Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      97 076
      Cytotoxic xanthones and biphenyls from the root of Garcinia linii
      J.-J. CHEN* (Jih-Jung Chen), I.-S. CHEN (Ih-Sheng Chen), C.-Y. DUH (Chang-Yih Duh) (*Department of Pharmacy, Tajen Institute of Technology, Pingtung, Taiwan 907, China; jjchen@ccsun.tajen.edu.tw)

      Planta Med. 70, 1195-1200 (2004). Analytical and preparative TLC of the new xanthones linixanthone A, B, C, garcibiphenyl A and B and garcibenzopyran on silica gel with n-hexane - ethyl acetate 5:1 and 10:3, and chloroform - methanol 10:1 and 5:1. Detection under UV light at 254 nm.

      Classification: 32e
      97 114
      TLC profiling of impurities of 1-(3,4-methylenedioxyphenyl)-2-nitropropene, an intermediate in MDMA synthesis
      J. Kochana*, J. Wilamowski, A. Parczewski (*Department of Analytical Chemistry, Faculty of Chemistry, Jagiellonian University, Ingardena 3, 30-060 Cracow, Poland; kochana@chemia.uj.edu.pl)

      Influence of sample preparation methods and conditions. J. Liq. Chrom. & Rel. Technol. 27, 2463-2470 (2004). TLC of 1-(3,4-methylenedioxyphenyl)-2-nitropropene, an intermediate product of MDMA (3,4-(methylenedioxy)methamphetamine, also known as ,ecstasy’, and impurities on silica gel in a horizontal chamber with chloroform - ethyl acetate 49:1. Detection of separated impurities under UV light at 254 and 366 nm.

      Classification: 32a
      97 143
      The retention behavior of some atypical antipsychotic drugs in normal-phase TLC
      R. SKIBINSKI, Genowefa MISZTAL*, L. KOMSTA, A. KOROLCZYK (*Department of Medicinal Chemistry, Medical University of Lublin, 4 Jaczewskiego Str., 20-090 Lublin, Poland)

      J. Planar Chromatogr. 19, 73-80 (2006). TLC of six atypical antipsychotic drugs (amisulpride, clozapine, olanzapine, quetiapine, risperidone, ziprasidone) on silica gel, amino, cyano, DIOL, and polyamide phases with mixtures of n-hexane and six polar modifiers (acetone, dioxane, diethylamine, ethanol, isopropanol, and tetrahydrofuran) in a horizontal DS chamber. After development the plates were inspected under UV light at 254 nm. Quantification by densitometry.

      Classification: 32a
      98 029
      Direct ToF-SIMS analysis of organic halides and amines on TLC plates
      A. PARENT, T. ANDERSON, D. MICHAELIS, G. JIANG, P. SAVAGE, M. LINDFORD* (*Department of Chemistry and Biochemistry, Brigham Young University, Provo, UT 84602, United States, mrlindford@chem.byu.edu)

      Appl. Surf. Sci. 252, 6746-6749 (2006). To show the application of direct time-of-flight secondary ion mass spectrometry (ToF-SIMS) to analyze a reaction mixture between an alpha-bromoamide (1), and picolylamine, to form the substitution product (3) via SN2 (1 and 3 are indistinguishable by TLC on silica gel with dichloromethane – methanol – ammonia 100:15:2), a series of organic halides with widely differing structures (trifluoromethanesulfonamide, a vinyl bromide, a silyl-protected primary bromide, and iodosobenzene diacetate) were separated on TLC plates under the same conditions. The resulting spots and background were analyzed by positive and negative ion spectra. In all cases, the halide signals were notably stronger than the background signals. In addition, a series of amines (1,1-carbonyl diimidazole, norepinephrine, adenosine, and cinchonidine) was separated on TLC plates and analyzed directly by ToF-SIMS. In all but one (adenosine), even quasi-molecular ions were observed.

      Classification: 4e
      98 055
      The retention behavior of selected porphyrins on silica gel, polyamide, and cellulose TLC plates
      Joanna NOWAKOWSKA (Medical University of Gdansk, Faculty of Pharmacy, Department of Physical Chemistry, Al. Gen. J. Hallera 107, 80-416, Gdansk, Poland)

      J. Planar Chromatogr. 19, 393-397 (2006). TLC of uroporphyrin I, uroporphyrin III, coproporphyrin I, coproporphyrin III, and protoporphyrin IX (as methyl esters) on polyamide 11, cellulose and silica gel with methanol, ethanol, propanol, butanol, acetonitrile and tetrahydrofuran in a saturated chamber. Porphyrins on cellulose were detected by placing in iodine vapor for 5 min; on silica gel and polyamide 11 the porphyrins were detected as red spots in UV light at 254 nm. Chromatographic retention data and a possible retention mechanism are discussed.

      Classification: 23a
      98 088
      Study of quality standard for Wumei Rendan pills (Chinese)
      X. MAO (Mao Xiuhong)*, K. WANG, SH. JI ( Ji Shen) (*Shanghai Municipal Inst. Drug Cont., Shanghai 200233, China)
      J. Chinese Trad. Patent Med. (Zhongchengyao) 27 (8), 896-899 (2005). TLC of Wumei Rendan pills on silica gel with ethyl acetate - formic acid - water 2:1:1. Detection by spraying with 10 % ethanolic H2SO4 solution followed by heating at 105 ºC. Identification of the fingerprint. Quantification of menthol by GC, and of ammonium glycyrrhiziate by HPLC.
      Classification: 32c
      98 128
      Use of a glutamic acid-containing aqueous-organic mobile phase for on-plate separation, detection, and identification of cationic and non-ionic surfactants by thin-layer chromatography
      A. MOHAMMAD*, H. SHAHAB (*Anal. Res. Lab., Dept. of Applied Chem., Fac. of Eng. and Tech., Aligarh Muslim Univ., Aligarh-202002, India)

      Acta Chrom. 17, 272-291 (2006). TLC on silica gel with 0.1 M glutamic acid – methanol – acetone 1:1:1 has been found to be highly suitable for separation and identification of cationic and non-ionic surfactants. Visualization by use of Draggendorf reagent or iodine vapour. Spectro-photometric determination of tetradecyltrimethylammonium bromide at 670 nm after the spot extraction. The method has been used for identification of tetradecyltrimethylammonium bromide and Triton TX-100 in saline water, river water, and domestic waste water. The effects of sample pH, polarity of the alcohol and nature of the amino acid in the mobile phase, and the presence of alumina, kieselguhr, or cellulose in the silica gel layer have been examined.

      Classification: 35a
      99 027
      Lipophilicity of selected steroid compounds - I) Investigations on RP-18 W stationary phase by RP-HPTLC
      Alina PYKA*, M. BABUSKA (*Department of Analytical Chemistry, Faculty of Pharmacy, Silesian Academy of Medicine, 4 Jagiellonska St., PL-41-200 Sosnowiec, Poland; alinapyka@wp.pl)

      J. Liq. Chromatogr. Relat. Technol. 29, 1891-1903 (2006). HPTLC of androsterone, epi-androsterone, dehydro-epi-androsterone, testosterone, stigmasterol, beta-sitosterol, estradiol, hydrocortisone, and cholesterol on RP-18 W with methanol - water, and acetonitrile - water in different composition, with chamber saturation. Detection by spraying with sulfuric acid - methanol 1:9 and heating at 120 °C for 15 min. Densitometric determination of RF values. The aim of the work was to compare the lipophilicity of selected steroids determined by RP-HPTLC on RP-18 W plates using different mobile phases with lipophilicity values estimated by computational methods.

      Classification: 13a
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