Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      125 057
      Application of analytical quality by design approach in method development for the simultaneous estimation of levocetrizine hydrochloride and montelukast sodium in their combined dosage form
      Jina DESAI*, P. DEDHIYA, H. PATEL, A. MISHRA, S. SHAH (*Maliba Pharmacy College, Uka Tarsadia University, Maliba Campus, Gopal Vidyanagar, Bardoli, Gujarat 394350, India, prafuldedhiya@gmail.com)

      J. Planar Chromatogr. 33, 119-129 (2020). HPTLC of levocetrizine hydrochloride (1) and montelukast sodium (2) on silica gel with ethyl acetate - methanol - triethylamine 125:125:1. Quantitative determination by absorbance measurement at 234 nm. The hRF values for (1) and (2) were 23 and 55, respectively. Linearity was between 100 and 500 ng/zone for (1) and 200 and 1000 ng/zone for (2). Intermediate precisions were below 2 % (n=3). The LOD and LOQ were 9 and 28 ng/zone for (1) and 22 and 65 ng/zone for (2), respectively. Recovery rate was between 99.3 and 100.1 % for (1) and 100.0 and 100.3 % for (2).

      Classification: 32a
      125 056
      Effect of superfine pulverization technology on the determination of vitamin C content in Fructus rosae laxae
      J. SUN (Sun Jing)*, A. ZHANG (Zhang Airong), N. WANG (Wang Ning), L. TIAN (Tian Li)* (*College of Traditional Chinese Medicine, Xinjiang Medical University, Urumqi 830011, Xinjiang, China, tianli109@126.com)

      J. Planar Chromatogr. 33, 79-87 (2020). HPTLC of vitamin C in the dried fruit of Rosa laxa on silica gel with ethyl acetate - absolute ethanol - water 40:24:15. Quantitative determination by absorbance measurement at 273 nm. The hRF value for vitamin C was 61. Linearity was between 0.25 and 1.2 µg/zone. Intermediate precisions were below 2 % (n=6). Average recovery was 98.4 %.

       

      Classification: 27, 32e
      125 005
      Densitometric simultaneous estimation of combination of empagliflozin, linagliptin and metformin hydrochloride used in the treatment of type 2 diabetes mellitus
      I. PATEL*, U. CHHALOTIYA*, H. JANI, D. KANSARA, D. SHAH (*Department of Pharmaceutical Chemistry and Analysis, Indukaka Ipcowala College of Pharmacy, Beyond GIDC, P.B. No. 53, Vitthal Udyognagar, Gujarat 388121, India, usmangani84@gmail.com)

      J. Planar Chromatogr. 33, 109-118 (2020). HPTLC of empagliflozin (1), linagliptin (2) and metformin hydrochloride (3) on silica gel with n-butanol - water - glacial acetic acid 6:3:1. Quantitative determination by absorbance measurement at 223 nm. The hRF values for (1) to (3) were 73, 52 and 33, respectively. Linearity was between 0.1-0.7 µg/zone for (1), 0.05-0.35 µg/zone for (2) and 10-70 µg/zone for (3). Intermediate precisions were below 2 % (n=3). The LOD and LOQ were 2 and 5 µg/zone for (1), 9 and 27 ng/zone for (2) and 19 and 59 ng/zone for (3), respectively. Recovery was between 99.4 and 100.7 % for (1), 99.3 and 100.5 % for (2) and 98.6 and 101.8 % for (3).

      Classification: 32a
      125 003
      A simple, rapid and sensitive high-performance thin-layer chromatographic method for the simultaneous estimation of berberine and 5-fluorouracil in rabbit plasma
      P. TAMANE*, R. PAI, V. POKHARKAR (*Department of Drug Regulatory Affairs, Bharati Vidyapeeth (Deemed to be) University, Poona College of Pharmacy, Erandwane, Pune, Maharashtra 411038, India, varsha.pokharkar@bharatividyapeeth.edu)

      J. Planar Chromatogr. 33, 169-177 (2020). HPTLC of berberine (1) and 5-fluorouracil (2) in rabbit plasma on silica gel with toluene - methanol - ethyl acetate - formic acid 6:2:6:1. Quantitative determination by absorbance measurement at 266 nm. The hRF values for (1) and (2) were 28 and 57, respectively. Linearity was between 20 and 300 ng/zone for both (1) and (2). Intermediate precisions were below 7 % (n=3). The LOQ was 29 ng/zone for (1) and 26 ng/zone for (2), respectively. Average recovery was 86.5 % for (1) and 87.2 % for (2).

      Classification: 32c
      125 055
      Thin-layer chromatographic enantioseparation of atenolol and propranolol using (S)-naproxen as chiral selector: direct and indirect approaches
      V. VASHISTHA, R. BHUSHAN* (*Department of Chemistry, GLA University, Mathura, Uttar Pradesh 281406, India, rbushfcy54@gmail.com)

      J. Planar Chromatogr. 33, 101-107 (2020). HPTLC of (RS)-atenolol and (RS)-propranolol on silica gel  impregnated with 50 mM (S)-naproxen as chiral selector with acetonitrile - dichloromethane - water 6:2:1 pH = 5 for (RS)-atenolol and 7:3:1 pH = 5 for (RS)-propanolol. Detection by exposure to iodine vapor. The LOD was 1.2 and 1.6 µg/mL for (1) and (2), respectively. The chiral selector allowed the separation of atenolol and propranolol with a resolution of 2.4.

      Classification: 38
      125 054
      Stability-indicating HPTLC method development for determination of arterolane maleate and piperaquine phosphate in combined dosage form
      S. GAILKWAD, A. BANSODE, N. PATADE, S. TATHE (*Department of Pharmaceutical Chemistry, Sinhgad Institute of Pharmacy, Narhe, Pune, Maharashtra 411041, India, shubhangi_pharma@rediffmail.com)

      J. Planar Chromatogr. 33, 131-139 (2020). HPTLC of arterolane maleate (1) and piperaquine phosphate (2) on silica gel with isopropyl alcohol - n-butanol - methanol - triethylamine 15:30:5:1. Quantitative determination by absorbance measurement at 232 nm. The hRF values for (1) and (2) were 64 and 18, respectively. Linearity was 150-900 ng/zone for (1) and 750-4500 ng/zone for (2). Intermediate precisions were below 2 % (n=6). The LOD and LOQ were 6 and 18 mg/zone for (1) and 23 and 70 ng/zone for (2), respectively. Mean recovery rate was 98.9 and 103.9 % for (2).

      Classification: 32a
      125 052
      A new thin-layer chromatography–direct bioautography assay for the qualitative and quantitative determination of peroxidase inhibitors in plant extracts
      R. DARWISH, E. SHAWKY, H. HAMMODA, F. HARRAZ (*Department of Pharmacognosy, Faculty of Pharmacy, Alkhartoom square, Alexandria University, Alexandria 21521, Egypt, eman.m.shawky@alexu.edu.eg)

      J. Planar Chromatogr. 33, 79-87 (2020). HPTLC of quercetin in the aerial parts of Juniperus communis, J. horizontalis and J. chinensis on silica gel with ethyl acetate - methanol - water - acetic acid 900:80:40:7. Assessment of peroxidase inhibition activity by dipping into peroxidase enzyme solution (10 mg/mL solution of peroxidase in cold phosphate buffer (pH 7), followed by dilution with 50 mL of phosphate buffer, pH 7) for 3 s, followed by heating at 35 ºC for 2 min, dipping into a hydrogen peroxide solution and finally dipping into a benzidine solution (4 g in 700 mL methanol). Linearity was between 0.85 and 9 µg/zone for quercetin. Intermediate precisions were below 3 % (n=3). The LOD and LOQ were 280 and 850 ng/zone. Recovery was between 96.6 and 99.7 %.

       

      Classification: 8a
      125 051
      Simultaneous identification of rutin, chlorogenic acid and gallic acid in Moringa oleifera by densitometric high-performance thin-layer chromatography method
      P. ALAM*, P. ALAM, M. SHARAF-ELDIN, M. ALQAMI (*Department of Biology, Sara Alghonaim Research Chair (SRC), College of Science and Humanities, Prince Sattam bin Abdulaziz University (PSAU), Alkharj 11942, Saudi Arabia, alamprez@gmail.com)

      J. Planar Chromatogr. 33, 27-32 (2020). HPTLC of rutin (1), chlorogenic acid (2) and gallic acid (3) in the seeds of Moringa oleifera on silica gel with ethyl acetate - acetone - water - formic acid 6:3:2:2. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (3) were 51, 72 and 83, respectively. Linearity was between 1000 and 7000 ng/zone for (1), 100 and 700 ng/zone for both (2) and (3). Intermediate precisions were below 1 % (n=6). The LOD and LOQ were 5 and 17 ng/mL for (1), 7 and 22 ng/mL for (2) and 7 and 20 ng/mL for (3), respectively. Recovery rate was between 98.1 and 99.5 % for (1), 98.8 and 99.5 % for (2) and 97.6 and 98.6 % for (3).

      Classification: 8a
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