Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
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      115 030
      Validated HPTLC fingerprinting and antioxidant activity evaluation of twenty-seven Romanian red wines
      A. HOSU, V. DANCIU, C. CIMPOIU* (*Babes-Bolyai University, Faculty of Chemistry and Chemical Engineering, 11 Arany Janos, 400082 Cluj-Napoca, Romania, ccimpoiu@chem.ubbcluj.ro)

      J. Food Comp. Anal. 41, 174-180 (2015). HPTLC fingerprint of red wines on silica gel with ethyl acetate - formic acid - acetic acid - water 10:1:1:2. Detection by dipping into NP reagent (1 g of diphenylborinic acid aminoethylester was dissolved in 200 mL ethyl acetate), followed by drying in cold air and dipping in PEG reagent (10 g of polyethylene glycol 400 is dissolved in 200 mL dichloromethane). Qualitative identification under UV 254 and 366 nm. Precisions of hRF values (% RSD) of three selected zones on two plates was below 0.02 %.

      Classification: 8a
      116 014
      The influence of image correction and chromatogram alignment on similarity measure of one-dimensional TLC by means of image analysis
      T. TANG (Tang Tie Xin), Y. GUO (Guo Yi Li), Q. LI (Li Qing), X. XU (Xu Xin Jun), D. WANG (Wang Dong Mei), D. YANG (Yang De Po)* (*School of Pharmaceutical Sciences, Sun Yat-sen University, Guangzhou 510006, P. R. China, lssydp@mail.sysu.edu.cn)

      J. Liq. Chromatogr. Relat. Technol. 38, 1279-1285 (2015). TLC of Citrus herbal medicines on NaOH-modified silica gel with ethyl acetate - methanol - water 100:17:13, followed by drying at room temperature and second development with toluene - ethyl acetate - formic acid - water 20:10:1:1. Detection by spraying with 1 % aluminium chloride ethanolic solution. The greyscale image captured under UV 365 nm was corrected by removing the quadratic baseline trend of the densitometric curve of every row.

      Classification: 3f
      116 049
      Characterization of saponins in peas (Pisum sativum L
      V. REIM, S. ROHN* (*Institute of Food Chemistry, Hamburg School of Food Science, University of Hamburg, Grindelallee 117, 20146 Hamburg, Germany, rohn@chemie.uni-hamburg.de)

      Food Res. Int. 76, 3-10 (2015). HPTLC of saponins in peas (Pisum sativum) on silica gel with chloroform - methanol - water 55:37:8. Detection by dipping into p-anisaldehyde sulfuric acid reagent for 2 s, drying for 10 min, followed by heating at 70 °C for 5 min. Quantitative determination by absorbance measurement at 545 nm. The hRF of soyasaponin βg was 60 as a violet-blue band and for soyasaponin I 57 as an orange band on a dark background. Saponin identification by hyphenation of HPTLC with mass spectrometry (MS) via a TLC–MS interface.

      Classification: 14
      116 080
      Thin-layer chromatography - autography - high resolution mass spectrometry analysis
      A. RAMALLO, M. SALAZAR, R. FURLAN* (*Rosario Research Institute for Drug Discovery, Rosario National University, Rosario, Argentina, rfurlan@fbioyf.unr.edu.a)

      Phytochem. Anal. 26, 404-412 (2015). TLC-autography of physostigmine in an extract of Brassica rapa with the acetylcholinesterase inhibitor on a TLC plate sprayed with a solution of α-naphthyl acetate (2.5 mg/mL) – fast blue B (2.5 mg/mL) 4:1 and with a acetylcholinesterase agar solution distributed over the TLC plate. The plate was developed with dichloromethane - methanol 9:1, ethyl acetate - methanol - water 5:5:2 and toluene - chloroform - ethanol 57:114:29. Further extraction and analysis with high resolution mass spectrometry. _x000D_

      Classification: 32e
      117 026
      Application of orthogonal pressurized planar electrochromatography to micropreparative separation of test dye mixture – preliminary results
      R. GAJOS, E. LOPACIUK, T. DZIDO* (*Department of Physical Chemistry, Chair of Chemistry, Medical University, Lublin, Poland, tadeusz.dzido@umlub.edu.pl)

      J. Planar Chromatogr. 29, 77-81 (2016). Orthogonal pressurized planar electrochromatography (OPPEC) of 4-(2-pyridylazo)resorcinol monosodium salt (1), patent blue (2), and azorubine (3) on RP-18W with 45 % methanol in buffer solution (pH 3.2, final concentration of buffer components in the mobile phase: 2.28 mmol/L of citric acid and 1.34 mmol/L of disodium hydrogen phosphate). The external pressure exerted on the adsorbent layer was set up as 15.0 bar. The polarization voltage applied to the electrodes was 1.5 kV, and the separation time was 150 min.

      Classification: 3d
      117 052
      Antiviral activity of Myracrodruon urundeuva against rotavirus
      Alzira B. CECILIO*, Pollyana de C. OLIVEIRA, S. CALDAS, Priscilla R.V. CAMPANA, Fernanda L. FRANCISCO, Maria Gorette R. DUARTE, Lorena de A.M. MENDONCA, Vera L. de ALMEIDA (*Ezequiel Dias Foundation, Belo Horizonte, MG, Brazil, alzira.cecilio@funed.mg.gov.br)

      Rev. Bras. Farmacogn. 26, 197-202 (2016). HPTLC of tannins (1), flavonoids (2), anthraquinones (3), terpenes (4), cardiotonic glycosides (5) and alkaloids (6) in Myracrodruon urundeuva on silica gel with toluene – acetic acid – formic acid 70:167:14 for (1), ethyl acetate – methanol – water 8:1:1 for (2), toluene – acetone – chloroform 8:5:7 for (3), hexane – ethyl acetate 1:1 for (4), ethyl acetate – methanol – water 20:3:2 for (5), and ethyl acetate – formic acid – acetic acid – water – ethyl methylketone 86:16:23:47:78 for (6). Detection by spraying with 1 % potassium ferricyanide – 2 % iron(III)chloride 1:1 for (1), 2 % aluminium chloride for (2), 5 % potassium hydroxide for (3), anisaldehyde-sulfuric acid reagent for (4), Kedde reagent for (5) and Dragendorff reagent for (6).

      Classification: 8a, 9, 14, 15
      117 084
      Cytotoxic steroidal glycosides from the whole plant of Calamus acanthophyllus
      H. PRAWAT*, C. MAHIDOL, W. KAWEETRIPOB, P. INTACHOTE, S. PISUTJAROENPONG, S. RUCHIRAWAT (*Chulabhorn Research Institute, Bangkok, Thailand; hunsa@cri.or.th)

      Planta Medica 82, 11/12, 1117-1121 (2016). TLC was applied for two purposes: first, to monitor the subfractionation of the methanol extract of the whole Calamus acanthophyllus (eluent and layer not given); second, to analyze the sugar composition of callaphylloside (a weakly cytotoxic pregnastanol saponoside). For this purpose, callaphylloside was heated for 3 h with HCl 2 N under reflux; TLC of the lyophilized and neutralized ethyl acetate extract of the mixture on silica gel with ethyl acetate – n-butanol – water 2:7:1 together with standards. The sugar moiety consisted in rhamnose and glucose (2 units of each, as confirmed through NMR of the compound)._x000D_

      Classification: 14, 32e
      117 112
      Stability-indicating chromatographic methods for the determination of sertindole
      N.A. EL-RAGEHY, N.Y. HASSAN, M. ABDELKAWY, M.A. TANTAWY* (*Anal. Chem. Dep., Fac. of Pharm., Cairo Univ., Kasr el Aini Street, 11562, Cairo, Egypt, matantawy@hotmail.com)

      J. Chromatogr. Sci. 52 (6) 559-565 (2014). TLC of sertindole subjected to stress stability studies, including acid, alkali, oxidative, photolytic and thermal degradation, on silica gel with methanol – ethyl acetate – 33 % ammonia 10:90:1, detection under UV 254 nm (the hRf was 71 for sertindole and 16 for its oxidative degradation product), identification by IR and GC/MS, quantification by densitometry at 227 nm with a linearity range of the calibration curve from 2 to 14 µg/band. The intermediate precisions and repeatabilities were < 2%. The method is suitable for quality control laboratories as stability-indicating method and for routine analysis without any preliminary separation step.

      Classification: 32c
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