Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
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      98 038
      Determination of fructose, glucose and sucrose in beverages by high-performance thin layer chromatography
      J. SHERMA*, D. L. ZULICK (*Dept. Of Chem., Lafayette Coll., Easton, PA 18042-1782, USA)

      Acta Chrom. 6, 7-12 (1996). HPTLC of fructose, glucose and sucrose on silica gel with concentration zone. Impregnation of the layer (except concentration zone) by spraying with 0.1 M sodium bisulfate solution, followed by drying and spraying with citrate buffer of pH 4.8. Three-fold development with acetonitrile - deionized water 17:3 after chamber saturation. Visualization by spraying with 1-naphthol - sulfuric acid reagent and heating at 110 °C. Quantification by densitometry at 515 nm.

      Classification: 10
      98 077
      Analysis of carisoprodol tablets by HPTLC with visible absorbance densitometry
      J. FISHER, J. SHERMA* (*Dept. of Chem., Lafayette Col., Easton, PA 18042, USA)

      Acta Chrom. 11, 96-101 (2001). HPTLC of the muscle relaxant carisoprodol on silica gel uniplates with inorganic binder and fluorescent indicator, prewashed with dichloromethane – methanol 1:1, with chloroform – acetone 4:1 as mobile phase. Detection by spraying with conc. sulfuric acid – methanol 1:1 followed by heating at 150 ºC for 5 min. Quantitative determination by absorbance measurement at 550 nm. The method was applied to tablets containing carisoprodol as the only active ingredient and to tablets containing carisoprodol with aspirin and with aspirin plus codeine phosphate.

      Classification: 32a
      98 105
      Quantitative determination of sildenafil citrate in herbal medicinal formulations by high-performance thin-layer chromatography
      T. S. REDDY, A. S. REDDY, P. S. DEVI* (*Analytical Chemistry Division, Indian Institute of Chemical Technology, Tarnaka, Hyderabad-500007, India)

      J. Planar Chromatogr. 19, 427-431 (2006). HPTLC of sildenafil citrate on silica gel, pre-washed with methanol, with toluene - acetone - methanol 3:1:1 in a saturated twin-trough chamber. Quantitative determination by absorbance measurement at 312 nm. The method was validated in accordance with ICH guidelines on the validation of analytical methods.

      Classification: 32a
      99 019
      Determination of the effects of estivation and starvation on neutral lipids and phospholipids in Biomphalaria glabrata (NMRI strain) and Helisoma trivolvis (Colorado strain) snails by quantitative High Performance Thin-Layer Chromatography-densitometry
      M. M. WHITE, B. FRIED*, J. SHERMA (*Department of Biology, Lafayette College, Easton, PA 18042, USA; friedb@lafayette.edu)

      J. Liq. Chromatogr. & Relat. Technol. 29, 2167-2180 (2006). HPTLC of neutral lipids on prewashed silica gel with petroleum ether - diethyl ether - glacial acetic acid 80:20:1; and of methyl and steryl esters with hexane - petroleum ether (35-60°C) - diethyl ether - glacial acetic acid 50:25:5:1 in a twin trough chamber saturated for 20 min. Detection by spraying with a 50 % solution of phosphomolybdic acid in ethanol, followed by heating at 115°C for 10 min. Polar lipids were separated with chloroform - methanol - water 65:25:4. Detection by spraying with 10 % cupric sulfate solution, followed by heating at 140 °C for 10 min. Quantitative determination by absorbance measurement at 610 nm for neutral lipids and at 370 nm for polar lipids.

      Classification: 11c
      99 101
      Validated High Performance Thin Layer Chromatography Method for Simultaneous Estimation of Ofloxacin and Ornidazole in Tablet Dosage Form
      M. GANDHIMATI*, T. K. RAVI, Nilima SHUKLA (*Department of Pharmaceutical Analysis,Sri Ramkrishna College of Pharmacy, 395, Sarojini Naidu Road, Coimbatore 641044, India)

      Ind. J. Pharm. Sci. 68 (6), 838-840 (2006). HPTLC of ofloxacin and ornidazole in tablet dosage form on silica gel with n-butanol - ethanol - ammonia 5:5:4. Quantitative determination by absorbance measurement at 295 nm. The method was found to be linear in the concentrate range of 1-5 ng/spot with recovery of 99.5-102.5 % for both compounds. The method was validated for linearity, accuracy, precision, repeatability, and specificity.

      Classification: 32a
      99 146
      Separation and evaluation of free radical-scavenging activity of phenol components of Emblica officinalis extract by using an HPTLC-DPPH method
      O. POZHARITSKAYA, S. IVANOVA, A. SHIKOV*, V. MAKAROV (*Interregional Center “Adaptogen”, Piskarevsky prosp., St.-Petersburg, Russia, alexs79@mail.ru)

      J. Sep. Sci. 30, 1250-1254 (2007). HPTLC of Emblica officinalis extract on silica gel with ethyl acetate – formic acid – glacial acetic acid – water 10:1:1:2. Primary detection under UV 280 nm. Antiradical activity of individual components was estimated on intensity of disappearance of violet/purple background of plate after dipping in DPPH radical solution (0.5 mM in methanol) at room temperature for 90 s and that 30 s at 60 °C. Quantitative determination by absorbance measurement at 517 nm as negative peak. DPPH radical scavenging activity of emblicanins A and B was 7.9 and 11.2 times more active than that of ascorbic acid and 1.3 and 1.8 times more active than gallic acid, respectively.

      Classification: 32e
      100 021
      Densitometric TLC analysis of azaarenes in grilled meat
      Beata JANOSZKA (Medical University of Silesia, Faculty of Medicine, Department of Chemistry, Jordana 19, 41-808 Zabrze, Poland; rokchemm@infomed.slam.katowice.pl)

      J. Planar Chromatogr. 20, 221-26 (2007). TLC of seven azaarenes, acridine, benzo(h)quinoline, benzo(a)acridine, benzo(c)acridine, dibenzo(a,c)acridine, dibenzo(a,j)acridine, and dibenzo(a,h)acridine, on RP-18 in a horizontal chamber with dichloromethane - n-hexane - 2-propanol 60:40:1. After drying visualization under UV light at 254 and 366 nm. Quantification by densitometric fluorescence measurement at 380 nm. Limits of determination were from 0.04 to 0.30 ng/zone.

      Classification: 5b
      100 039
      Assessing the authenticity of absinthe
      Silvia GONZALEZ, J. GEISSER, Hannelore HEGER, D. LACHENMEIER* (*Chemisches und Veterinäruntersuchungsamt (CVUA) Karlsruhe, Weissenburgerstr. 3, 76187 Karlsruhe, Germany; Lachenmeier@web.de)

      CBS 97, 6-7 (2006). HPTLC of absinthe (a beverage of the wormwood plant, Artemisia absinthium) on silica gel with acetone - acetic acid (98 %) - toluene - dichloromethane 1:1:3:5 over 70 mm. Detection by dipping in a solution of acetic anhydride - sulphuric acid - ethanol 1:1:10 followed by heating at 104 °C for 5 min. Quantitative determination by absorbance measurement at 554 nm. The hRf value of absinthin was 64 and selectivity regarding matrix was given. Linearity was between 0.1 and 10 g/L. The limit of detection and quantification for absinthin was 0.05 and 0.11 g/L, respectively. The precisions were better than 13.5 % (intraday) and 15.8 % (interday).

      Classification: 15a
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