Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      111 082
      HPTLC method for analysis of sertraline in pure bulk and lipidic nano delivery system
      A. HUSSAIN, M. RAHMAN*, M. HUSSAIN, M. MIRZA, Z. IQBAL, R. HARWANSH, L. RATNAKAR (*Faculty of Pharmacy, Integral University, Kursi Road, Lucknow-226026, India, rahmanpharma@gmail.com)

      J. Liq. Chromatogr. Relat. Technol. 36, 700-716 (2013). HPTLC of sertraline in bulk and formulation on silica gel with toulene - ethyl acetate 1:5+1 drop ammonia. Quantitative determination by absorbance measurement at 273 nm. The hRf value of sertraline was 70. Linearity was in the range of 25-2000 ng/zone. LOD and LOQ were 15.3 and 46.8 ng/zone. Intermediate precision was below 0.83 %. Recovery range was in the range of 99.6-100.3 %. The hRf values of acid and base-induced degradation products were 40, 52, 90 and 25.

      Classification: 32a
      111 100
      (Study of the method for the quality control of Jiegu Xujin capsules by thin-layer chromatography) (Chinese)
      F. LIAO (Liao Fang)*, D. ZHANG (Zhang Dan), M. LI (Li Min), CH. LI (Li Chunlin), M. LAN (Lan Minghui), R. YIN (Yin Rongli) (*Chengdu Municip. Xindu District Hosp. of Trad Chinese Med., Sichuan, Chengdu 610500, China)

      Jiangxi J. of Trad. Chinese Med. 43 (354), 62-64 (2012). Jiegu Xujin capsules are a herbal TCM for the treatment of fractures, bone dislocation and joint pain. For quality control, TLC on silica gel 1) for Rhizoma Drynariae and the standard naringin, with cyclohexane – ethyl acetate – formic acid – water 2:24:5:6, detection under UV 366 nm; 2) for Radix Angelicae Sinensis and Rhizoma Ligustici Chuanxiong, with n-hexane – ethyl acetate 9:1, detection under UV 366 nm; 3) for Eupolyphaga seu steleophaga, with toluene – dichloromethane – acetone 10:10:1, detection by spraying with 3 % vanillin in sulfuric acid – ethanol 1:200 and heat at 105 °C, viewing in daylight; 4) for Radix Notoginseng and the standards ginsenoside Rb1, Re, Rg1, R1, with the lower phase of chloroform – methanol – water 13:7:2, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing under UV 366 nm.

      Classification: 32e
      111 118
      Quantification and side component analysis of the cosmetic active tiliroside using planar chromatography
      M. SCHULZ*, Susanne MINARIK, Michaela OBERLE, Sylvia EISENBERG (*Merck KGaA, MM-LER-CP. Frankfurterstr. 250, 64293 Darmstadt, Germany, michael.schulz@merckgroup.com)

      CBS 107, 11-12 (2011) HPTLC of tiliroside (a cosmetic active obtained by extraction from a plant of the family Sterculiaceae) and side components kaempferol-3-glucoside, kaempferol-3-rutinoside, kaempferol, and coumaric acid on silica gel with ethyl acetate - formic acid - acetic acid- water 100:11:11:27 + 1% heptane. Detection under UV 366 nm after spraying with natural products reagent (1 % diphenylborinic acid 2-aminoethylester in methanol) and under white light after spraying with anisaldehyde sulfuric acid reagent (0.5 mL anisaldehyde in 85 mL methanol with 10 mL acetic acid and 8 mL conc. sulfuric acid) and heating at 90-125 °C for 15 min. Quantitative absorption measurement of tiliroside at 315 nm using a 4-point calibration via peak area. The tiliroside contents in the sample extracts were determined as: 1 = 1.09 µg (RSD = 0.4 %), 2 = 0.93 µg (RSD = 0.8 %), 3 = 1.19 µg (RSD = 1.2 %) and 4 = 3.32 µg (RSD = 0.3 %). During the side component analysis no kaempferol, coumaric acid, and glucose were detected in the tiliroside samples. Small amounts of kaempferol-3-glucoside and kaempferol-3-rutinoside were found. HPTLC covers several tasks: quantification of the active ingredient in a complex plant matrix for determining the quality of the raw material, in-process control for monitoring the impurity profile during the manufacturing process and the quantification of the active ingredient in the final product.

      Classification: 32e
      111 136
      Simultaneous densitometric determination of hydrocortisone acetate and 2-phenoxyethanol in creams
      D. WIDIRETANI, I. LUAILIA, G. INDRAYANTO* (*Section Analytical Development, Department R & D, Bernofarm Pharmaceutical Company, Sidoarjo, Indonesia; and G. Indrayanto, Faculty of Pharmacy, Airlangga University, Dharmawangsa dalam, Surabaya 60286, Indonesia, gunawanindrayanto@yahoo.com)

      J. Planar Chromatogr. 26, 37-42 (2013). HPTLC of hydrocortisone acetate (1) and 2-phenoxyethanol (2) in cream on RP-18 with water-methanol 4:11. Quantitative determination by absorbance measurement at 270 nm. Linearity was in the range of 4.2-13.0 µg/zone for (1) and 0.8-4.3 µg/zone for (2). LOD and LOQ were 0.6 and 1.7 µg/zone for (1) and 0.2 and 0.5 µg/zone for (2), respectively. Intermediate precision was below 2 %.

      Classification: 32a
      111 152
      (Study of a method for the quality control of Kuanzhong Laokou pills by thin-layer chromatography) (Chinese)
      X. ZHAO (Zhao Xin)*, X. LI (Li Xianyi), P. ZHANG (Zhang Peng) (*Inst. for Drug & Instr. Contr., Joint Logistics Dep., Shenyang Military Region, Chinese PLA, Liaoning, Shenyang 110026, China)

      Chinese J. of Lishizhen Trad. Med. & Pharm. 23 (2), 502-503 (2012). Kuanzhong Laokou pills are a herbal TCM for treating thoracic abdominal bloating and stomach pain. For quality control TLC on silica gel 1) for Rhizoma atractylodis macrocephalae, with petroleum ether (60-90 °C) – ethyl acetate 50:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:200 and heating mildly, viewing in daylight; 2) for Pericarpium citri reticulatae, with ethyl acetate – butanone – formic acid – water 7:2:1:1, detection by spraying with 1 % ferric chloride in ethanol and viewing under UV 366 nm; 3) for Radix aucklandiae, with cyclohexane - ethyl acetate 17:3, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:200 and heating mildly, viewing in daylight; 4) for Radix et rhizoma rhei, with petroleum ether (30-60 °C) – ethyl formate – formic acid 15:5:1, detection under UV 366 nm or by exposing to ammonia vapor and viewing in daylight.

      Classification: 32e
      112 032
      Development of a novel high-performance thin-layer chromatographic–densitometric method for the detection of tallow adulteration in cow ghee
      S. DE*, P. NARIYA, N. JIRANKALGIKAR (*RMD Research and Development Center, Waghaldhara, Valsad, India, subratde@gmail.com)

      J. Planar Chromatogr. 26, 486-490 (2013). HPTLC of tallow in cow ghee on silica gel with n-hexane - diethyl ether 2:3 + 1 drop glacial acetic acid for unsaponifiable fraction (1) and n-hexane - diethyl ether 13:7 + 1 drop glacial acetic acid for saponifiable fraction (2). Detection by spraying with 10% methanolic sulfuric acid reagent followed by heating at 110 ºC for 5-10 min. Zones at hRf values of 9 and 20 were identified as tallow concentration increased.

      Classification: 11c
      112 058
      New and selective HPTLC–densitometric method for determination of pioglitazone hydrochloride
      A. MOHAMED, F. MOHAMED, S. AHMED, Y. MOHAMED* (*Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Assiut University, Egypt, gadeedegypt2008@yahoo.com)

      J. Planar Chromatogr. 26, 209-214 (2013). HPTLC of pioglitazone hydrochloride on silica gel with chloroform - methanol 10:1. Detection by spraying with 0.5 % o-phthalaldehyde in ethanol, followed by heating at 70 ºC for 15 min. Quantitative determination by scanning with a flatbed scanner and a gel analysis software. Linearity was in the range of 200-3000 ng/zone. LOD and LOQ were 65 and 197 ng/zone, respectively. Recovery was in the range of 98-102 %. Intermediate/interday/intra-day precision was below 2 %.

      Classification: 23e
      112 083
      (Study on the method for the quality control of Shengma Gegen granules) (Chinese)
      Q. HU (Hu Qing)*, J LI (Li Jianhua), Q. SHEN (Shen Qingliang) (*Henan Hosp. of China Armed Police Forces, Henan, Zhengzhou 450052, China)

      J. of Chinese Med. 26 (169), 716-718 (2012). Shengma Gegen granules are a herbal TCM preparation for the treatment of viral hepatitis type C, drug-induced liver diseases, and postherpetic neuralgia. For quality control, TLC on silica gel 1) for Rhizoma Cimicifugae, with benzene – chloroform – glacial acetic acid 12:2:1, detection under UV 366 nm; 2) for Radix Paeoniae Rubra, with chloroform – ethyl acetate – methanol – formic acid 200:25:50:1, detection by spraying with 2 % vanillin in sulfuric acid – ethanol 1:200 and heating mildly until the zones are visible in daylight. Quantification of puerarin by HPLC.

      Classification: 32e
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