Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

Page
      122 053
      High-performance thin-layer chromatography-direct bioautography as a method of choice for alpha-amylase and antioxidant activity evaluation in marine algae
      Snezana AGATONOVIC-KUSTRIN*, D.W. MORTON (*School of Pharmacy, Monash University Malaysia, Jalan Lagoon Selatan, Bandar Sunway, 47500, Selangor Darul Ehsan, Malaysia)

      J. Chromatogr. A 1530, 197-203 (2017). Evaluation of the phenolic and stigmasterol content and comparison of the antioxidant and antidiabetic activities by HPTLC combined with DPPH* free radical method and α-amylase assay towards ethanol and ethyl acetate extracts of 10 marine macroalgae species (3 chlorophyta, 4 phaeophyta and 3 rhodophyta). HPTLC on silica gel with n-hexane – ethyl acetate – acetic acid 20:9:1 over 80 mm. Detection either by dipping into 0.4 % DPPH* solution followed by storing in the dark for 30 min before evaluation, or by dipping into anisaldehyde – sulfuric acid reagent or neutralized ferric chloride solution (prepared by adding dilute sodium hydroxide to freshly prepared 2 % ferric chloride in methanol until precipitation occurs, followed by filtering), both followed by heating at 100 °C for 10 min. Quantitative evaluation by absorbance measurement at 470 nm for detection of α-amylase inhibition and at 550 nm for stigmasterol. The results showed higher antioxidant activity in the ethyl acetate extracts than in ethanol extracts, and higher amounts of fucoxanthin, stigmasterol and α-amylase inhibitory activities in ethyl acetate extracts. The results proved the relation of higher α-amylase inhibition in ethyl acetate extracts due to the presence of triterpenes and sterols, and no contribution of fucoxanthin to it.

      Classification: 13c, 15a
      122 073
      Simultaneous densitometric determination of eight food colors and four sweeteners in candies, jellies, beverages and pharmaceuticals by normal-phase high performance thin-layer chromatography using a single elution protocol
      A.P. NAMBIAR, M. SANYAL, P.S. SHRIVASTAV* (*Dep. of Chem., School of Sci., Gujarat Univ., Ahmedabad, 380009, Gujarat, India, pranav_shrivastav@yahoo.com)

      J. Chromatogr. A 1572, 152-161 (2018). Description of a novel application of HPTLC for separation and quantification of eight food colors (amaranth, allura red, erythrosine, fast green, indigo carmine, quinoline yellow, sunset yellow and tartrazine) and four intense sweeteners (acesulfame, aspartame, saccharin and neohesperidin) on silica gel with acetonitrile – water - ethyl acetate - 10 % aqueous ammonia 9:1:1:1. Quantitative determination by densitometry at 210, 295, 450 and 550 nm. The LOD and LOQ ranged from 0.2 to 10 ng/zone and from 1 to 30 ng/zone, respectively. The correlation coefficient (r2) values for the calibration curves were ≥ 0.9973 for all the additives. The recovery of different additives obtained from food products, beverages and pharmaceuticals ranged from 96.6 to 106.7 %.

      Classification: 30
      55 054
      Quantitative determination of biologically active constituents in crude extracts of medicinal plants by thin-layer chromatography-densitometry
      M. VANHAELEN, R. VANHAELEN-PASTRE

      II. Eleutherococcus senticosus maxim, panax ginseng Meyer and picrorrhiza kurroa Royle. J. Chromatogr. 312, 497-503 (1984). HPTLC of the title compound on silica with 1,2-dichloroethane - ethanol -methanol -water 65:22:22:7. Detection with a mixture (1:1) of 1 % vanillin in ethanol and 5 % sulfuric acid in ethanol. Densitometry at 530 nm after color stabilization (5 min.). The same method gave excellent results for the analysis of crude ginseng extracts. Also HPTLC of picrorrhiza kurroa extracts with dichloromethane-methanol - water 40:10:1. Detection at 268 and 285 nm. Precise and accurate HPTLC-densitometry method for the standardization of plant drugs.

      Classification: 14, 32e
      57 009
      Measurement of lipophilicity by GLC
      E. JANOS, T. CSERHATI

      V. Danube Symposium on Chromatography, Yalta, November 11-16, 1985. TLC on silica, impregnated with 5 % paraffin oil in hexane, developed with methanol - water with different organic phase ratio in the mobile phase.

      Classification: 2c
      58 082
      Resolution of optical isomers by TLC - Enantiomeric purity of L-DOPA
      K. GUENTHER, J. MARTENS, M. SCHICKEDANZ

      Fresenius Z. Anal. Chem. 322, 513-514 (1985). Proof of enantiomeric purity by TLC of D- and L- (3, 4-dihydroxyphenylalanine) on MN-chiral plates with methanol -water - acetonitrile 5:5:3. Spots are visualized using 0.1 % ninhydrin reagent.

      Classification: 18a
      60 086
      Thin layer chromatographic method for rapid identification and quantification of corticosteroid sodium phosphates in pharmaceutical preparations
      B. DAS, S.K. CHATTERJEE, S.K. DAS, (India Dept. Biochemistry, Central Drugs Lab., 3 Kyd Str., Calcutta 700 016, India)

      J. Liquid Chrom. 9, 3461-3457 (1986). Isolation of dexamethasone sodium phosphate and betamethasone sodium phosphate after alkaline phosphatase reaction. TLC on silica with chloroform - methanol - water 180:15:1 or dichloromethane - ether - methanol -water 77:15:8:1; location under short wave UV. Quantification after extraction with ethanol by absorbance at 240 nm. Average recovery 100.56 resp. 100.46 %. Assay of unesterified steroids and identification of preservatives (e.g. methyl or propyl parabenzoates, phenol, benzylalcohol) may be carried out by the same method.

      Classification: 13a
      61 256
      The use of overpressure thin-layer chromatography in the quality-control of radioactive drugs
      G. KLIVENYI*, G. JANOKI, J. TÖRKO, (*Inst. „Frédéric Joliot-Curie“, H-1775 Budapest, P.O. Box 101, Hungary)

      (Hungarian). Gyógyszerészet 31, 221-224 (1987). OPTLC of Albumon, Fyton, Pyron of 99m/Tc labelled on silica with acetone.

      Classification: 32a, 34
      67 138
      Determination of the enantiomeric composition of 2-methoxy-3-(1'-methylpropyl)pyrazine from Galbanum oil using achiral and chiral lanthanide shift reagents
      S. MIHARA, H. MASUDA, O. NISHIMURA, H. TATEBA, (Ogawa & Co., Ltd., 6-329 Akabanemishi, Kita-ku, Tokyo 115, Japan)

      J. Agric. Food Chem. 38, 465-467 (1990). Analytical and preparative TLC of 2-methoxy-methyl-popyl-pyrazine on silica with acetone - hexane 1:9 and dichloromethane - ethyl acetate 6:1.

      Classification: 23e
Page