Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

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      113 021
      Evaluation of goitrogenic and antithyroidal effect of the fern Adiantum capillus-veneris
      A. VIJAYALAKSHMI*, K. KUMAR (*Department of Pharmacognosy, SRM College of Pharmacy, SRM University, Kattankulathur, Tamil Nadu, India, aviji_1975@rediffmail.com)

      Rev. Bras. Farmacogn. 23, 802-810 (2013). HPTLC of quercetin (1) and gallic acid (2) in Adiantum capillus-veneris on silica gel with toluene - ethyl acetate - formic acid 5:4:1. Quantitative determination by absorbance measurement at 254 nm. The hRF values for (1) and (2) were 53 and 84. Linearity was in the range of 200-1600 ng/zone for both (1) and (2).

      Classification: 7, 8a
      113 054
      Simultaneous determination of sulphadiazine sodium and
      trimethoprim in medicated fish feed, fish tissues and in their veterinary pharmaceutical formulation by thin-layer chromatography–densitometry
      F. KHATTAB, S. RIAD, M. REZK, H. MARZOUK* (*Analytical Chemistry Department, Faculty of Pharmacy, Cairo University, Kasr El-Aini St., 11562 Cairo, Egypt, h.marzouk@yahoo.com)

      J. Planar Chromatogr. 27, 113-119 (2014). HPTLC of sulphadiazine sodium (1) and trimethoprim (2) in medicated fish feed, fish tissues, and in their veterinary pharmaceutical formulation on silica gel with chloroform - toluene - ethanol - glacial acetic acid 9:9:2:2. Quantitative determination by absorbance measurement at 270 nm. The hRF values for (1) and (2) were 48 and 16, respectively. Linearity was in the range of 100-2000 ng/zone for (1) and 100-1000 ng/zone for (2). The intermediate/interday/intra-day precisions were below 3 % (n=3). Mean recoveries for (1) and (2) were 99.6 and 97.9 %, respectively.

      Classification: 28a
      114 006
      Development of a work-flow for high-performance thin-layer chromatography data processing for untargeted metabolomics
      Coralie AUDOIN, S. HOLDERITH, Khadidja ROMARI, O. THOMAS, G. GENTA-JOUVE* (*Laboratory of Pharmacognosy and Chemistry of Natural Substances, UMR CRNS 8638 COMETE, Faculty of Pharmaceutical Sciences and Biology, Paris Descartes University, 75270 Paris Cedex 06, France, gregory.genta-jouve@parisdescartes.fr)

      J. Planar Chromatogr. 27, 328-332 (2014). HPTLC of crude extracts of micro-algae Dunaliella bioculata, Phaeodactylum tricornutum, and Scenedesmus obliquus on silica gel with dichloromethane - methanol 95:5. Data analysis of pictures digitally acquired at UV 254 nm and UV 366 nm included baseline correction, chromatogram alignment, principal component analysis (PCA) de-noising and diffusion drift correction. The workflow allowed to obtain a peak list containing hRF values, intensities and areas for statistical analysis.

      Classification: 3f, 4e
      117 053
      Marker compounds in Java tea characterized by HPTLC
      Tiên DO*, R. DE VAUMAS** (*CAMAG, Sonnenmattstrasse 11, 4132 Muttenz,
      Switzerland, tien.do@camag.com, **Extrasynthese, Impasse Jacquard – CS
      30062, 69727 Genay Cedex, France, rdv@extrasynthese.com)

      CBS 115, 13-15 (2015). HPTLC of Java tea (Orthosiphon species) and standards rhamnazin, apigenin-4,5,7-trimethylether, 6-methoxyluteolin, luteolin tetramethylether, scutellarein tetramethylether, tangeretin,_x000D_ eupatorin, eupatorin-5-methylether, and sinensetin on silica gel with toluene – ethyl acetate – methanol 11:8:1 with chamber saturation for 20 min to the migration distance of 70 mm. Detection under UV 254 nm and 366 nm. Densitometric evaluation by absorbance measurement at 254 nm. Elution of zones with TLC-MS Interface into a single mass spectrometer. Together with the already established sinensetin, scutellarein tetramethylether, eupatorin, and eupatorin-5-methylether were determined as specific markers suitable for the identification of Orthosiphon aristatus (Blume) Miq. by HPTLC. The presence of these four markers in the flavonoid profile is specific for Java tea.

      Classification: 8
      120 024
      Effect-directed fingerprints of 77 botanical extracts via a generic high-performance thin-layer chromatography method combined with assays and mass spectrometry
      S. KRÜGER, L. HÜSKEN, R. FORNASARI, I. SCAINELLI, Gertrud E. MORLOCK* (*Justus Liebig Univ. Giessen, Inst. of Nutrit. Sci., Chair of Food Sci., Heinrich-Buff-Ring 26-32, 35392 Giessen, Germany, gertrud.morlock@uni-giessen.de)

      J. Chromatogr. A 1529, 93-106 (2017). Presentation of the quantitative effect-directed profiles of 77 industrially and freshly extracted botanicals like herbs, spices, vegetables and fruits, widely used as food ingredients, dietary supplements or traditional medicine for their quality assessment with regard to potential health-promoting activities. Fast assignment of single active compounds and evaluation of their contribution to the overall activity, originating from a food or botanical sample by combination of HPTLC hyphenated with UV/Vis/FLD detection and effect-directed analysis, using the 2,2-diphenyl-1-picrylhydrazyl radical, Gram-negative Aliivibrio fischeri, Gram-positive Bacillus subtilis, acetylcholinesterase and tyrosinase assays. Characterization of bioactive compounds of interest eluted using an elution head-based interface by HPTLC-UV/Vis/FLD-EDA-ESI-(HR)MS method. Demonstration of the excellent quantification power of the method by applying for rosmarinic acid, contents ranged from 4.5 mg/g (rooibos) to 32.6 mg/g (rosemary), for kaempferol-3-glucoside from 0.6 mg/g (caraway) to 4.4 mg/g (wine leaves), and for quercetin-3-glucoside from 1.1 mg/g (hawthorn leaves) to 17.7 mg/g (thyme). The mean repeatabilities (%RSD, n=18) were ≤ 2.2 % for the three compounds and the mean intermediate precision (%RSD, n=3) was 5.2 % over three different days.

      Classification: 4e
      120 081
      Novel validated HPTLC method for the analysis of two binary mixtures containing tamsulosin hydrochloride with antimuscarinic agents
      E.I. EL-KIMARY* E.F. KHAMIS, S.F. BELAL, M.M. ABDEL MONEIM (*Fac. of Pharm., Dep. of Pharm. Anal. Chem., Univ. of Alexandria, Khartoum Square, El-Messalah, Alexandria 21521, Egypt, eman_elkimary@yahoo.com)

      J. Chromatogr. Sci. 56 (1), 81-91 (2018). HPTLC of mixures of tamsulosin hydrochloride (TAM) with either tolterodine tartrate (TOL) or solifenacin succinate (SOL) in bulk drug and in combined dosage forms on on silica gel with ethyl acetate – methanol – ammonia 120:80:1. Quantification by densitometry at 224 nm. Linearity was between 0.1-0.7, 0.4-4 and 1-6 μg/band for TAM, TOL and SOL, respectively.

      Classification: 32c
      121 077
      Stability-indicating HPLC and HPTLC methods for determination of agomelatine and its degradation products
      M.M. ABDELRAHMAN, I.A. NAGUIB, M.R. EL GHOBASHY, N.A. ALI* (*Medicolegal Authority, Justice Ministry, 114 Bairam El Tounsy St., El Sayeda Zeinab, 11647 Cairo, Egypt, n.aboyazeed@yahoo.com)

      J. Chromatogr. Sci. 56, 317-326 (2018). Development of an accurate, sensitive and highly selective stability-indicating method for simultaneous determination of agomelatine (AGM) and its forced degradation products (Deg I and II) by HPTLC on silica gel with chloroform – methanol – ammonia 90:10:1. Quantitative determination by densitometry at 230 nm over the concentration range of 0.2-1.2 μg/band for AGM in pure form and human plasma, and 0.1-1 μg/band for both Deg I and II. The method was successfully applied for the analysis of AGM in pharmaceutical formulations. Statistical comparison of the results to those obtained by HPLC revealed its high accuracy and good precision.

      Classification: 32c
      55 067
      Study of some quaternary ammonium compounds in grape berries of different vitis vinifera L
      O. JUHASZ, N. CONG, S. FATER, P. KOZMA

      varieties by analytical OPLC. Proc. Intern. Symposium on TLC with special Emphasis on OPLC, Szeged, 46 (1984). OPLC (OPTLC) of trimethyl-L-lysine on silica with propanol - methanol - 0.l M sodium acetate in water 20:3:30. Detection with Dragendorff reagent. Densitometry by absorbance at 525 nm.

      Classification: 18a
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