Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
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Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      103 040
      Thin-layer chromatography analysis of fructooligosaccharides in biological samples
      Katarina REIFFOVA*, Radomira NEMCOVA (*University of P.J. Safarik, Faculty of Natural Sciences, Institute of Chemistry Sciences, Moyzesova 11, 040 01 Kosice, Slovak Republic)

      J. Chromatogr. A 1110 (1-2), 214-221 (2006). Presentation of a rapid, simple and inexpensive method for the analysis of fructooligosaccharides as feed additives (prebiotics) in complicated biological samples with minimal pre-treatment. TLC of fructooligosaccharides in dietetic products and in samples from intestinal tract of monogastric animals on silica gel (impregnated with sodium acetate) with butanol - ethanol - water 5:3:2 with chamber saturation. Detection by spraying with diphenylamine - aniline - phosphoric acid in acetone. Quantitative determination by absorbance measurement at 370 nm.

      Classification: 10
      103 087
      Development of a densitometric method for the determination of cephalexin as an alternative to the standard HPLC procedure
      S. CORAN*, M. ALBERTI, V. GIANNELLINI, A. BALDI, G. PICCHIONI, F. PAOLI (*Dept. of Science Pharmaceutical, University of Firenze, Via G. Capponi 9, 50121 Firenze, Italy)

      J. Pharm. Biomed. Anal. 18, 271-274 (1998). HPTLC of cephalexin on silica gel (prewashed with the mobile phase) with ethyl acetate - acetic acid - water 7:2:1. Quantitative determination by absorbance measurement at 263 nm. The method was linear in the range of 200-1600 ng/spot, average recovery was 101 %. The analytical results obtained by HPTLC were comparable with the HPLC method of USP XXIII. The HPTLC method was suggested as alternative to the USP method considering the high throughput.

      Classification: 32a
      103 112
      Estimation of apigenin, an anxiolytic constituent, in Turnera aphrodisiaca
      S. KUMAR*, R. MADAAN, A. SHARMA (*S. D. College of Pharmacy, Barnala 148101, India)

      Ind. J. of Pharma Sci. 70(6), 847-851 (2008). HPTLC of apigenin in segregated parts (leaves, stems, flowers and fruits) of Turnera aphrodisiaca on silica gel with toluene - ethyl acetate 1:4. Quantitative determination by absorbance measurement at 336 nm. Flowers were found to contain maximum amount of apigenin whereas leaves contained the least. Apigenin contents in methanolic extracts of aerial plant parts were fourteen times lower than in acid hydrolyzed methanolic extracts, indicating the presence of most of apigenin in glycosidic form. The plant material collected in September showed maximum contents of apigenin.

      Classification: 32e
      103 138
      Efficient and sensitive method for quantitative analysis of 6-gingerol in marketed Ayurvedic formulation
      K.K. ROUT*, S.K. MISHRA (*Pharmacognosy and Phytochemistry Division, University Department of Pharmaceutical Sciences, Utkal University, Vani Vihar, Bhubaneswar 751004, Orissa, India; kd_rout@yahoo.co.in)

      J. Planar Chromatogr. 22, 127-131 (2009). HPTLC of 6-gingerol, extracts of Suprabha and market samples of ginger on silica gel (prewashed with methanol) with n-hexane - acetone 18:7 in a twin trough chamber saturated for 4 min at 20 +/- 4 °C and 36 +/- 3 % relative humidity. Quantitative determination by absorbance measurement at 286 nm. The limit of detection and quantification was 40 and 150 ng/band, respectively.

      Classification: 32e
      104 013
      A comparative study on several algorithms for denoising of thin-layer densitograms
      L. KOMSTA (Department of Medicinal Chemistry, Medical University of Lublin, Jaczewskiego 4, 20-090 Lublin, Poland)

      Anal. Chim. Acta 641 (1-2), 52-58 (2009). Comparison of classical filtering techniques (Savitzky–Golay, Adaptive Degree Polynomial Filter, Fourier denoising, Butterworth and Chebyshev IIR filters) and wavelet shrinkage (31 mother wavelets, 3 thresholding techniques and 11 decomposition levels) with the original noisy signal and a reference signal which was denoised experimentally by averaging 64 measurements. The best similarity to the reference signal was obtained with filters, however the signal was slightly oversmoothed. The wavelet shrinkage method gave less denoised signals. There was a significant influence of the thresholding technique and decomposition level, and best conditions were at level 2 or 3 and soft thresholding), whereas changing of the mother wavelet almost did not change the result. The presented results can be used as general recommendations for denoising densitometric fingerprints before applying further chemometric algorithms. The best choices were: Savitzky–Golay filter of appropriate window width (optimized against autocorrelation) or wavelet shrinkage with Haar wavelet, soft thresholding and high decomposition level.

      Classification: 4c
      104 040
      Determination of available lysine by planar chromatography
      M. VEGA*, M. ARANDA (*University of Concepcion, Faculty of Pharmacy, Department of Food Science, Nutrition and Dietetic, Barrio Universitario s/n Casilla 237, PO 403-0249 Concepcion, Chile; mveha@udec.cl)

      J. AOAC Int. 92, 699-702 (2009). HPTLC of a dinitrophenyl-lysine derivative (produced by incubation with 1-fluoro-2,4-dinitrobenzene and hydolyzation with hydrochloric acid) on silica gel (prewashed with methanol) with n-propanol - 25 % ammonia 7:3 in a twin trough chamber. Quantitative determination by absorbance measurement at 360 nm. The method was linear (r2 = 0.9991) in the range from 12.5 to 125.0 ng/band. Repeatability (%RSD) and intermediate precision (%RSD) in matrix were 0.8 % and 3.6 %, respectively. Recoveries of spiked samples at two levels ranged from 72 to 85 % with RSD from 3 to 8%. This method is a reliable, high throughput and low cost analytical method for the salmon feed industry.

      Classification: 18a
      104 067
      Development of validated HPTLC method for the estimation of buclizine hydrochloride in tablet dosage form
      B. ARUN*, A. SUGANTHI, A. FATHIMUNNISA, T. RAVI (*College of Pharmacy, Sri Ramakrishna Institute of Paramedical Science, Coimbatore, Tamil Nadu, India)

      Abstract No. F-276, 61st IPC (2009). HPTLC of buclizine hydrochloride on silica gel with methanol - chloroform - ammonia 8:1:1 %. Quantitative determination by absorbance measurement at 234 nm. The calibration curve was linear in the range of 100-700 ng/spot. The limit of detection and limit of quantification were 20 and 100 ng/spot, respectively.

      Classification: 32a
      104 083
      Rapid densitometric determination of Allium sativum in polyherbal oil formulations
      Nidhi DUBEY*, N. DUBEY, R. MEHTA, A. SALUJA (*Devi Ahilya Vishwavidyalaya, School of Pharmacy, Indore, M.P., India)

      60th Indian Pharmaceutical Congress PA-202 (2008). HPTLC of allyl disulphide (an active ingredient of Allium sativum, garlic) on silica gel with n-hexane. The hRf value was 52. Quantitative determination by absorbance measurement at 298 nm. The linearity range was 200-1200 ng/spot. Several polyherbal formulations containing garlic were analyzed with the proposed method using allyl disulphide as marker.

      Classification: 32e
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