Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      98 112
      Rapid densitometric quantitative screening of the myricitrin content of crude methanolic extracts of leaves from a variety of Acer species
      M. WLODARCZYK, G. MATYSIK, W. CISOWSKI, M. GLENSK* (*Department of Pharmacognosy, Wroclaw Medical University, Nankiera 1, 50-140 Wroclaw, Poland)

      J. Planar Chromatogr. 19, 378-382 (2006). TLC and HPTLC of myricitrin on silica gel, pre-washed with methanol, in a horizontal chamber with chloroform -methanol - formic acid - water 10:4:1:0.95. Quantitative determination by absorbance measurement at 254 nm.

      Classification: 32e
      99 073
      Two-stage fractionation of a mixture of 10 pesticides by TLC and HPLC
      T. TUZIMSKI (Department of Physical Chemistry, Faculty of Pharmacy, Medical University, Staszica 6, 20-081, Lublin, Poland; ttuzim@panaceum.am.lublin.pl)

      J. Liq. Chromatogr. Relat. Technol. 28, 463-476 (2005). TLC of 10 pesticides (triadimenol, metazachlor, triadinefon, quinoxyfen, fenoxycarb, propaquizafob, piperonyl butoxide, quizalofop-P, buprofezin, oxyfluorfen) on silica gel with ethyl acetate - diisopropyl ether 1:9. Evaluation under UV 254 nm.The separated eight fractions were separated with NP and RP systems on RP-18 W and on cyano phase. Evaluation by densitometry and video densitometry. In addition preparative TLC on silica gel with a non-aqueous eluent.

      Classification: 29
      99 114
      TP-HPTLC and HPTLC methods for the estimation of carvedilol in bulk drug and pharmaceutical formulations
      L. J. PATEL*, B. N. SUHAGIA, P. B. SHAH, R. R. SHAH (*Shri B. M. Shah College of Pharmacy, Modasa 383315, India)

      Indian J. Pharm. Sci. 68 (6), 790-793 (2007). HPTLC of carvedilol in bulk drug and pharmaceutical formulations, on silica gel with ethyl acetate - toluene - methanol 2:8:7. Quantitative absorbance measurement at 242 nm. The hRf value of carvedilol was 65. The method was found to be linear over the concentration range of 50-300 ng/spot with recovery of 98.3-101.1%.The method was validated for accuracy and precision. Comparison with an HPLC method showed the HPTLC method to be advantageous regarding sample throughput.

      Classification: 32a
      99 153
      Application of Thin-Layer Chromatography to the investigation of oscillatory instability of selected profen enantiomers in physiological salt
      M. SAJEWICZ, R. PIETKA, A. PIENIAK, Teresa KOWALSKA* (*Silesian University, 9 Szkolna Street, 40-006 Katowice, Poland; kowalska@us.edu.pl)

      J. Liq. Chromatogr. Relat. Technol. 29, 2059-2069 (2006). TLC of S-(+)-ibuprofen, S-(+)-naproxen, and R,S-(+/-)-2-phenylpropionic acid on silica gel (prewashed with methanol - water 9:1 and impregnated with a 0.03 mol/L solution of L-arginine in methanol by dipping for 2 s at 22 +/- 2 °C) with acetonitrile - methanol - water 10:2:3 for naproxen and 20:4:3 for 2-phenylpropionic acid. Both mobile phases contained several drops of acetic acid to fix the pH at 4.8. Densitometric evaluation at 210 nm.

      Keywords: densitometry
      Classification: 32a
      100 028
      Two new derivatization reagents for planar chromatographic quantification of sucralose in dietetic products
      Gertrud MORLOCK*, M. A. VEGA-HERRERRA (*University of Hohenheim, Institute of Food Chemistry, Garbenstrasse 28, 70599 Stuttgart, Germany; g.morlock@uni-hohenheim.de)

      J. Planar Chromatogr. 20, 411-417 (2007). HPTLC of sucralose in dietetic products on silica gel impregnated with 0.1 M dipotassium hydrogen phosphate solution, and on amino phase with acetonitrile - water 17:3. Also a mixture of sucralose, sucrose, glucose, fructose was separated on amino phases with acetonitrile - water 3:1. Detection by dipping in 2-naphthol sulfuric acid reagent and aniline diphenylamine ortho-phosphoric acid reagent, followed by heating at 120 °C. Post-chromatographic derivatization on aluminium-backed amino plates was performed by heating the plate 190 °C for 20 min. Evaluation under UV light at 366 nm. For fluorescence enhancement the amino plate was dipped into a 1:2 solution of paraffin in n-hexane. Densitometric quantification by fluorescence measurement at 366 nm and by absorbance measurement at 500 and 405 nm.

      Classification: 10a
      100 050
      Detection of a covalent-ionic carbinolamine intermediate in aqueous media by SDTLC on silica gel plates
      Anamaria REVERDITO*, M.H. GARCÍA, A. SALERNO, O.A. LOCANI, I.A. PERILLO (*Department of Organic Chemistry, Faculty of Pharmacy and Biochemistry, University of Buenos Aires, 956 Junin St, 1113 Buenos Aires, Argentina; iperillo@ffyb.uba.ar)

      J. Planar Chromatogr. 20, 227-230 (2007). When the components of a reaction mixture cannot be quantified by UV-visible spectrophotometry because of overlapping of their absorption bands, the components can be separated and quantified by spectrodensitometric thin-layer chromatography (SDTLC). As example serves an aminolysis reaction mixture. TLC of imidazolidine and 1-(p-chlorophenyl)-2-phenyl-3-methylimidazoline on silica gel in a twin-trough chamber saturated for 5 min with chloroform - methanol 4:1 for the first development to a distance 55 mm, and after drying development with benzene to a distance of 65 mm. Densitometric scanning at 260 nm in absorption mode.

      Classification: 23e
      100 075
      A rapid RP-HPTLC densitometry method for simultaneous determination of major flavonoids in important medicinal plants
      P. BHANDARI, N. KUMAR, A. GUPTA, B. SINGH*, V. KAUL (*Natural Plant Products Division, Institute of Himalayan Bioresource Technology, Palampur, India, bikram_npp@rediffmail.com)

      J. Sep. Sci. 30, 2092-2096 (2007). HPTLC of flavonoids in Bauhinia variegata, Bacopa monnieri, Centella asiatica, Ginkgo biloba, Lonicera japonica, Rosa bourboniana, Rosa brunonii, and Rosa damascena on RP-18 with two-fold development with water (5 % formic acid) – methanol 7:3 and water (5 % formic acid) – methanol 1:1 as mobile phases. Quantitative determination by absorbance measurement at 280 nm. The hRf values of apigenin (1), quercetin (2), rutin (3), luteolin (4), and quercitrin (5) were 19, 29, 34, 51, and 63, respectively. Linearity was between 150 and 800 ng/zone for (1) and (3) and between 200 and 1000 ng/zone for (2), (4) and (5). The limits of detection and quantification for (1) – (5) were 30 and 166 ng/zone, 40 and 200 ng/zone, 20 and 150 ng/zone, 40 and 200 ng/zone, and 40 and 200 ng/zone, respectively. Recovery was between 97 and 99.8% for (1) – (5).

      Classification: 32e
      100 097
      The normal-phase retention behavior of some angiotensin-II receptor antagonists
      T.W. INGLOT*, K. DABROWSKA, G. MISZTAL (*Department of Medicinal Chemistry, Skubiszewski Medical University, Jaczewskiego 4, 20-090 Lublin, Poland; chemia.lekow@am.lublin.pl)

      J. Planar Chromatogr. 20, 293-301 (2007). TLC of candesartan, eprosartan, losartan, telmisartan, and valsartan on silica gel, aluminum oxide, amino-, cyano-, and diol-phase in a horizontal chamber in sandwich technique. Diol-phases were developed with hexane - isopropanol - formic acid 40:60:1, cyano-phases with hexane - dioxane - formic acid 30:70:1. Detection and quantification at 254 nm.

      Classification: 32a
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