Cumulative CAMAG Bibliography Service CCBS

Our CCBS database includes more than 11,000 abstracts of publications. Perform your own detailed search of TLC/HPTLC literature and find relevant information.

The Cumulative CAMAG Bibliography Service CCBS contains all abstracts of CBS issues beginning with CBS 51. The database is updated after the publication of every other CBS edition. Currently the Cumulative CAMAG Bibliography Service includes more than 11'000 abstracts of publications between 1983 and today. With the online version you can perform your own detailed TLC/HPTLC literature search:

  • Full text search: Enter a keyword, e.g. an author's name, a substance, a technique, a reagent or a term and see all related publications
  • Browse and search by CBS classification: Select one of the 38 CBS classification categories where you want to search by a keyword
  • Keyword register: select an initial character and browse associated keywords
  • Search by CBS edition: Select a CBS edition and find all related publications

Registered users can create a tailor made PDF of selected articles throughout CCBS search – simply use the cart icon on the right hand of each abstract to create your individual selection of abstracts. You can export your saved items to PDF by clicking the download icon.

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      115 067
      Quantitative determination of paroxetine in human serum by high-performance thin-layer chromatography
      S. MENNICKENT*, Cristina CIFUENTES, M. VEGA, Gisela RIOS, Marta DE DIEGO (*Department of Pharmacy, Faculty of Pharmacy, University of Concepcion, P.O. Box 237, Concepcion, Chile, smennick@udec.cl)

      J. Planar Chromatogr. 28, 229-233 (2015). HPTLC of paroxetine in human serum on silica gel with toluene - acetone - ethanol - ammonia 25 % in water 9:5:2:1. Quantitative determination by absorbance measurement at 294 nm. Linearity was between 0.01 and 0.14 ng/µL. The intra-day precisions were between 0.9 % and 2.2 % (n=5) and the inter-day precisions were between 1.0 % and 3.9 % (n=9). The LOD and LOQ was 0.3 and 0.6 ng/zone, respectively. Recoveries were between 91.5 % and 96.5 %.

      Classification: 32c
      118 082
      Simultaneous determination of menthol and eucalyptol by the densitometric HPTLC method in some external analgesic formulations
      P. ALAM*, S.I. ALQASOUMI, M.S. ABDEL-KADER (*Dep. of Pharmacognosy, Coll. of Pharm., Salman Bin Abdulaziz Univ., PO Box 173, Al-Kharj 11942, Saudi Arabia, prawez_pharma@yahoo.com)

      J. Chromatogr. Sci. 54 (1), 58-63 (2016). Description of a method for simultaneous determination of the two monoterpenes menthol and eucalyptol, contained in several analgesic pharmaceutical formulations for external use, by HPTLC on silica gel with hexane – ethyl acetate 4:1. The hRF value of menthol was 34 ± 4 and of eucalyptol 56 ± 4. Linearity was between 100–800 ng/zone (r2 = 0.9979) for menthol and 52–1107 ng/zone (r2 = 0.9937) for eucalyptol.

      Classification: 32c
      120 057
      Detection of steroids and selective androgen receptor
      modulators
      M. GRILL, Melanie BROSZAT* (*CAMAG, Sonnenmattstr. 11, 4132 Muttenz, Switzerland, melanie.broszat@camag.com)

      CBS 118, 1-4 (2017). Screening of steroids and selective androgen receptor modulators (SARMs) in bodybuilding supplements by HPTLC of methanedienone, ibutamoren, and ostarine on silica gel with n-heptane – ethyl acetate 1:1 (steroids) and dichloromethane – methanol 9:1 (SARMs) to the migration distance of 70 mm. Detection by immersion into (1) toluene sulfonic acid reagent (10 % in ethanol) followed by heating at 150 °C for 3 min, or (2) Seebach reagent (5 g phosphomolybdic acid, 2 g cerium sulfate and 12 mL sulfuric acid made up to a volume of 200 mL with water) followed by heating at 110 °C for 5 min. Detection under UV 254 nm, 366 nm and under white light. Densitometric evaluation by multi-wavelength scan at the respective absorption maxima. For example for the steroid testosterone the LOD was 8 ng/zone (absorbance measurement at 250 nm). Direct elution of target zones into the MS and analysis in positive ionization mode.

      Classification: 13
      121 067
      Stability-indicating high-performance thin-layer chromatographic determination of ondansetron in pure form and pharmaceutical formulations
      R. SARAYA*, R. SALAM, G. HADAD (*Department of Pharmaceutical Analytical Chemistry, Faculty of Pharmacy, Port Said University, Port Said, Egypt, dr_saraya@yahoo.com)

      J. Planar Chromatogr. 31, 122-128 (2018). HPTLC of ondansetron with chloroform ‒ methanol ‒ ethyl acetate 7:2:1. Quantitative determination by absorbance measurement at 302 nm. The hRf value for ondansetron was 67. Linearity was in the range of 25-500 ng/zone. The intermediate precision was below 1 % (n=3). The LOD and LOQ were 5 and 15 ng/zone, respectively. Average recovery was 100.3 %. The method allowed the separation of the drug from its different degradation products.

      Classification: 23e, 32a
      55 026
      HPTLC separation of PGF2, PGE1, PGE2, PGA1, prostaglandins and quantitative determination in situ by induced fluorescence
      P. BRUNO, M. CASELLI, C. GARAPPA, A.TRAINI

      J. High Resol. Chromatogr. 7, 593-595 (1984). HPTLC of the title compounds on silica with ethanol - ether - ethyl acetate - chloroform 12:33:22:33. Detection by spraying with 5 % cupric acetate in 15 % aqueous phosphoric acid and heating at 110 °C for 10 minutes. Fluorometry at 366 nm. Sensitivity 1-10 ng.

      Classification: 11b, 32f
      55 091
      Comparative analysis of tocopherols by thin-layer chromatography and high-performance liquid chromatography
      B. RUGGERI, T. WATKINS, R. GRAY, R. TOMLINS

      J. Chromatogr. 291, 377-383 (1984). TLC of tocopherols on silica with hexane - isopropylether 85:15 or acetone - benzene - water 91:30:8. Detection with 10 % copper(II)sulfate-phosphoric acid followed by charring at 190" for 10 minutes. Quantitative scanning by absorbance at 350 nm. TLC was found advantageous over HPLC when analyzing a large number of samples.

      Classification: 27
      56 020
      Photothermal deflection densitometer for thin-layer chromatography
      T. CHEN, M. MORRIS

      Anal. Chem. 56, 19-21 (1984) Description of TLC densitometer based on photothermal deflection of an argon ion laser of 20 mW at 488 nm as the source and a 2-MW He-Ne laser as the probe. System demonstrated with a chronatogram of 1,2-naphthoquinone, phenonthrenequinone and -ionone. Detection limit 30 ng -7.5 pg.

      Keywords: densitometry
      Classification: 3f
      56 129
      Modification of the rapid screening method for aflatoxin in corn for quantitative use
      J. SPILMANN

      J.A.O.A.C. 68, 453-456 (1985). Quantitative determination of aflatoxins B1, B2, G1, G2 on silica with anhydrous ether, then after drying with chloroform - acetone 9:1. Detection by UV. In situ densitometry.

      Classification: 28b
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