Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      111 095
      (Study on the method for the quality control of Luman-12 by thin-layer chromatography) (Chinese)
      SH. LI (Li Shenghua) (Bayan Nur Municip. Inst. for Drug Contr., Inner Mongolia, Bayan Nur, Linhe 015000, China)

      Chinese J. Ethnopharm.(9), 36-38 (2012). Luman-12 is a traditional Mongolian herbal medicine preparation for treatment of cough, asthma, etc. For quality control of the main component herbal drugs TLC on silica gel 1) for Radix Polygalae, with toluene – ethyl acetate – formic acid 28:8:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing in daylight; 2) for Radix Glycyrrhizae, with toluene – ethyl acetate – formic acid 10:8:1, detection under UV 366 nm; 3) for Piper nigrum, with benzene – ethyl acetate – acetone 7:2:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing in daylight.

      Classification: 32e
      111 118
      Quantification and side component analysis of the cosmetic active tiliroside using planar chromatography
      M. SCHULZ*, Susanne MINARIK, Michaela OBERLE, Sylvia EISENBERG (*Merck KGaA, MM-LER-CP. Frankfurterstr. 250, 64293 Darmstadt, Germany, michael.schulz@merckgroup.com)

      CBS 107, 11-12 (2011) HPTLC of tiliroside (a cosmetic active obtained by extraction from a plant of the family Sterculiaceae) and side components kaempferol-3-glucoside, kaempferol-3-rutinoside, kaempferol, and coumaric acid on silica gel with ethyl acetate - formic acid - acetic acid- water 100:11:11:27 + 1% heptane. Detection under UV 366 nm after spraying with natural products reagent (1 % diphenylborinic acid 2-aminoethylester in methanol) and under white light after spraying with anisaldehyde sulfuric acid reagent (0.5 mL anisaldehyde in 85 mL methanol with 10 mL acetic acid and 8 mL conc. sulfuric acid) and heating at 90-125 °C for 15 min. Quantitative absorption measurement of tiliroside at 315 nm using a 4-point calibration via peak area. The tiliroside contents in the sample extracts were determined as: 1 = 1.09 µg (RSD = 0.4 %), 2 = 0.93 µg (RSD = 0.8 %), 3 = 1.19 µg (RSD = 1.2 %) and 4 = 3.32 µg (RSD = 0.3 %). During the side component analysis no kaempferol, coumaric acid, and glucose were detected in the tiliroside samples. Small amounts of kaempferol-3-glucoside and kaempferol-3-rutinoside were found. HPTLC covers several tasks: quantification of the active ingredient in a complex plant matrix for determining the quality of the raw material, in-process control for monitoring the impurity profile during the manufacturing process and the quantification of the active ingredient in the final product.

      Classification: 32e
      111 140
      (Study of the preparation and the method for the quality control of Ruxian pills) (Chinese)
      J. XU (Xu Jing), W. WANG (Wang Wei), B. SHAO (Shao Bing), Y. LIU (Liu Yan)* (*Inst. of Clinical Pharm. & Drug, The 2nd Afiliated Hosp., Harbin Univ. of Med., Heilongjiang, Harbin 150086, China)

      Acta of Trad. Chinese Med. & Pharm. 40 (3), 100-102 (2012). Ruxian pills are a herbal TCM for treatment of abdominal mass accumulation and breast tumors etc. The medicine is prepared by blending the decoction and powders of the component drugs with honey in proper proportion and then processing into pills. For quality control, TLC on silica gel 1) for Radix Angelicae Sinensis, with n-hexane – ethyl acetate 9:1, detection under UV 366 nm; 2) for Radix Paeoniae Rubra, with chloroform – ethyl acetate – methanol – water 200:25:50:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:25 and heating at 105 °C, viewing in daylight; 3) for Spina gleditsiae, with toluene – ethyl acetate – formic acid 7:2:1, detection under UV 366 nm. Using this method the optimum extraction conditions for preparing the decoction from the crude drugs as well as the stability during storage of the final preparation were studied.

      Classification: 32e
      111 156
      (Study on the method for the quality control of Emilia sonchifolia (Linn
      X. ZOU (Zou Xiaohua), CH. ZHAO (Zhao Chao), X. ZHOU (Zhou Xin)* (*The Key Lab. for Inform. System of Mount. Areas & Prot. of Ecol. Environment, Guizhou Normal Univ., Guizhou, Guiyang 550001, China)

      by thin-layer chromatography) (Chinese). J. of Guizhou Normal Univ. (Natural Sci.) 30 (3), 9-11 (2012). Emilia sonchifolia (Linn.) DC. is a TCM herb used in the formulations for treating conjunctivitis, tonsillitis, pneumonia, infectious hepatitis, dysentery, diarrhea, urinary tract infection, etc. For quality control TLC of the herb extracts an the standard emodin on silica gel with chloroform – methanol – formic acid 300:10:1, detection 1) under UV 366 nm; 2) by exposing to ammonia vapors and viewing under UV 366 nm.

      Classification: 32e
      112 049
      Color and chemical reactions of selected sesquiterpene lactones and ecdysones from Asteraceae on TLC plates
      G. NOWAK*, M. URBANSKA, J. NAWROT, M. BERNARD, R. PAC (*Department of Medicinal and Cosmetic Natural Products, Poznan University of Medical Sciences, Mazowiecka Str. 33, 60-623 Poznan, Poland, gnowak@ump.edu.pl)

      J. Planar Chromatogr. 26, 289-293 (2013). TLC of guaianolides and four other types of sesquiterpenoids, namely germacranolides, seco-pseudoguaianolides, and pseudoguaianolides, as well as two phytoecdysteroids in the aerial parts of Centaurea bella, Dugaldia hoopesii, Inula aschersoniana, Serratula wolffii, Stizolophus balsamita and Zoegea baldschuanica on silica gel with mixtures of methylene chloride and acetone in ratios 8:1, 7:1, 5:1, 3:1, 2:1 and 1:1 for sesquiterpenes and methylene chloride - acetone 1:2 as well as methylene chloride - methanol 5:1 for the separation of ecdysones. Detection by spraying with anisaldehyde reagent (anisaldehyde 0.5 mL; acetic acid 10 mL; methanol 85 mL; sulfuric acid 4.5 mL), followed by heating at 103 ºC for 3 min. The color evaluation allowed for correlation with the presence of substituents on the sesquiterpene ring with high probability.

      Classification: 15a
      112 088
      (Study of the method for the quality control of Inula nervosa Wall, a traditional Chinese medicinal herb) (Chinese)
      K. LI (Li Ke)*, D. CHEN (Chen Dan), Y. HU (Hu Yibing), L. SHI (Shi Leizhe), R. LI (Li Ruocun) (*Hunan Provinc. Acad. of Trad. Chinese Med. Hunan, Changsha 420013, China)

      Chinese J. of Ethnomed. & Ethnopharm. 20, 30-32 (2012). Inula nervosa Wall is a herbal TCM drug with anti rheumatism effects. It is frequently used as key component in herbal TCM preparations for the treatment of rheumatism. For quality control, TLC of the volatile oil (obtained by steam distillation of the crude drug) diluted 1:100 with acetone, and the standards thymol and thymyl isobutyrate, on homemade layers (coated using a slurry of silica gel in 1 % NaOH solution), with cyclohexane – toluene 3:4, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 1:200 and heating at 105 °C until the zones are visible in daylight.

      Classification: 32e
      112 113
      (Study of the method for the quality control of Tongfenglishi Koufuye oral liquid) (Chinese)
      L. WANG (Wang Linli)*, D. MENG (Meng Desheng), Y. PENG (Peng Yixin) (*Dep. of Pharm., Daping Hosp. Affil. to Inst. of field surgery, Chinese PLA Third Milit. Med. Univ., Chongqing 400042, China)

      J. of China Pharm. 21 (15), 49-50 (2012). Tongfenglishi Koufuye oral liquid is a herbal TCM preparation for the treatment of rheumatic arthralgia, the numbness of limbs, swollen carbuncles and hyperlipidemia. For quality control, TLC on silica gel 1) for Radix et Rhizoma Rhei, with petroleum ether (30-60°C) – ethyl formate – formic acid 15:5:1, detection in daylight; 2) for Fructus Crataegi, with cyclohexane – chloroform – ethyl acetate 20:5:8, detection by spraying with 10 % sulfuric acid in ethanol, heating at 110 °C and viewing in daylight; 3) for Semen Vaccariae, with chloroform – methanol – water 15:7:2, detection by spraying with 5 % potassium iodobismuthate in HCl – water 1:200 and viewing in daylight. Quantification of emodin by HPLC.

      Classification: 32e
      112 130
      (Study of the method for quick determination of rhaponiticin in antibacterial Kangjun Xiaoyan Jiaonang capsules by thin-layer chromatography) (Chinese)
      J. ZHAO (Zhao Jiping)*, A. LIU (Liu Aiping) (*Xiantao Municip. Inst. for Drug & Food Contr., Hubei, Xiantao 433000, China)

      J. of China Pharm. 26 (6), 620-622 (2012). Rheum palmatum L., a herbal TCM drug for clearing away body heat, eliminating toxin and nourishing skin, is commonly used as a component of herbal TCM preparations. However, a homologous herb, Rumex madaio Makino (syn. Rumex daiwoo Makino) is sometimes mistaken for Rheum palmatum in drug production. For quality control of rhaponiticin in antibacterial Kangjun Xiaoyan Jiaonang capsules, TLC of the extracts and the standard rhaponiticin on silica gel with ethyl acetate – acetone – water 10:7:1, detection under UV 366 nm. Quantification of rhaponiticin by HPLC. The method was successfully applied to nine batches of real life samples from five pharmaceutical factories.

      Classification: 32e
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