Cumulative CAMAG Bibliography Service CCBS
Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.
The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:
- Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
- Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
- Keyword register: select an initial character and browse associated keywords
- Search by CBS edition: Select a CBS edition and find all related publications
Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.
J. Planar Chromatogr. 27, 438-443 (2014). HPTLC of (1) alpha-amyrin, (2) lupeol, and (3) beta-sitosterol in the leaves of Kalanchoe pinnata, Bombax ceiba, and Morus alba on silica gel with toluene – ethyl acetate 19:1. Detection by dipping into anisaldehyde–sulphuric acid reagent for 1 min, followed by heating at 100 °C for 5 min. Quantitative determination by absorbance measurement at 525 nm. The hRF values of (1) to (3) were 71, 28 and 16 respectively. Linearities were in the range of 160-560 ng/zone for (1), 150-900 ng/zone for (2) and 80-480 ng/zone for (3). The intermediate precision was below 2 % (n=3) for (1) to (3). The LOD and LOQ were 60 and 160 ng/zone for (1), 50 and 150 ng/zone for (2) and 20 and 48 ng/zone for (3), respectively. Average recoveries for (1) to (3) were 100.7, 99.8 and 100.1 %, respectively.
Chinese J. Sci. & Technol. Review 17, 220-221 (2013). Zhihe Piba Keli pill is a TCM compound for the treatment of cough. For quality control, microemulsion TLC of Stemona sessilifolia (Miq.) Miq., Morus alba L. and Cynanchum glaucescens (Decne.) Hand.-Mazz on polyamide thin-films with (SDS - n-butanol – n-heptane 2.7:6.3:1.0) – formic acid 9:1, detection at UV 366 nm. Demonstration by applying to real life samples indicated that the procedure was suited for quality control.
J. Planar Chromatogr. 27, 346-356 (2014). HPTLC fingerprint of the leaves of Arctium lappa and Fagus sylvatica, herba of Epilobium hirsutum, Lythrum salicaria, and Artemisia dracunculoides; and fruits of Cydonia oblonga and leaves of Hippophae rhamnoides and Aronia melanocarpa on silica gel with ethyl acetate – acetic acid – formic acid – water 50:6:6:13 for flavonoid glycosides and chloroform – acetic acid – methanol – water 16:8:3:2 for saponins. Detection by immersion into natural product reagent followed by PEG 400 reagent. Qualitative identification at UV 366 nm.
J. Liq. Chromatogr. Relat. Technol. 38, 1113-1120 (2015). HPTLC of orbifloxacin (1), danofloxacin (2), ciprofloxacin (3), norfloxacin (4), enrofloxacin (5), marbofloxacin (6), difloxacin (7) and ofloxacin (8) on silica gel with 1,4-dioxane - ammonia - tetrahydrofuran 6:3:2. Quantitative determination by absorbance measurement at 320 nm. The hRF value was 19 for (4), 23 for (3), 30 for (2), 37 for (8), 40 for (6), 44 for (5), 56 for (1) and 59 for (7). Linearity was in the range of 159-513 ng/zone for (1), 99-238 ng/zone for (2), 97-244 ng/zone for (3), 69-163 ng/zone for (4), 63-170 ng/zone for (5), 103-250 ng/zone for (6), 84-251 ng/zone for (7) and 94-260 ng/zone for (8). LOD and LOQ were 53 and 159 ng/zone for (1), 32 and 98 ng/zone for (2), 32 and 97 ng/zone for (3), 23 and 69 ng/zone for (4), 21 and 63 ng/zone for (5), 34 and 103 ng/zone for (6), 28 and 84 ng/zone for (7) and 31 and 94 ng/zone for (8), respectively. Selection of appropriate viscosity of the mobile phase may be important in obtaining optimal chromatographic separation.
chromatography-densitometry
J. Planar Chromatogr. 28, 287-293 (2015). HPTLC of bacoside A in the leaves of Bacopa monnieri on silica gel with ethyl acetate - methanol - water 4:1:1. Detection by spraying with 1 % vanillin in 10 % methanolic sulfuric acid. Quantitative determination by absorbance measurement at 598 nm. The hRF value for bacoside A was 53. LOD and LOQ were 60 and 180 ng/zone, respectively. The intermediate precision was below 1 % (n=3). Recovery ranged between 97 and 100 %.
Trends Anal. Chem. 69, 114-122 (2015). The review discusses methods for the identification of bulk drugs and the active ingredients in formulations. The paper describes a general scheme for the profiling of related organic impurities in drugs involving the use of chromatographic techniques, including TLC.
J. Planar Chromatogr. 28, 380-385 (2015). HPTLC of taurocholic acid (1), glycodeoxycholic acid (2) and taurodeoxycholic acid (3) in ten Thai edible plants on silica gel with chloroform - methanol - acetic acid 7:2:1. Quantitative determination by absorbance measurement at 366 nm. Linearity was in the range of 34-2200 ng/zone for (1), 33-2100 ng/zone for (2) and 30-1900 ng/zone for (3). LOD and LOQ were 10 and 50 ng/zone for (1), 20 and 40 ng/zone for (2) and 10 and 50 ng/zone for (3). The intermediate precision was below 1.2 % (n=6). Average recovery for (1) to (3) was 99, 100 and 100 %, respectively.
J. Planar Chromatogr. 28, 354-361 (2015). TLC of rosuvastatin (1) and fenofibrate (2), rosuvastatin (1) and ezetimibe (3) and rosuvastatin (1) and aspirin (4) (in three different pharmaceutical combination products) on silica gel with toluene - acetone - acetic acid 30:10:1. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) to (4) were 19, 83, 43 and 53, respectively. Linearity was in the range of 500-4000 ng/zone for all four drugs. LOD and LOQ were 77 and 234 ng/zone for (1), 38 and 116 ng/zone for (2), 108 and 327 ng/zone for (3) and 144 and 438 ng/zone for (4), respectively. The intermediate precision was below 1 % (n=3). Average recovery ranged between 98.9 and 99.4 % for (1) to (4).