Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      110 098
      (Study on the method for the quality control of E Ling capsules by thin-layer chromatography) (Chinese)
      Y. LIANG (Liang Yuanyuan)*, Y. HUANG (Huang Yuping) (*New Drug R & D Center, Guangzhou Univ. of Trad. Chinese Med. & Pharm., Guangzhou 510006, China)

      J. of China Pharm. 26 (5), 503-504 (2012). E Ling capsule is a herbal TCM for activating blood circulation to dissipate blood stasis, relieving pain, eliminating stagnation, and is prescribed clinically to treat pelvic endometriosis. For quality control, TLC of the extracts of the medicine on silica gel 1) for the root of red-rooted salvia, with toluene – ethyl acetate 19:1, detection by viewing in daylight; 2) for Fructus Aurantii, first over 4 cm with ethyl acetate – methanol – water 100:17:10, then over 8 cm with toluene – ethyl acetate – formic acid – water 20:10:1:1, detection at UV 366 nm after spraying with 1 % aluminium chloride in ethanol; 3) for Rhizoma Corydalis, with n-hexane – chloroform – methanol 15:8:2, detection at UV 366 nm.

      Classification: 32e
      110 131
      (Study on quality standard of Dingxuan granules) (Chinese)
      H. QI (Qi Hong)*, CH. LIU (Liu Chuantong) (*The People’s Hosp. of Shimen, Hunan, Changde 415300, China)

      J. of China Pharm. 21 (3), 16-18 (2012). Dingxuan granules are a herbal TCM preparation with nourishing effect on liver and kidney and curative effect on Meniere's syndrome. For quality control, TLC of the extracts of the medicine 1) for Radix Polygoni multiflori preparata, on silica gel first over 3.5 cm with chloroform – methanol 7:3, then over 7 cm with chloroform – methanol 20:1, detection at UV 366 nm; 2) for Radix Paeoniae alba, on silica gel with chloroform – methanol 4:1, detection by spraying with 5 % vanillin in sulfuric acid – ethanol 4:1 and heating at 105 °C, viewing under daylight; 3) for the fruit of Chinese wolfberry, on silica gel developed with chloroform – ethyl acetate – formic acid 2:3:1, detection at UV 366 nm; 4) for Angelica sinensis, on silica gel with n-hexane – ethyl acetate 17:3, detection at UV 366 nm.

      Classification: 32e
      110 155
      (Study on the method for the quality control of Ningxin pills) (Chinese)
      Y. WANG (Wang Ying) (Chongqing Municip. Trad. Chinese Med. Hosp., Chongqing 400021, China)

      Chinese J. of Trad. Chinese Med. for Emerg. 21 (5), 738-739 (2012). Ningxin pills are a TCM preparation with special efficiency on promoting blood circulation, removing blood stasis, relieving pain and are prescribed clinically to treat coronary disease and angina pectoris. For quality control, TLC of the extracts on silica gel 1) for Panax Notoginseng (Burk.) F.H.Chen, Radix Ginseng rubra, with the lower phase of chloroform – ethyl acetate – methanol – water 15:40:22:10, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C, viewing in daylight; 2) for Rhizoma Corydalis, with toluene – acetone 9:2, detection by exposure to iodine vapors and evaluation at UV 366 nm; 3) for borneol, with petroleum ether (30-60 ºC) – ethyl acetate – chloroform 11:1:3, detection by spraying with 1 % vanillin in sulfuric acid – ethanol 1:4 and heating at 105 °C, viewing in daylight.

      Classification: 32e
      110 175
      (The quality assay of Shenqixinjikang compound oral liquid by thin-layer chromatography) (Chinese)
      M. ZHANG (Zhang Mingzi)*, SH. JU (Ju Shanji), Y. HAN (Han Yingchen) (*Yanbian Autonomous Prefecture Test Inst. of Food & Pharm., Jilin, Yanbian 133001, China)

      J. of China Pharm. 21 (4), 30-31 (2012). Shenqixinjikang compound oral liquid, as a TCM preparation is specially effective for invigorating the circulation of blood, inducing resuscitation, relieving pain, and is prescribed clinically to cure cardiopalmus and angina pectoris. For quality control, TLC of the extracts of the medicine 1) for Rhizoma Polygoni Cuspidati, on silica gel with petroleum ether ( 60-90 ºC) – formyl acetate – formic acid 15:5:1, detection at UV 366 nm; 2) for Leguminosae, on silica gel with n-butanol – acetic acid – water 5:1:4, detection by spraying with 10 % sulfuric acid in ethanol and heating at 105 °C for 5 min followed by evaluation under daylight or UV 366 nm; 3) for Rehmannia, on silica gel with chloroform – methanol – water 14:6:1, detection by spraying with 3 % vanillin in ethanol – sulfuric acid 100:1 and heating at 105 °C followed by evaluation under daylight.

      Classification: 32e
      111 025
      Lipophilicity of oils and fats estimated by TLC
      R. NASCU, C. SARBU* (*Faculty of Chemistry and Chemical Engineering, Babes-Bolyai University, Arany Janos Str. No. 11, Cluj Napoca, 400028, Romania, csarbu@chem.ubbcluj.ro)

      J. Sep. Sci. 36, 1317-1326 (2013). HPTLC of 1. aflatoxine G1; 2. ochratoxine A; 3. zearalenone; 4. quinine; 5. cinconine, 6. hydroquinine; 7. o-(4-chlorobenzoyl) hydroquinine; 8. hydroquinine 4-methyl-2-quinolyl ether; 9. (DHQ)2 Phal; 10. (DHQ)2 AQN and 11. camptothecin on RP-18, RP-8, and RP-2 with 85 to 95 % methanol in steps of 2.5 %. In the case of the other stationary phases, the methanol fraction modification was of 5 %. The methanol fraction ranged from 75 to 95 % for RP-18 W, from 35 to 55 % for amino phase, from 50 to 70 % for diol phase, and finally from 65 to 85 % for cyano phase. Qualitative identification by absorbance measurement at 254 and 366 nm. The lipophilicity indices indicated that the mRM appears to be the most suited descriptor.

      Classification: 11c
      111 063
      (Study of the method for the identification of Shangke Tiegao wound plaster by thin-layer chromatography) (Chinese)
      S. CHEN (Chen Suying)*, J. HUANG (Huang Jian), X. ZHUANG (Zhuang Xuechao), Y. CHEN (Chen Yunzi) (*Prepar. Centre, Fushan Municip. Hosp. of Trad. Chinese Med., Guangdong, Fushan 528000, China)

      Yunan J. of Chinese Trad. Med. & Pharm. 34 (2), 44-46 (2013). As a herbal TCM preparation for treating sprain, contusion, blood stasis and innominate toxic swelling, Shangke Tiegao wound plaster is a new generation of trauma plaster preparations, based on the traditional trauma powder and a hot melt pressure sensitive adhesive which improves the release of the drug and reduces skin irritation. The new formulation not only retains the original dosage form and characteristics of the efficacy of transdermal drug delivery, but is also convenient to use. For quality control, TLC on silica gel 1) for Coptis chinensis Franch, with toluene – ethyl acetate – isopropanol – methanol – ammonia 12:6:3:3:1, detection under UV 366 nm; 2) for Radix et Rhizoma Rhei, with n-hexane – ethyl acetate – formic acid 60:20:1, detection at 254 nm; 3) for Fructus Gardeniae, with ethyl acetate – acetone – formic acid – water 5:5:1:1, detection by spraying with 10 % sulfuric acid in ethanol and heating at 110 °C, viewing in daylight; 4) for Radix Sanguisorbae, with toluene (saturated with water) - ethyl acetate – formic acid 6:3:1, detection by spraying with 1 % ferric chloride in ethanol and viewing in daylight.

      Classification: 32e
      111 085
      (Study of the method for the quality control of Kalimeris indica (Linn
      R. JIANG (Jiang Rongbin), X. ZHOU (Zhou Xin)* (*Res. Center for Quality Contr. of Natural Med., Guizhou Normal Univ., Guizhou, Guiyang 550001, China)

      by thin-layer chromatography) (Chinese). J. of Guizhou Normal Univ. (Natural Sci.) 30 (3), 1-3 (2012). Kalimeris indica (Linn.) Sch. is a perennial herb used in TCM preparations for treating cold fever, hepatitis, parotitis, pharyngitis, indigestion, etc. For quality control, TLC on silica gel with chloroform – methanol 9:1, detection by spraying with 5 % sulfuric acid in ethanol and heating at 105 °C, viewing in daylgiht. The standard was alpha-spinasteryl-3-O-ß-D-glucoside.

      Classification: 32e
      111 109
      TLC and TLC–MS screening of ursolic, oleanolic and betulinic acids in plant extracts
      K. NAUMOSKA, B. SIMONOVSKA, A. ALBREHT, Irena VOVK* (*National Institute of Chemistry, Laboratory for Food Chemistry, Hajdrihova 19, 1001 Ljubljana, Slovenia, irena.vovk@ki.si)

      J. Planar Chromatogr. 26, 125-131 (2013). HPTLC of positional isomers ursolic (1) and oleanolic (2) acids and their structural isomer betulinic acid (3) in the leaves or whole fruits of fresh vegetables on RP-18 phase with n-hexane - ethyl acetate 5:1. Qualitative identification by absorbance measurement at 366 nm. The hRf of compounds (1) to (3) were 42, 48 and 62, respectively.

      Classification: 32e
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