366 nm; 3) for Borneolum Syntheticum, on silica gel with toluene – ethyl acetate 19:1, detection by spraying with 5 % vanillin-sulfuric acid reagent and heating at 105 °C; 4) for Fructus Sophorae, on silica gel with chloroform – methanol – water – formic acid 700:300:50:1, detection by spraying with 1 % AlCl3 in ethanol, heating and evaluation under UV 366 nm.

      Classification: 32e
      108 025
      Spectrodensitometric evaluation and determination of fluconazole and its impurities in pharmaceutical formulation by high-performance thin-layer chromatography
      B. RAMESH, P. NARAYANA, A. REDDY, P. DEVI (*Analytical Chemistry Div, Indian Institute of Chemical Technology, Tarnaka, Hyderabad, (A.P.), India)

      Journal of Pharmacy Research 4(5), 1401-1404 (2011). HPTLC of fluconazole and its structurally related impurities, on silica gel (prewashed with methanol) with n-butanol - water - acetic acid 8:2:1 with chamber saturation for 20 min. The hRf value of fluconazole was 67 and of the two separated impurities 49 (impurity B) and 79 (impurity E). Quantitative determination by densitometry in absorbance mode at 254 nm. The method was linear in the range of 1-6 µg/band for fluconazole and 0.5-2.5 µg/band for both impurities.

      Classification: 6
      108 050
      HPTLC estimation of nateglinide in bulk drug and tablet dosage form
      D. KALE*, R. KAKDE (*Dept. of Pharmaceutical Sciences, R.T.M. Nagpur University, Amravati Rd., Nagpur, India)

      Asian Journal of Chemistry 23(10), 4351-4354 (2011). HPTLC of nateglinide in tablet dosage form on silica gel with n-hexane - methanol - isopropanol 75:15:10. The hRf value was 56. Quantitative evaluation by absorbance measurement at 210 nm. The method was linear in the range of 300-1000 ng/band. The average recovery was 98.5 %.

      Classification: 17a
      108 081
      Application of hydrophilic interaction TLC systems for separation of high polar glycoside compounds from the flowers of selected Verbascum species
      L. CIESLA. M. HAJNOS, Monika WAKSMUNDZKA-HAJNOS* (*Department of Inorganic Chemeistry, Medical University of Lublin, 4a Chodzki St., 20-093 Lublin, Poland; monika.hajnos@am.lublin.pl)

      J. Planar Chromatogr. 24, 295-300 (2011). TLC of Verbascum extracts (e. g. iridoids, and triterpene saponins) on silica gel in a horizontal chamber saturated with mobile phase for 10 min, by 2D separation with ethyl acetate - methanol - water 25 % ammonia 55:35:9:1 in the first direction and methanol - ethyl acetate - water - acetic acid 5:45:13:11 in a perpendicular direction. Detection by dipping in vanillin-sulfuric acid reagent for 1 s followed by heating for 10 min at 105 °C. The method was validated for its specifity, precision (repeatability and intermediate precision), stability, and robustness. Use of an image-processing program for the construction of an ’average’ fingerprint.

      Classification: 32e
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