Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

Page
      94 037
      TLC separation of Unicaria tomentosa alkaloids on chemically modified stationary phases
      M. GLENSK*, B. ZBIKOWSKA, W. CISOWSKI (*Department of Pharmacognosy, University of Medicine, pl. Nankiera1, 50-140 Wroclaw, Poland)

      J. Planar Chromatogr. 17, 14-17 (2004). HPTLC of oxindole alkaloids on silica gel, Diol-, CN-, NH2-, and RP-18-phases. Normal-phase TLC with 1) ethyl acetate - methanol - water 200:27:20; 2) ethyl acetate - methanol - water - acetic acid 100:2.7:5:3; 3) ethyl acetate - methanol - water - formic acid 100:2.7:5:3; 4) ethyl acetate - isopropanol - ammonia 100:2:1. RP TLC with water - methanol 7:3 containing 0.25 % ammonia; development in horizontal chamber (sandwich configuration) at room temperature. Two-dimensional TLC with mobile phase 2 in the first direction and, after drying, with mobile phase 3 in the second direction. Evaluation under UV 254 nm and after derivatization with iodine reagent or with Dragendorff reagent. TLC separations were documented by scanning. Silica and cyanopropyl layers with acidic aqueous mobile phases gave the best separation.

      Classification: 22
      94 058
      (Study of the quality standard for Xiaozhi tablets
      X. DING (Ding Xiaoyan), S. YANG (Yang Songqing), W. Jiang (Jiang Weike), T. ZHOU (Zhou Tao) (Guiyang Dechangxiang Pharm. Co. Ltd., Guiyang, Guizhou 550001, China)

      Chinese J. Trad. Patent Med. (Zhongchengyao) 26 (5), 371-373 (2004). TLC of Xiaozhi tablet extracts on silica gel with 1) ethyl acetate - formic acid - water 5:2:1; 2) benzene - acetone - ethyl acetate - ammonia 4:6:8:1; 3) chloroform - methanol - ammonia 40:10:1. Detection 1) under UV light; 2) by spraying with 5 % solution of potassium iodobismuthate. Identification by fingerprint techniques. Quantification of matrine by HPLC with method validation.

      Classification: 32c
      94 083
      Application of TLC and GC-MS to the detection of capsaicin from hot peppers (Capsicum annuum)
      Maria-Ioana MOISE*. C. MARUTOIU, D. N. BADEA, C.-A. GAVRILA, C. PATROESCU (*Lucian Blaga University of Sibiu, Faculty of Agricultural Sciences, Food Industry and Environmental Protection, 7 - 9 Dr Ioan Ratiu St, 2400 Sibiu, Romania)

      J. Planar Chromatogr. 17, 147-148 (2004). TLC of capsaicin on silica gel with concentration zone with toluene - acetone - chloroform 8:7:5 and 9:6:5. Detection by spraying with a 0.25 % ethanolic solution of 2,6-dichloroquinone-4-chlorimide or by exposure to iodine vapor.

      Classification: 32e
      94 109
      (Study of the quality standard for sugar-free Qixuekang oral liquid
      X. ZHU (Zhu Xuan), H. TANG (Tnag Haiying), M. CHEN (Chen Man) (Jiangsu Xiansheng Pharm. Co., Ltd., Nanjing, Jiangsu 210042, China)

      Chinese J. Trad. Patent Med. (Zhongchengyao) 26 (6), 449-452 (2004). TLC of Qixuekang oral liquid extract on silica gel with 1) chloroform - ethyl acetate - methanol - water 15:40:22:10; 2) chloroform - methanol - water 28:10:1. Detection 1) by spraying with 10 % H2SO4 in ethanol and heating; 2) under UV 365 nm. Identification by fingerprint techniques. Quantification of notoginsenoside R1 by HPLC with method validation.

      Classification: 32c
      95 038
      Optimization of the separation of some aflatoxins by thin-layer chromatography
      C. MARUTOIU*, S. PUIU, M. I. MOISE, L. SORAN, O. F. MARUTOIU, L. BOBOS (* „Lucian Blaga“ University from Sibiu, Department of Chemistry, 7-9 Ion Ratiu Street, RO-2400 Sibiu, Romania)

      J. Planar Chromatogr. 17, 372-374 (2004). TLC of aflatoxins B1, B2, G1, and G2 on silica gel with chloroform - acetone 23:2 in unsaturated chambers. Detection under UV light at 366 nm. Selection of the optimum mobile phase composition by software programs.

      Classification: 28b
      95 067
      (Differentiation and identification of Xanthium sibiricum Patr
      SH. HU (Hu Shuangfeng) (Ningbo Municip. Inst. Drug Cont., Ningbo, Zhejiang 315040, China)

      seed and the phoney, Xanthium Spinosam L. seed) (Chinese). Chinese J. Hosp. Pharm. (Zhongguo Yiyuan yaoxue Zazhi) 25 (2), 185-187 (2005). HPTLC on silica gel with n-butanol - glacial acetic acid - water 4:1:5. Detection by exposing to ammonia vapours. Identification by fingerprint technique combined with morphological differentiation and UV spectra comparison.

      Classification: 32c
      95 102
      The effect of the electronegativity of donor atoms in coordinated beta-diketonato ligands on the chromatographic behavior of metal complexes
      R. M. BAOSIC, D. M. MILOJKOVIC-OPSENICA, Z. L. TESIC* (*Faculty of Chemistry, University of Belgrade, Studentski trg 16, P. O. Box 158, 11001 Belgrade, Serbia and Montenegro)

      J. Planar Chromatogr. 17, 250-254 (2004). TLC of three series of beta - diketonato complexes of the type [M(acac)3-n(phacphac)n], [M(acac)3-n(phacphSac)n], and [M(acac)3-n(phSacphSac)n] (where M represents cobalt(III), chromium(III), or ruthenium(III), acac is the 2,4-pentanedionato ion, phacphac is the 1,3-diphenyl-1,3-propanedionato ion, phacphSac is 3-mercapto-1,3-diphenyl-prop-2-en-1-one, phSacphSac is the 3-mercapto-1,3-diphenyl-prop-2-en-1-thion ion, and n = 0-3) on silica gel with five mono-component (chloroform, toluene, dichloromethane, xylene, tetrahydronaphthalene) and five two-component eluents (n-amyl acetate - carbon tetrachloride 1:1, n-butyl acetate - carbon tetrachloride 2:3, chloroform - carbon tetrachloride 1:1 and 3:7, and dichloromethane - carbon tetrachloride 4:1. Separations were performed in a horizontal chamber after equilibration for 30 min. After development the colored spots were readily visible.

      Classification: 2c, 33a
      96 050
      Use of ninhydrin for detection of silylated amino acids
      B. Basak, D. Bandyopadhyay, A. Banerji, Asima Chatterjee* (*Center of Advanced Studies on Natural Products Including Organic Synthesis, Department of Chemistry, Calcutta University, 92 A. P. C. Road, Kolkata 700 009, India)

      J. Planar Chromatogr. 18, 251-252 (2005). TLC of 22 silylated amino acids on silica gel with butanol. After spotting the plates with the amino acid solutions the samples were sprayed with hexamethyldisilazane reagent (1 % solution in acetone), dried, heated at 110 °C for 20 min, and cooled. The developed plates were dried, sprayed with ninhydrin (0.25 % solution in acetone), dried completely, then further heated at 110 °C for 20 min. Detection limits of this method within 10 min are comparable with those of other methods.

      Classification: 18a
Page