Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      123 058
      Use of 1,2-napthoquinone-4-sulfonate (Folin’s reagent) for the Thin-Layer Chromatographic detection of p-phenylenediamine
      S. KOTE*, S. DHOBALE, V. THAKARE, B. MORE (*Regional Forensic Science Laboratory, Home Department, State of Maharashtra, Amravati 444606, India, santosh.kote27@gmail.com)

      J. Planar Chromatogr. 32, 59-60 (2019). TLC of p-phenylenediamine on silica gel with ethyl acetate - diethyl ether 1:1. Detection by spraying with aqueous alkaline solution of Folin’s reagent (0.5 % Folin’s reagent in 5 % sodium carbonate solution). The hRF value of p-phenylenediamine was 45. The LOD for p-phenylenediamine was approximately 3 μg by visual evaluation.

      Classification: 30a
      123 059
      Use of diphenylamine reagent for High-Performance Thin-Layer Chromatographic Detection of organochloro insecticide endosulfan in biological samples
      U. PAWAR*, C. PAWAR, U. KULKARNI, R. PARDESHI, M. FAROOQUI, D. SHINDE (*Regional Forensic Science Laboratories, Aurangabad, MS, India, upawar929@gmail.com)

      J. Planar Chromatogr. 32, 65-68 (2019). HPTLC of endosulfan in biological samples (pieces of stomach, intestine, liver, spleen, kidney, and lungs) on silica gel with hexane - acetone 4:1. Detection by spraying with a 10 % sodium hydroxide solution and then with diphenylamine reagent (2 g diphenylamine in 20 mL glacial acetic acid and 20 mL ethyl acetate), following by exposure to sunlight for 10 min. The hRF values of the endosulfan coordination complex (alpha and beta isomers) were 66 and 85. Zones were stable for 8 to 10 days.

      Classification: 29a
      123 060
      Superiority of Thin-Layer Chromatography over High-Performance Liquid Chromatography in enantioseparation
      D. SINGH, P. MALIK, R. BHUSHAN (*Department of Chemistry, Indian Institute of Technology Roorkee, Roorkee 247667, India, rbushfcy54@gmail.com)

      J. Planar Chromatogr. 32, 7-12 (2019). HPTLC of (RS)-mexiletine on RP-18 plates impregnated with 0.03 mM bovine serum albumin as chiral additive with acetonitrile - dichloromethane - methanol 1:1:1. Detection by exposure to iodine vapors. Resolution was 2.3 for the HPTLC method and 1.9 using an HPLC method. The HPTLC analysis took nearly 7 min, whereas HPLC took nearly 265 min to get the results.

      Classification: 38
      100 009
      Indirect resolution of enantiomers of penicillamine by TLC and HPLC using Marfey's reagent and its variants
      R. BHUSHAN*, H. BRÜCKNER, V. KUMAR (*Department of Chemistry, Indian Institute of Technology Roorkee, Roorkee 247 667, India)

      Biomed. Chromatogr. 21 (10), 1064-1068 (2007). Indirect chiral separation of penicillamine (3,3-dimethylcysteine) enantiomers after derivatization with Marfey's reagent (FDNP-Ala-NH2) and two of its structural variants, FDNP-Phe-NH2 and FDNP-Val-NH2, with phenol - water 3:1 and solvent combinations of acetonitrile and triethylamine phosphate buffer in normal and reversed-phase TLC, respectively. Also separation of the diastereomers on a reversed-phase HPLC column with gradient elution of acetonitrile and 0.01 m trifluoroacetic acid. Comparison of the results due to these three reagents. Successful application of the method for checking the enantiomeric impurity of l-penicillamine in d-penicillamine and to check the enantiomeric purity of pharmaceutical formulations of d-penicillamine.

      Classification: 3d
      100 044
      Mixed surfactants enable separation of lysine from other essential amino acids in TLC on silica gel
      A. MOHAMMAD*, S. LAEEQ (*Department of Applied Chemistry, Faculty of Engineering and Technology, Aligarh Muslim University, Aligarh 202002, India; mohammadali4u@rediffmail.com)

      J. Planar Chromatogr. 20, 423-427 (2007). TLC of 8 essential amino acids (L-lysine, L-valine, L-isoleucine, DL-threonine, L-methionine, L-leucine, DL-phenylalanine, DL-tryptophan) on silica gel with 17 mobile phases, of which the mixed aqueous surfactant solution Triton X-100 (0.001 mM) - sodium dodecyl sulfate, 0.081 mM - acetone 1:1:5 was identified as the best mobile phase for specific separation of lysine. Visualization by spraying with 0.3 % ninhydrin in acetone. Limit of detection was 0.5 µg/zone.

      Classification: 18a
      100 073
      High-performance thin-layer chromatography method for quantitative determination of oenothein B and quercetin glucuronide in aqueous extract of Epilobii angustifolii herba
      Agnieszka BAZYLKO*, Anna K. KISS, J. KOWALSKI (*Department of Pharmacognosy and Molecular Basis of Phytotherapy, Faculty of Pharmacy, Warsaw Medical University, ul. Banacha 1, 02-097 Warszawa, Poland)

      J. Chromatogr. A 1173 (1-2), 146-150 (2007). HPTLC of oenothein B and quercetin glucuronide in aqueous extract of Epilobii angustifolii herba on RP-18 W phase with 1) 25 % acetonitrile in water (with 50 mM H3PO4) over 80 mm for oenothein B, and 2) with acetonitrile over 40 mm for quercetin glucuronide. Quantification of oenothein B and quercetin glucuronide by densitometry at 270 and 350 nm, respectively. Linearity was between 1.14 and 2.28 µg/zone for oenothein B and 77 and 691 ng/zone for quercetin glucuronide. Aqueous extract of Epilobii angustifolii herba contained 152.46 ± 4.92 mg/g oenothein B and 22.07 ± 1.38 mg/g quercetin glucuronide.

      Classification: 32c
      100 133
      Effect of the physicochemical properties of N,N-disubstituted-2-phenylacetamide derivatives on their retention behavior in RP-TLC
      Nada PERISIC-JANJIC*, G. VASTAG, J. TOMIC, S. PETROVIC (*Department of Chemistry, Faculty of Sciences, Trg D. Obradovica 3, 21000 Novi Sad, Serbia; nadap@uns.ns.ac.yu)

      J. Planar Chromatogr. 20, 353-359 (2007). TLC of 8 N,N-disubstituted-2-phenylacetamides on RP-18 with acetone, acetonitrile, tetrahydrofuran, dioxane, methanol, ethanol, 1-propanol, and 2-propanol as organic modifiers of aqueous mobile phases. The retention observed with different mobile-phase modifiers was correlated, and good correlation was obtained between lipophilicity measured chromatographically and biological activity predictors. Detection under UV light at 254 nm.

      Classification: 32a
      100 184
      Selective separation of dodecyltrimethylammonium bromide from other cationic and nonionic surfactants
      A. MOHAMMAD*, N. HAQ (*Analytical Research Laboratory, Department of Applied Chemistry, Aligarh Muslim University, Aligarh-202002, U. P., India; mohammadali4u@rediffmail.com)

      J. Planar Chromatogr. 20, 347-351 (2007). TLC of DTAB on soil, silica gel, alumina, and kieselguhr with fifteen mobile phases, such as aqueous solutions of ammonium sulfate and urea, with chamber saturation for 10 min. Detection by spraying with modified Dragendorff reagent. Among the systems studied the best system for selective separation of DTAB from multicomponent mixtures of other surfactants was kieselguhr - 0.1 M ammonium sulfate. Semi-quantitative determination by spot-area measurement.

      Classification: 35a
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