Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      99 158
      Simple preparative isolation of salvinorin A from the hallucinogenic sage, Salvia divinorum, by centrifugal partition chromatography
      O. SHIROTA*, K. NAGAMATSU, S. SEKITA (*Laboratory of Pharmacognosy and Natural Products Chemistry, Faculty of Pharmaceutical Sciences at Kagawa Campus, Tokushima Bunri University, 1314-1 Shido, Kagawa, 769-2193, Japan; shirota@kph.bunri-u.ac.jp)

      J. Liq. Chromatogr. & Relat. Technol. 30, 1105-1114 (2007). TLC of salvinorin A, a potent naturally occuring kappa-opioid selective agonist, on silica gel and on RP-18 with n-hexane - ethyl acetate 1:1. Detection by spraying with vanillin - phosphoric acid reagent followed by heating.

      Classification: 32e
      100 004
      Partial least-squares study of the effects of organic modifier and physicochemical properties on the retention of some thiazoles
      Tatjana DJAKOVIC-SEKULIC*, N. PERISIC-JANJIC, C. SARBU, Z. LOZANOV-CRVENKOVIC (*Department of Chemistry, Faculty of Sciences, University of Novi Sad, Trg D. Obradovica 3, 21000 Novi Sad, Serbia; tanja@ih.ns.ac.yu)

      J. Planar Chromatogr. 20, 251-257 (2007). TLC with aqueous ammonia-organic modifier (acetonitrile, dioxane, acetone) mobile phases has been used to study the effect on retention of the chromatographic system and the physicochemical properties of twelve 2,4-dioxotetrahydro-1,3-thiazoles. Principal-component analysis and partial least-squares regression were used to determine the molecular properties with the greatest effect on retention for each modifier. Good correlation was obtained between experimental and calculated retention data. HPTLC on RP-18 without chamber saturation. Detection under UV 254 nm.

      Classification: 2c
      100 035
      Modeling of Thin-Layer Chromatographic separation of androstane isomers
      L. JÄNTSCHI, S. HODISAN, C. CIMPOIU, A. HOSU, E. DARVASI, T. HODISAN* (*’Babes-Bolyai’ University, Faculty of Chemistry and Chemical Engineering, 11 Arany Janos, 400028 Cluj-Napoca, Romania; thodisan@chem.ubbcluj.ro)

      J. Planar Chromatogr. 20, 91-94 (2007). Descripton of the modeling of TLC separation of androstane isomers to find the optimum mobile phase. A mathematical model was developed and tested. The model takes into account the interaction between solvents and uses a complex function for modeling. The proposed mathematical model gives results similar to those obtained by use of other optimization models, e. g. the Simplex and Prisma methods. TLC of 5alpha-androstan-3beta-ol, 5alpha-androstan-3alpha-ol, 5alpha-androstan-17beta-ol, 5beta-androstan-3alpha,17beta-diol, 5alpha-androstan-3beta,17beta-diol on silica gel in a saturated chamber using different mixtures of chloroform, acetone, and petroleum ether resulting in an optimum mobile phase composition of 55:19:26. Detection by spraying with 5 % ammonium molybdate and 5 % sulfuric acid in water and heating to 80 °C.

      Classification: 13a
      100 063
      Monitoring the origin of wine by reversed-phase Thin-Layer Chromatography
      Claudia CIMPOIU*, A. HOSU, R. BRICIU, V. MICLAUS (*“Babes-Bolyai“ University, Faculty of Chemistry and Chemical Engineering, 11 Arany Janos, 400028 Cluj-Napoca, Romania; ccimpoiu@chem.ubbcluj.ro)

      J. Planar Chromatogr. 20, 407-410 (2007). TLC of the color pigments from different sorts of red wine (Cabernet Sauvignon, Merlot, and Burgundy) on RP-18 with acetonitrile - water - formic acid 20:29:1 in a saturated chamber. Evaluation in visible light and under UV light at 366 nm, and by spraying with a methanolic solution of 0.5 mg/mL DPPH radical (2,2.diphenyl-1-picrylhydrazyl). Densitometric evaluation. RP-TLC is a tool for monitoring wine, for identification of the origin, and for detection of adulteration.

      Classification: 30b
      100 109
      Estimation of guggulsterone E and Z in solid dosage forms containing Commiphora mukul, Hook
      J.K. LALLA*, P.D. HAMRAPURKAR, S.J. SACKET (*Prin. K. M. Kundnani College of Pharmacy, Plot No. 23, Jote Joy Building, Rambhau Salgaonkar Road, Cuffe Parade, Colaba, Mumbai 400 005, India; jklalla@mtnl.net, jklalla@vsnl.net)

      J. Planar Chromatogr. 20, 197-202 (2007). HPTLC of guggulsterone E and Z on silica gel prewashed with methanol with petroleum ether - ethyl acetate - formic acid 30:10:1 in a twin-trough chamber saturated for 20 min. Detection and densitometric scanning at 254 nm.

      Classification: 32e
      100 180
      Thin-Layer Chromatography of Aluminium
      P.A.M. NAJAR*, R.N. CHOUHAN, J.U. JEURKAR, S.D. DOLAS, K.V.R. RAO (*Jawaharlal Nehru Aluminium Research Development and Design Centre, Amaravati Road, Nagpur, India)

      J. Chromatogr. Sci. 45 (5), 263-268 (2007). TLC of microgram levels of iron, silicon, copper, nickel, titanium, magnesium, manganese, and zinc present in a high concentration aluminium matrix, on silica gel with aqueous sodium chloride solution. Quantification by densitometry. Comparison of the densitometric quantitative determination results of iron, silicon, nickel, and copper with the respective optical emission spectral analytical data.

      Classification: 33
      101 019
      Anthocyanin- and proanthocyanidin-rich extracts of berries in food supplements - analysis with problems
      Liselotte KRENN*, M. STEITZ, C. SCHLICHT, H. KURTH, F. GAEDCKE (*Department of Pharmacognosy, University of Vienna, Althanstrasse 14, 1090 Vienna, Austria; liselotte.krenn@univie.ac.at)

      Pharmazie 62, 803-812 (2007). TLC of anthocyanins in aronia, blueberry and lingonberry extracts and the respective preparations (e.g. capsules, lozenges, granulate) on silica gel with ethyl acetate - water - anhydrous formic acid 10:3:2 and 10:4:1. Detection in white light prior and after spraying with iron(III)chloride solution or with vanillin phosphoric acid reagent.

      Classification: 8a
      101 047
      A validated stability-indicating TLC method for determination of forskolin in crude drug and pharmaceutical dosage form
      S. AHMAD*, M. RIZWAN, Rabea PARVEEN, M. MUJEEB, M. AQUIL (*Department of Pharmacognosy and Phytochemistry, Faculty of Pharmacy, Hamdard University, New Delhi, 110062, India, sahmad_jh@yahoo.co.in)

      Chromatographia 67 (5-6), 441-447 (2008). HPTLC of forskolinon on silica gel aluminium foil with benzene - methanol 9:1. Quantitative determination by densitometry in the absorbance mode at 545 nm after spraying with anisaldehyde sulphuric acid reagent. The method was validated: linearity was between 100 and 1000 ng/spot (r = 0.994) and the limits of detection and quantification were 8 and 27 ng/spot respectively. Application of the proposed method for determination of forskolin in Coleus forskohlii root and in capsule dosage forms, which showed 0.18 and 0.57 % w/w of forskolin, which was subjected to acid and alkali hydrolysis, oxidation, photodegradation and heat degradation. The method shows good repeatability, selectivity and accuracy, and effectively separates forskolin from components of C. forskohlii root, from excipients of capsule as well as the degradation products of forskolin. It can be used for routine analysis and as a stability-indicating method.

      Classification: 32c
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